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Thermo Scientific 50131250, Руководство по эксплуатации


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Thermo Scientific Barnstead GenPure with xCAD 

 

Ultrapure water system

 

 

18

8.1  Flow chart, GenPure Standard with xCAD 

 
 

 

 
 
A-F1 Filter 

cartridge 

A-F2 Sterile 

filter 

A-P1 Circulation 

pump 

FIS400 Digital 

flowmeter 

QIA 300 

Conductivity, feedwater 

QIA 301 

Conductivity, ultra pure water 

TIA 500 

Temperature sensor 

V1 Pressure 

reducer 

V2 Check 

valve 

V3 Solenoid 

valve 

V4 

Rinsing solenoid valve 

V5 

Check valve 1 bar 

 
 
 

Содержание 50131250

Страница 1: ...ons Thermo Scientific Barnstead GenPure Water Purification System with xCAD Serial no These Operating Instructions must be read prior to installation and start up 50131281 Stand 11 12 Rights to technical changes reserved ...

Страница 2: ...e function Ultrapure water system type GenPure with xCAD GenPure UF with xCAD GenPure UV with xCAD GenPure UV UF with xCAD GenPure UV TOC with xCAD GenPure UV TOC UF with xCAD article number bench version 50131286 50131250 50131254 50131252 50131296 50131298 wall version 50131300 50131302 50131317 50131315 50131321 50131323 The agreement with further valid guidelines regulations following for the ...

Страница 3: ...ed in us Before you start to install and operate your pure water system please carefully read the infor mation given in these Operating Instructions on how to correctly carry out installation and how to properly operate the system This is particularly important as we the manufacturer cannot accept liability for any damage occurring as a result of improper operation of this system or from use of it...

Страница 4: ...xCAD 20 8 4 Flow chart GenPure UV UF with xCAD 21 8 5 Flow chart GenPure UV TOC with xCAD 22 8 6 Flow chart GenPure UV TOC UF with xCAD 23 9 Setting up the system 24 9 1 Installation area 24 9 2 Connectors 25 9 3 General setting up of the system bench version xCAD 26 9 4 Setting up the system wall version xCAD 27 9 5 Wall mounting GenPure system 30 9 6 Mounting the power pack voltage supply 31 9 7...

Страница 5: ... sending interval 45 12 2 8 Selecting the language 46 12 2 9 Switching units 46 12 2 10 Switching temperature compensation on or off 46 12 2 11 Entering the system type and serial number 47 12 2 12 Water dispensing via volume control 47 12 3 Printer output 48 12 3 1 Standard messages 48 12 3 2 Code messages 48 12 3 3 Fault messages 49 13 Maintenance 50 13 1 Maintenance intervals 51 13 2 Replacing ...

Страница 6: ...ation sign Protective conductor connection Connect the power supply to an electrical socket with a protective connection The information provided in these operating instructions is only valid for the system which has the serial number which is to be entered on the front page Please enter the serial number of your GenPure with xCAD system in the space provided on the front page Read the serial numb...

Страница 7: ...tem for damage 3 2 Complaints Should the system have been damaged during transport Immediately contact the post office railway or forwarding agent Keep the packaging including the outer cardboard box for a possible inspection and or return shipment 3 3 Packaging and return shipment Whenever possible use the original packaging and packing materials Should these no longer be available Pack the syste...

Страница 8: ...the ultra pure water system installation area The feedwater pressure must be at least 0 1 bar and at most 6 bar Should the feed water pressure be higher then an additional pressure reducer must be installed Water purification systems must have a safety device acc to DIN EN 1717 to protect the tap water from contamination A grounded 100 240V 50 60Hz socket must be available The installation area mu...

Страница 9: ...stem 9 The term of the guarantee is12 months Never look directly at a switched on UV lamp because UV light endangers eyesight Never switch the UV lamp on when is has been taken out of the metal cylinder Only authorized personnel are to carry out UV lamp replacement ...

