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Properties of the  TITRONIC

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universal  

Piston Burette

1.1 General

The TITRONIC

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  Piston Burette which requires just the space of a DIN A4 sheet can be used to

carry out all common titrations, dosing processes as well as incremental dosing in a simple manner.

The accurately functioning dosing system meets the essential precondition for correct titration and dosing.
In addition to the high-precision glass cylinder made of DURAN

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 borosilicate glass, the play-free mo-

tor/spindle system ensures correct dosing, incremental dosing, and titration results.

Incremental dosing offers furthermore the use in balance reactions and as an electronic dropping funnel.

The very simple operator prompting allows you uncomplicated working. The display will ask you to select
the respective function or to set the corresponding parameters. Even during the execution of a function the
burette’s display will keep you at any time informed about its present status.

The two RS-232-C interfaces enable series daisy chaining of more than one  TITRONIC

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  Piston

Burettes for connection to a computer (PC).

The TM 96 Stirrer and the TZ 3665 Stand Rod attach directly to the TITRONIC

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  Piston Burette.

The electrical contacts (15 V =) connect automatically when the stirrer is being installed. This means that
the electrical power for the TM 96 Stirrer is supplied from the  TITRONIC

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  Piston Burette.

All parts coming into contact with the titration and dosing solutions are made of chemically resistant mate-
rials. Analysis accuracy is guaranteed by the high-precision glass cylinder and the spindle for the piston
feed. The controlled three/two-way valve, the easy-to-read consumption display with its additional status
messages, the stand/stirrer system, and the practical manual key button make the TITRONIC

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Piston Burette a device with comfortable use properties.

Within the present operating instructions, the TITRONIC

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  Piston Burettes with 20 ml or 50 ml

cylinder are collectively referred to as TITRONIC

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  Piston Burette.

1.2 Dosing and titration solutions

To save titration solution and to render the disposal of the chemicals after the analysis as simple as possi-
ble, we recommend to select any titration-solution consumption between 5 ml and a 15 ml for titration

Solutions to be used:

In practice, any solutions and liquids with the viscosity of < = 10 mm² / s can be used, such as e.g. con-
centrated sulphuric acid. However, chemicals attacking glass, PTFE, or FEP, or which are explosive, such
as hydrofluoric acid, sodium azide, or bromine must not be used! Suspensions with a high solid contents
may block or damage the dosing system.

General rules:

The respectively applicable safety guidelines on handling chemicals are to be observed under all circum-
stances. This applies in particular to inflammable and/or etching liquids.

Notes:

When used in this text, the following signs have the following meaning:

!

= note on possible danger

<< ... >> = contents of the display
< ....... > = key

&

= please refer to, for instance, figure, chapter, operating instructions

Содержание TITRONIC universal

Страница 1: ...sanleitung Kolbenb rette TITRONIC universal Operating Instructions Piston Burette TITRONIC universal Mode d emploi Burette piston TITRONIC universal Manual de instrucciones Bureta de mbolo TITRONIC un...

Страница 2: ...iversal without changing the described properties Mode d emploi Page 49 72 Instructions importantes Pri re de lire et d observer attentivement le mode d emploi avant la premi re mise en marche de la B...

Страница 3: ...pplier s Certificate We certify that the equipment EN ISO 9001 part 4 10 4 Final inspection and testing and that the specified requirements for the product are met Certificat du fournisseur Nous certi...

Страница 4: ...TRONIC universal Piston Burette 33 4 1 Keys and contrast 33 4 2 Switch on image setting the filling time 33 4 3 Selecting the national language 34 4 4 Rinsing and initial filling 34 4 5 Filling 35 4 6...

Страница 5: ...26 Fig 1 TITRONIC universal Piston Burette with TM 96 Stirrer with manual key button with stand with electrode burette tip holder with burette tip TZ 1503 with bottle top TZ 2005...

Страница 6: ...contact with the titration and dosing solutions are made of chemically resistant mate rials Analysis accuracy is guaranteed by the high precision glass cylinder and the spindle for the piston feed Th...

