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Accessories and consumables

Accessories

C 6010

Decomposition vessel

C 6012

Decomposition vessel

C 5010.5

Crucible holder, large

C 5010.8

Crucible holder, small

C 21

Pelleting press

C 29

Pressure reducer, oxygen

C 6030

Gas washing station

C 27

Calorimeter instrument set

C 5041.10

Connecting cable 9-pin / 3m

C 6040

Calwin

C 1.50

Dot-matrix printer

C 60.1020

Organizer

Consumables

C 723

Benzoic acid blister pack, 50 pieces

C 723

Benzoic acid big pack

C 43

Benzoic acid NIST 39i

C 710.4

Cotton wool threads cut to length

C 710.8

Cotton wool threads cut to length, thick

C 16

Parafilm 1000 x 50

C 17

Paraffin liquid 30 ml

C 15

Paraffin strips 600 pieces/package

C 9

Gelatine capsules (100 pieces)

C 10

Acetobutyrate capsules (100 pieces)

C 12 A

Combustion bag, 70 x 40 mm (100 pieces)

C 12

Combustion bag, 40 x 35 mm (100 pieces)

AOD 1.11

Control standard for sulphur and chlorine

AOD 1.12

Control standard for fluorine and bromine

C 1.103

Ignition wire

C 1.123

Ignition wire, platinum

C 14

Combustible crucible (100 pieces)

C 5 VA

VA combustion crucible set (25 pieces)

C 710.2 VA

VA Combustion crucible large (25 pieces)

C 4

Quartz dish

C 6

Quartz dish large

C 6000.10

Spare parts kit 1000

C 6000.12

Spare parts kit 1000

For further accessories see

www.ika.com

Technical data

Measuring range max

40000

Measuring mode dynamic 22 °C

yes

Measuring mode isoperibolic 22 °C

yes

Measuring mode dynamic 30 °C

yes

Measuring mode isoperibolic 30 °C

yes

Measuring time* dynamic approx.

min

Measuring time* isoperibolic approx

min

Reproducibility dynamic (1g benzoic acid NBS39i)

% RSD

0.15

Reproducibility isoperibolic (1g benzoic acid NBS39i)

% RSD

0.05

Touchscreen

yes

Working temperature min.

°C

Working temperature max.

°C

Temperature measurement resolution

0.0001

Cooling medium temperature min.

°C

Cooling medium temperature max.

°C

Cooling medium permissible operating pressure

bar

1.5

In accordance with

IKA

warranty conditions, the warranty period

is 12 months. For claims under the warranty please contact your

local dealer. You may also send the machine direct to our factory,

enclosing the delivery invoice and giving reasons for the claim. You

will be liable for freight costs.

The warranty does not cover worn out parts, nor does it apply to

faults resulting from improper use, insufficient care or maintenan-

cenot carried out in accordance with the instructions in this operat-

ing manual.

Warranty

Содержание C 3000 isoperibol

Страница 1: ...IKA C 3000 isoperibol 20000011772 Operating instructions EN C 3000_092016...

Страница 2: ...Device setup Touch Screen Lift Stylus for operating the touch screen Decomposition vessel Water filter Water Oxygen Interfaces Mains power supply 2...

Страница 3: ...and operating elements 11 Explanation of the screen display 11 Schematic representation of the display components 11 Weighted sample 13 Work with the device 14 Switching on the device 14 System test...

Страница 4: ...m 31 Help 31 Maintenance 31 Hardware details 32 Info 32 Cleaning 33 Cleaning the system 33 Servicing and cleaning the filter 33 Troubleshooting 34 Fault rectification 35 Checks 36 Warranty 37 Accessor...

Страница 5: ...sive bacteriologically contaminated toxic Please observe the relevant regulations when handling oxygen DANGER Warning oxygen as a compressed gas is oxidising intensively aids combustion can react viol...

Страница 6: ...ces The accessories of the system ensure customized adapta tion to laboratory tasks The system is characterized by the following features Relieves you of routine tasks through automated measurement pr...

Страница 7: ...e Transport and storage Transport and storage conditions The system must be protected against mechanical impact vibra tions dust deposits and corrosive ambient air during transporta tion and storage I...

Страница 8: ...n the chapter Safety instructions Please read these operating instructions carefully IKA consider themselves responsible for the safety reliability and performance of the appliance only when the devic...

Страница 9: ...truction IKA C 25 Connecting the oxygen supply IKA C 29 Connection to the mains power supply O2 connection tube IN max 4 MPa Insert the O2 connection tube into the calorimeter IN port until it clicks...

Страница 10: ...r USB DEVICE USB interface only for service USB HOST Interface for connection of a printer or with a USB mouse On off switch NOTICE Switch the device off at the on off switch only when directed to do...

Страница 11: ...r view based presentations of display components are described in the relevant section The contents of the screen display are often distributed over sev eral tabs You can switch between tabs at any ti...

Страница 12: ...oint in time are gath ered together as clickable buttons along the bottom edge of the screen To initiate an action it is sufficient to click on one of the discrete areas showing the relevant images or...