Страница 10: ...ly pure particle free and sterile filtered ultra pure water To ensure long service lives of the high quality purification media this type of ultra pure water system must be fed with water from upstream pre purification steps reverse osmosis ion ex change distillation 5 1 Application areas Analytical techniques in laboratories HPLC High Performance Liquid Chromatograhy IC Ion Chromatography ICP Ind...

Страница 11: ...Basic system UV photooxidation and TOC meas urement ultrafiltration with xCAD bench version GenPure UV TOC UF article no 50131323 Basic system UV photooxidation and TOC meas urement ultrafiltration with xCAD wall version Please check your version against the article number given on the delivery note 1x GenPure with xCAD acc to the version Article no 5013xx incl Assembly kit for bench and wall vers...

Страница 12: ...connector kit Article no 25 0075 consisting of Union nut R 3 4 Article no 14 0003 Insert R 1 4 Article no 14 0189 Screwed connector R 1 4 Article no 14 0075 Gasket R 3 4 Article no 21 5008 PE Hose 8 mm o d 2 m Article no 18 0036 Dirt trap sieve for union nut R 3 4 Article no 14 0390 ...

Страница 13: ...al filter and if appropriate the final filter Temperature 2 35 C Pressure 0 1 6 bar Product water quality Standard UV UF UV UF UV TOC UV TOC UF Resistance Reference temperature 25 C MΩxcm at 25 C 18 2 18 2 18 2 18 2 18 2 18 2 TOC ppb 5 10 1 5 5 10 1 5 1 5 1 5 Bacteria CFU ml 1 1 1 1 1 1 Bacterial En dotoxines EU ml 0 001 0 001 0 001 Particles 0 2 µm 1 ml 1 ml 1 ml 1 ml 1 ml 1 ml Flow rate L min up...

Страница 14: ...Pure with xCAD Ultrapure water system 14 Dimensions xCAD bench version Height approx 725 mm Width 260 mm Depth approx 530 mm Weight 12 kg Dimensions xCAD wall version Height approx 655 mm Width 260 mm Depth approx 530 mm Weight 5 kg ...

Страница 15: ...3 8 A System connection DC 24 V 80 W Serial interface RS 232 Protection Class Class II external SMPS certified as Class I Electrical connections xCAD 2x SUB D socket 25 pin Airborne sound emission Sound pressure level 49 db A Ambient conditions DIN EN 61010 1 VDE 0411 1 2011 02 Usage Indoor rooms Height Up to 2000 m Temperature range From 5 C to 40 C Relative humidity Maximum relative humidity 80 ...

Страница 16: ...r Pressure reducer NBR Pump head Nylon with glass fibre UV Lamp High purity quartz UV Housing Stainless steel Filter cartridge PP UF Housing Polycarbonate Rinsing solenoid valve PA Dispensing valve PVDF Conductivity measuring cell POM stainless steel Distributor block POM Connections POM Hoses PE Gaskets EPDM ...

Страница 17: ... TOC UV TOC UF with xCAD Tap water that has been pretreated upstream by reverse osmosis ion exchange or distillation passes through a pressure reducer and into the GenPure ultra pure water system where the conductivity is monitored A pump forces this feedwater through UV photooxidation after which the conductivity is again measured to determine the TOC value The water then flows through the filter...

Страница 18: ...ndard with xCAD A F1 Filter cartridge A F2 Sterile filter A P1 Circulation pump FIS400 Digital flowmeter QIA 300 Conductivity feedwater QIA 301 Conductivity ultra pure water TIA 500 Temperature sensor V1 Pressure reducer V2 Check valve V3 Solenoid valve V4 Rinsing solenoid valve V5 Check valve 1 bar ...

Страница 19: ... A F1 Filter cartridge A F2 Sterile filter A P1 Circulation pump A UV1 UV Photooxidation FIS400 Digital flowmeter QIA 300 Conductivity feedwater QIA 301 Conductivity ultra pure water TIA 500 Temperature sensor V1 Pressure reducer V2 Check valve V3 Solenoid valve V4 Rinsing solenoid valve V5 Check valve 1 bar ...