Страница 7: ...ieht bereinstimmt mit den Normen und mit dem normativen Dokument We declare under our sole responsibility that the product Piston Burette TITRONIC universal to which this declaration relates is in con...

Страница 8: ...ading and 2 trailing decimal digits with a resolution of 0 01 ml Display Matrix LCD display 69 x 39 mm 64 x 128 pixels with background lighting contrast can be set using a knurled wheel Connections Ma...

Страница 9: ...ONIC universal Piston Burette from the place of work Examples for the assumption that a safe operation is no longer possible the package is damaged the TITRONIC universal Piston Burette shows visible...

Страница 10: ...he operating voltage of the TITRONIC universal Piston Burette matches the mains voltage The operating voltage is indicated on the specification plate on the bottom of the TITRONIC universal Piston Bur...

Страница 11: ...off Mains cable Interface 2 RS 232 C Connector for manual key button Interface 1 RS 232 C The transfer parameters for the RS 232 C interface can be selected according to RS 232 C interface chapter Att...

Страница 12: ...ered using the keyboard In dialogue mode the display shows which active keys can be pressed for further work The manual key button is used to start the START STOP and the FILL function and to output t...

Страница 13: ...ction of the cylinder contents Filling time F2 Setting the filling time System F3 Selection of the national language and setting of the serial parameters Menu Mode Selection of the functions Dosing ti...

Страница 14: ...al Piston Burette the display will show the respective basic menu of a function Here you use the FILL or the grey key of the manual key button to start the Filling function Upon completion of the manu...

Страница 15: ...you can reset the input to the last valid parameters by pressing the F4 key Fig 16 Fig 17 Dosing parameter Nominal vol 015 00ml Change digit Next digit OK F1 ESC F4 Dosing parameter Speed 40 00ml min...

Страница 16: ...wn including 2 nd stage high speed and keep it depressed The titration solution will be dosed as long as the key is kept depressed The display will show the volume and the selected rate stage with the...

Страница 17: ...ith the display of the TITRONIC universal Piston Burette Setting the parameters chapter The stored parameters remain active even after the burette is switched off 4 9 Incremental dosing Use the MODE k...

Страница 18: ...g with each other require the same transfer parameters The following transfer parameters are set ex factory Baud rate 4800 baud Data bits 7 Bit Stop bits 1 Parity No If you wish to change the data tra...

Страница 19: ...ton Burette This piston burette in turn will now check the address and will respond to this command just like the first burette Any information data strings arriving at the interface 2 of the TITRONIC...

Страница 20: ...ce Z 1 Titration Z 2 Dosing Z 3 Incremental dosing aaMO1 Set titration function aaY aaMO2 Set dosing function aaY aaMO3 Set incremental dosing function aaY aaRA Interchangeable unit inquiry of volume...

Страница 21: ...2 or Fig 9 item 2 Important note The disassembly of the dosing unit as such is only possible using a special tool TZ 3630 and should only be done by experienced persons The sealing lip of the PTFE pis...

Страница 22: ...the cylinder and in the hoses The disturbances to be anticipated are the greater the more the new solu tion differs from the previous type and concentration In the case of highly different solutions t...

Страница 23: ...rips after use Air bubbles in the system Set longer filling time When installing the dosing unit the piston rod is not pulled in correctly the device rattles Oblique application of piston rod Re apply...

Страница 24: ...30 If moisture is actually present one can conclude that the piston in the cylinder is no longer tight Check the hoses screwed connections and seals for visible damage contamination and leakage assem...

Страница 25: ...r repair please state the titration solution last used on the accompanying papers or on the TITRONIC universal Piston Burette itself Otherwise the service department will dispose of the damaged or rep...

Страница 26: ...uter PC with 25 channel plug 1 side 4 channel mini DIN plug 2 side 25 channel sub Miniature D plug TZ 3097 1 5 m data cable RS 232 C for computer PC with 9 channel plug 1 side 4 channel mini DIN plug...

Страница 27: ...48 Order numbers Fig 31 M3 X 10 mm TZ 3660 TZ 1503 TZ 3460 TZ 3025 TZ 2008 TZ 2005 TZ 3095 TITRONIC universal TZ 3665 TZ 3680...

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