Страница 13: ...h as Designation Here again the entire area is available to be clicked A complete vir tual keyboard is opened Note The maximum input is 23 characters Selection box Weighted sample After the virtual ke...

Страница 14: ...pump and heater approx 30 to 45 seconds Testing the internal water circuit with the condenser and water supply plus the heater once again approx 30 to 45 seconds Testing whether the temperature of the...

Страница 15: ...e formed for example ash Often however the combustion products that form the basis of the standards are not the only products that are formed In such cases an analysis of the fuel sample and the produ...

Страница 16: ...ble absorption solution is placed in the decomposition vessel before the trial according to the rel evant standards With this absorption fluid and the combustion water the combustion gases form acids...

Страница 17: ...ecomposition vessel must then not be swapped with parts from other vessels In addition the thermal capacity depends to a small extent on the measurement procedure used The thermal capacity determined...

Страница 18: ...thread to the centre of the ignition wire using a loop 2 Weigh out the substance directly into the crucible with an accuracy of 0 1 mg If necessary put some distilled water or a solution into the dec...

Страница 19: ...e maximum permissible engery input You can also select specific types of combustion aids from the list In such cases you must enter the weight of this combustion aid so that the external energy can be...

Страница 20: ...ition vessel in the calorimeter and press Start The cover will close automatically If you accidentally press the Start button before you have hung a decomposition vessel in the calorimeter you will re...

Страница 21: ...ed calorific value and the calculated thermal capacity also appear here You can cancel the measurement at any time by clicking on Can cel After a measurement the screen switches automatically to the M...

Страница 22: ...these parameters and the relevant calculation formulae for the complete results can be found in the respective standard The screens are adapted to suit the standard that was selected When you have com...

Страница 23: ...f measurements currently displayed is prin ted not in combination with serial printer C 1 50 Delete selected measurement This deletes the selected measurement from the displayed list and also from the...

Страница 24: ...aluation button for the measurement to evaluate it for the first time or to reevalu ate it chapter Evaluation Alternatively you can use the actions provided by the menu as described above Once you hav...

Страница 25: ...calculation of the C mean value or to exclude it if it had previously been selected Then switch to the Statistics tab Statistics tab Average value standard deviation and maximum deviation relate to t...

Страница 26: ...dditional check calibrations You can use the check and warning lines to decide whether the C value has shifted and therefore a reselection and recalculation is necessary To exit this menu you must use...

Страница 27: ...ill be used for any subsequent re evaluation Otherwise the cur rent setting for the evaluation procedure will be used Measurements evaluated previously are not affected by this change Display unit Thi...

Страница 28: ...mperature at the inlet must not fall below 12 C FUT screen visible If selected the FUT screen will be shown at startup Select the menu option to connect the C 3000 to the water supply line Do not exce...

Страница 29: ...ary you can change the values for Baud rate parity data bits and stop bits Click on OK to use all the changed settings for the subsequent calorimetric procedures Click on Cancel to leave all the setti...

Страница 30: ...SB printers which the use the PCL printer language to the C 3000 We recommend the HP Business Inkjet 1200 or its successor models Network printer When you have selected a network printer you must then...

Страница 31: ...ight hand field with the arrow symbol Here you can obtain detailed information on the topic Click on the left hand field with the arrow symbol to revert to the overview of topics and if necessary sele...

Страница 32: ...urement channels various counters and statuses of accessories You cannot make any changes here The information displayed can be forwarded to Service Engineers who have access to various settings Info...

Страница 33: ...also be wiped away with an absorbent non fibrous cloth Repairs Please only send devices in for repair that have been clea ned and are free of materials which might present health hazards For this use...

Страница 34: ...ctly the Confirm button is clicked After you have taken the actions de scribed in the Help or in the operating instructions click on the Restart button to start the system test On successful completio...

Страница 35: ...e weighted sample of the sample may be insufficient The calorific value of the sample is too small use a combustion aid The oxygen pressure is insufficient The stirrer is not working The sample has no...

Страница 36: ...k using the calorimeter can be performed only once the sys tem test has been completed suc cessfully Acknowledge the error message in order to switch to the System Check status Press the Restart butto...

Страница 37: ...arge 25 pieces C 4 Quartz dish C 6 Quartz dish large C 6000 10 Spare parts kit 1000 C 6000 12 Spare parts kit 1000 For further accessories see www ika com Technical data Measuring range max J 40000 Me...

Страница 38: ...8 yes Evaluation to ASTM D5865 yes Evaluation to ISO 1928 yes Evaluation to GB T213 yes Width mm 500 Depth mm 450 Height mm 450 Weight kg 29 Permissible ambient temperature min C 20 Permissible ambien...

Страница 39: ......

Страница 40: ...IKA Werke GmbH Co KG Janke Kunkel Str 10 D 79219 Staufen Tel 49 7633 831 0 Fax 49 7633 831 98 sales ika de www ika com 20012285a...

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