Страница 20: ... F1 Filter cartridge A F2 Sterile filter A F3 Ultrafiltration module A P1 Circulation pump FIS400 Digital flowmeter QIA 300 Conductivity feedwater QIA 301 Conductivity ultra pure water TIA 500 Temperature sensor V1 Pressure reducer V2 Check valve V3 Solenoid valve V4 Rinsing solenoid valve V5 Check valve 1 bar ...

Страница 21: ...cartridge A F2 Sterile filter A F3 Ultrafiltration module A P1 Circulation pump A UV1 UV Photooxidation FIS 400 Digital flowmeter QIA 300 Conductivity feedwater QIA 301 Conductivity ultra pure water TIA 500 Temperature sensor V1 Pressure reducer V2 Check valve V3 Solenoid valve V4 Rinsing solenoid valve V5 Check valve 1 bar ...

Страница 22: ... Sterile filter A P1 Circulation pump A UV1 UV Photooxidation FIS400 Digital flowmeter QIA 300 Conductivity feedwater QIA 301 UV Intensity QI 302 Conductivity TOC measurement QIA 303 Conductivity ultra pure water TIA 500 Temperature sensor V1 Pressure reducer V2 Check valve V3 Solenoid valve V4 Rinsing solenoid valve V5 Check valve 1 bar ...

Страница 23: ...ter A F3 Ultrafiltration module A P1 Circulation pump A UV1 UV Photooxidation FIS400 Digital flowmeter QIA 300 Conductivity feedwater QIA 301 UV Intensity QI 302 Conductivity TOC measurement QIA 303 Conductivity ultra pure water TIA 500 Temperature sensor V1 Pressure reducer V2 Check valve V3 Solenoid valve V4 Rinsing solenoid valve V5 Check valve 1 bar ...

Страница 24: ...e wall mounted A smooth wall is required Check the statics of the wall it must be sufficiently loadable for weight see Technical specifications Floor drain DN 50 Free gravity fall to drain Should no such floor drain be available then for safety reasons a water watcher ar ticle no 16 0129 must be installed Free gravity fall to drain must be ensured Safety socket 100 240V 50 60Hz Sufficient working ...

Страница 25: ...d 5 Ultra pure water connector 6 mm o d to xCAD 6 Ultra pure water connector 4 mm o d to xCAD 7 Connector for optional printer art no 09 2207 8 Mains plug 100 240V 50 60Hz power supply Connectors xCAD 1 Connector for 25 pin sockets system control 2 Connector for 25 pin sockets system control 5 Ultra pure water connector 6 mm o d to GenPure 6 Ultra pure water connector 4 mm o d to GenPure 9 Dispens...

Страница 26: ...dge in the guide in the system plug the quick connect connectors on so that they audibly click into position and put the cartridge cover back on 4 Connect the 8 mm o d hose that is provided in the connector kit to feedwater connector 3 of the GenPure system 5 Now make a pressureless connection between the 8 mm o d hose 4 and the drain The drain to the sewer must be max Are 1m above the rinsing wat...

Страница 27: ...d to use the sterile filter 10 that is standardly supplied screw it in the R 1 4 female thread outlet of the dispensing valve 9 of the xCAD 10 Connect the mains plug 8 of the voltage supply to an earthed 100 240V 50 60Hz socket 11 Open the feedwater supply 12 Check all connections for leaks 9 4 Setting up the system wall version xCAD Proceed as follows to set your GenPure with xCAD wall version ul...

Страница 28: ...schnitt in der Wand für Kabel und Schlauchdurchführung nach hinten possible wall cut outs for cable and hose taken out at the back 3 Bore the holes for the 6 mm plugs and make the necessary cut out 4 Fix the wall mount in position with the plugs and screws provided 5 Lead the 25 pin plugs extension cables and 4 mm and 6 mm o d hoses through the wall to the wall mount and connect the 25 pin plug 1 ...

Страница 29: ... in the connector kit to the feedwater connector 3 of the GenPure system 13 Now use the 8 mm o d hose to make a pressureless connection between the system connector 4 and the drain The drain to the sewer must be max Are 1m above the rinsing water connector of the Unit 14 Plug the two extension cables with 25 pin plugs in the sockets 1 and 2 of the GenPure system and screw them tight 15 If you inte...

