Appendix C: Performing Routine Procedures with SynerJY
69
7.
Run
the experiment for several seconds then click
Stop
.
8.
Zoom
in on the central peak.
9.
View the spectra. A focused, aligned CCD will provide a distinct peak of large
amplitude, generally symmetrical to the limits of the design of the spectrometer.
The peak should be less than or equal to 5 pixels wide across the Full Width of
Half the Maximum height (FWHM). Excessive asymmetry of the peak is a sign
that the slit image is not aligned to the pixel columns; diminished shape and
magnitude are symptomatic of defocusing.
10.
Stop
the acquisition.
11.
While in
Data Preview
, select
Detectors
and set
five
equal areas in the
Free
Form Area
list.
12.
Click the
Reformat
button to display the areas then click Apply to apply the area
change as a parameter.
13.
Select
Continuous
and
Run
the experiment. When aligned the five spectra will
overlap but may not show similar intensity. Each spectrum should be 3-5 pixels
wide at FWHM. To adjust the focus of the CCD camera, rotate the focus wheel
with your fingers to drive the CCD flange out from the body. To bring the camera
focus in, it is necessary to hold the camera against the wheel while rotating the
focus wheel.
14.
To adjust the alignment (rotation) of the CCD camera, insert a 1.5 mm allen key
into the hole in the side of the unit to engage the CCD rotation adjustment set
Содержание JOBIN YVON SYNAPSE
Страница 1: ...SYNAPSE CCD Detection System User Manual Part Number 81100 Revision 2...
Страница 10: ...Preface x...
Страница 14: ...System Description and Specifications 4...
Страница 28: ...Detector System Installation 18...
Страница 38: ...Initial Power up and Operation 28...
Страница 48: ...Temperature Control 38...
Страница 71: ...61 Appendix A Dimensional Drawings Figure 1 Figure 16 Synapse Detector Head Note Dimensions are in inches mm...
Страница 72: ...Appendix A Dimensional Drawings 62 Figure 17 Distance from Focal Plane to CCD Chip...
Страница 73: ...Appendix A Dimensional Drawings 63 Figure 18 Synapse Power Supply Unit...
Страница 74: ...Appendix A Dimensional Drawings 64...
Страница 86: ...Appendix C Performing Routine Procedures with SynerJY 76...
Страница 100: ...Appendix E Accessories 90...
Страница 104: ...Warranty 94...
Страница 113: ...103 Notes...
Страница 114: ...104 Notes...