Страница 30: ... frill 8 mm or 5 16 inch to make the two holes in the wall that are required as shown in the diagram above Plug the nylon S8 dowels that are supplied in the assembly kit in the holes Screw the 5 2 x 50 mm screw hooks that are also supplied in the assembly kit in the dowels Lift the GenPure system 2 people are required for this and hang the back side of it on the screw hooks ...

Страница 31: ...back of the power pack as shown in the above Figure Stick the universal adapter to a smooth wall surface or screw it to the wall using the dowels and screws supplied in the assembly kit When the universal holder and universal adapter have been fitted hang the power pack in Plug the connecting cable appliance cable in the power pack socket Connect the power pack to the ultra pure water system Conne...

Страница 32: ...Thermo Scientific Barnstead GenPure with xCAD Ultrapure water system 32 9 7 Examples of system set ups Connection to a pretreatment Connection to a Pacific TII system with storage tank ...

Страница 33: ...entific Barnstead GenPure with xCAD Ultrapure water system 33 Connection to a storage tank Caution When connected to a storage tank the system must be switched to nonstop operation for ultra pure water dispensing ...

Страница 34: ...ystem on by pressing this button After a compulsory rinse the sys tem switches to the last operating mode To vent air from the system switch the system 3 times successively to Rinsing in the menu and collect and discard approx 5 litres of water each time The ultra pure water limiting value can be gone below during this procedure Use this NONSTOP key to switch the system to the Nonstop operating mo...

Страница 35: ...Thermo Scientific Barnstead GenPure with xCAD Ultrapure water system 35 11 Operating elements Intervall ppb 18 2 MΩxcm 18 5 C UV TC ...

Страница 36: ... ended 2 h When Nonstop operation is manually stopped by a press on the Interval key then the UV lamp is not switched off until it has been burning for 0 5 hours During the time that the UV lamp is burning the intensity of the UV light in monitored The dis play of the UV intensity is made in the menu The TOC value is also displayed User menu All of the measured values operating times and limiting ...

Страница 37: ...1 25 MΩxcm Limit value feed 2 0 µS cm 12 1 2 Ultra pure water limiting value Two presses on the menu key in this menu allow the fault display for the pure water limit ing value and the pure water limiting value to be set As soon as the fault display is switched on the fault will be displayed both in Stand by mode and in Production mode When the fault display is switched off the fault is only displ...

Страница 38: ... counter The operating time counter for the filter cartridge is set in this menu by a fourth press on the menu key and the entry of a valid serial number for the filter cartridge The display shows Ser No Cartridge Press Enter 12 1 5 Rinsing A fifth press on the menu key in this menu allows rinsing to be carried out if this is neces sary Triggering is made by confirming the requirement with a press...

Страница 39: ...hat has been set in the OEM menu When the half of the disinfection time has passed the rinsing solenoid valve opens and stays open up to the end of the dis infection process The New filter cartridge Install one message is given when the disin fection process has finished On confirming this with Enter the system returns to the last operating mode During disinfection the count down of the disinfecti...

Страница 40: ...look through the faults in the fault storage Should several faults have occured then two faults each with date and time are shown in the display Appropriate pressing of the arrow keys brings previous and subsequent faults to display A press on the menu key or the Enter key returns the display to the last operating mode The display shows Error history Press enter Show of faults in the fault storage...

Страница 41: ...to the settings can only be carried out when a correct code from the Assignment Table that follows is entered and confirmed with the Enter key The unlocking remains active for 5 minutes Each access via the code is issued to the printer RS 232 complete with date time and abbreviated code number Code 0001 corresponds to code 150 Code 0002 to code 250 etc The display shows Code Press enter 0000 Code ...

Страница 42: ...d GenPure with xCAD Ultrapure water system 42 Assignment Table for code numbers that allow the system to be unlocked Code no Printer output Person 150 0001 250 0002 350 0003 450 0004 550 0005 650 0006 750 0007 850 0008 950 0009 ...

Страница 43: ... menu prompt can be worked on To simplify changing settings press the UV key to select the number in a numerical value which you want to change Now use the arrow keys to enter the wanted number from 0 to 9 at that selected position A press on the menu key takes you to the next menu prompt The OEM menu call display shows OEM Menu 12 2 1 Setting the maximum operating temperature The maximum temperat...

Страница 44: ...etting range 10 60 sec The display shows OEM Menu Rinse time 30 sec 12 2 3 Changing the disinfection time Basic setting 30 min Setting range 15 90 min The display shows OEM Menu Disinfect time 30 min 12 2 4 Setting the interval pump time Basic setting 5 min Setting range 1 30 min The display shows OEM Menu Pump interval 05 min ...

Страница 45: ...he real time clock Basic setting The actual date Setting range 1 12 Month 1 31 day 0 24 h 0 60 min The display shows OEM Menu Day 30 Month 12 Year 2008 Hour 12 Min 30 12 2 7 Setting the sending interval In this menu the sending interval is set for transmissions of measured values and fault messages to the RS 232 interface Basic setting 1 hour Setting range 0 5 12 hours The display shows OEM Menu S...

Страница 46: ...nch German The display shows OEM Menu Language English 12 2 9 Switching units Basic setting Resistance MΩxcm Setting range Resistance MΩxcm Specific electrical resistance MΩ cm The display shows OEM Menu µS cm MΩ cm MΩxcm 12 2 10 Switching temperature compensation on or off Basic setting on Setting range on off The display shows OEM Menu Temp comp On ...

Страница 47: ...me is shown in line 2 of the dis play This is the volume of ultra pure water that was last dispensed A single press on the push button on the grip allows the litre volume to be changed within the range from 0 01 bis 65 5 litres by means of the arrow keys The UV key can be used to position the cursor at a particular number that you wish to change A second press on the push button causes dispensing ...

Страница 48: ...3 04 08 15 15 GenPure Standard S No 3988 08 Interv TC on UV off LF1 18 2 MΩxcm LF2 10 0 MΩxcm LF3 0 000 MΩxcm Temp 16 8 C TOC 0 ppb UV Intens 0 The standard record includes all measured values With systems that are not equipped with TOC measurement and UV intensity measurement 0 is given as measured value 12 3 2 Code messages Whenever a code number is entered in the system control and confirmed wi...

Страница 49: ...stem 49 12 3 3 Fault messages When a fault message is shown in the display e g for the ultra pure water limiting value then the fault message is printed out at the end of the sending interval Print out e g 03 04 08 17 09 GenPure Standard S No 3988 08 Lim val pure w ...

Страница 50: ...ty of the guarantee this is only to be carried out by a service professional which is expressly authorized to do such work The staff who are trained on and operate the system are committed to carry out daily weekly checks The maintenance work specified on the maintenance record supplied with these Operating In structions should to be carried out weekly CAUTION The cleaning and disinfection of your...

Страница 51: ...erformance Material Flow chart no Article no Interval Filter cartridge F1 09 2005 12 Months Sterilefiltercapsule F2 09 1003 12 Months Ultrafiltration membrane F3 50133980 24 Months Please keep in mind that the life of your consumables is directly dependent on the quality of the feed water and the amount of water used daily The interval is contingent on the feedwater quality so that a shorter one m...

Страница 52: ... the filter car tridge and close the connectors with the stoppers you have saved 6 Draw the spent filter cartridge out from the guide and push the new filter cartridge in 7 Remove the stoppers from the new filter cartridge and save them 8 Fit the quick connects to the filter cartridge so that they audibly click into position 9 Replace the cartridge cover 10 Open the supply of feedwater 11 Switch t...

Страница 53: ...r the system 4 Unscrew the stopper from the disinfectant cartridge fill the cartridge with water then empty the contents of a box respectively a syringe of the cleaning solution into the wa ter Important For effective disinfection the cartridge must be completely filled with water 5 Screw the stopper back on the disinfectant cartridge and connect the cartridge in the system as under Changing the f...

Страница 54: ...Thermo Scientific Barnstead GenPure with xCAD Ultrapure water system 54 ...

Страница 55: ... must be properly disposed of It can be returned to the manufacturer for safe disposal according to EEC Guideline 2002 96 EC We therefore request our customers in Germany and other member States in the European Economic Area to contact our local service centre or our headquarters Thermo Electron LED GmbH Stockland 3 D 56412 Niederelbert Germany WEEE Reg no DE 12471402 In countries outside of the E...

Страница 56: ...ter cartridge with a new one System control no longer reacts Improper operation Unplug the mains plug for 5 seconds Water flows out Leaky hose connection Feedwater pressure 6 bar Check and seal the hose connection Install a pressure reducer Dispensed water flow rate is too low UF Module blocked Pre pressure too low Internal pressure too low Replace UF module Increase pre pressure Readjust pressure...

Страница 57: ...o low Feedwater temperature too high Reduce temperature by running water off Reduce interval pump time Check and suit the limiting value Reduce feedwater temperature Fault message Measuring cell LF1 Measuring cell cable break System control defect Conductivity of ultra pure water ouside measuring range Replace measuring cell Replace system control see Conductivity 18 2 MΩxcm Fault message Measurin...

Страница 58: ...rd 16 0364 10 Microprocessor system control interface 50131346 11 Booster for UV lamp optional 22 0088 12 QIA303 TIA500 Conductivity measuring cell ultra pure water Conductivity measuring cell temperature sensor 50133992 13 V2 Check valve 15 0009 14 QIA301 UV Intensity sensor optional 16 0222 15 V5 Check valve 15 0019 16 Fuseholder for glas tube fuse 5x20mm Glas tube fuse 5x20mm 3 15 A slow 501339...

Страница 59: ... system 59 16 2 xCAD 19 18 20 17 No R I no Article designation Article no 17 Microprocessor system control 26 0025 18 A F2 Sterile filter capsule 0 2 m 09 1003 19 Press button 16 0370 20 V3 Solenoid valve 15 0101 Extension cable SUB D 25 pin GenPure xCAD 16 0375 ...

Страница 60: ...mo Scientific 275 Aiken Road Asheville NC 28804 USA Enquiries from USA Canada Sales 1 866 984 3766 Service 1 800 438 4851 Enquiries from Latin America Sales 1 866 984 3766 Service 1 866 984 3766 Enquiries from Asia China Sales 86 10 8419 3588 Service Toll free 8008105118 Support Mobile 4006505118 or 86 10 8419 3588 India Sales 91 22 6716 2200 Service Toll free 1 800 22 8374 or 91 22 6716 2200 Japa...

Страница 61: ... Straße 1 D 63505 Langenselbold Phone Sales Toll free 0800 1 536 376 or 49 6184 90 6940 Service Toll free 0800 1 112110 or 49 6184 90 6940 E Mail info labequipment de thermoftsher com Italy Sales 39 02 95059 341 Service 39 02 95059 250 Netherlands Sales 31 76 579 5555 Service 31 76 579 5639 Russa CIS Sales 7 812 703 4215 Service 7 812 703 4215 Spain Portugal Sales 34 93 223 0918 Service 34 93 223 ...

Страница 62: ...Thermo Scientific Barnstead GenPure with xCAD Ultrapure water system 62 18 Terminal assignment ...

Страница 63: ...a pure water volume flow L h Tempe rature C TOC value ppb UV intensity UV lamp operating time h Last change of filter cartridge Last cleaning disinfection Last change of pretreatment Remarks Signature Any false entry is considered to constitute a falsification of documents The following points are to be observed to safeguard the quality of the system 1x Weekly enter measured values The pretreatmen...

Страница 64: ...15 Spain Portugal 34 93 223 09 18 Switzerland 41 44 454 12 12 UK Ireland 44 870 609 9203 Asia Australia 61 39757 4300 China 86 21 6865 4588 or 86 10 8419 3588 India toll free 1800 22 8374 India 91 22 6716 2200 Japan 81 45 453 9220 New Zealand 64 9 980 6700 Other Asian countries 852 2885 4613 Countries not listed 49 6184 90 6940 2011 Thermo Fisher Scientific Inc All rights reserved All trademarks a...

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