Eicom ENO-30, Руководство пользователя

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6-8. Start up ----------------------------------------------------------------------------------- 28
7. SAMPLE INJECTION ------------------------------------------------------------------------------------------------------------------- 29
7-1. Manual Injector Operation ----------------------------------------------------------- 29
7-2. Sample Amount ------------------------------------------------------------------------ 30
7-3. Autosampler Operation (optional) ------------------------------------------------- 30
8. SHUTDOWN AFTER ANALYSIS ----------------------------------------------------------------------------------------------------- 31
8-1. Short Shutdown, less than 2 weeks ---------------------------------------------- 31
8-2. Complete Shutdown, over 2 weeks ----------------------------------------------- 31
9. RESTART ---------------------------------------------------------------------------------------------------------------------------------- 32
9-1 After complete shutdown procedure ----------------------------------------------- 32
9-2. After short shutdown procedure ---------------------------------------------------- 32
10. PRECOLUMN --------------------------------------------------------------------------------------------------------------------------- 34
10-1. Determining the Precolumn Condition ------------------------------------------ 34
10-2. How to Repack the Precolumn --------------------------------------------------- 35
10-3. Filter Exchange ----------------------------------------------------------------------- 37
11. SEPARATION COLUMN (NO-PAK) ----------------------------------------------------------------------------------------------- 38
11-1. NO-PAK --------------------------------------------------------------------------------- 38
11-2. Identification of Separation Quality ---------------------------------------------- 38
11-3. Washing the Separation Column ------------------------------------------------- 38
12. REDUCTION COLUMN (NO-RED) ------------------------------------------------------------------------------------------------ 39
12-1. Structure and Maintenance -------------------------------------------------------- 39
12-2. Timing to Exchange ----------------------------------------------------------------- 39
12-3. Damage -------------------------------------------------------------------------------- 39
13. TROUBLESHOOTING ---------------------------------------------------------------------------------------------------------------- 40
13-1. Pump Problems ---------------------------------------------------------------------- 40
13-2. Checking the Flow Rate ------------------------------------------------------------ 40
13-4. Removing Air Bubbles -------------------------------------------------------------- 40
13-4. High Carrier Pump pressure ------------------------------------------------------ 41
13-5. Unstable Baseline -------------------------------------------------------------------- 41
13-6. Peak Shape --------------------------------------------------------------------------- 41
14. MAINTENANCE ------------------------------------------------------------------------------------------------------------------------- 42
14-1. Pump Head Parts -------------------------------------------------------------------- 42
14-2. Changing the Piston Seal and Piston ------------------------------------------- 43
15. APPENDICES --------------------------------------------------------------------------------------------------------------------------- 47
15-1. Autosampler and Data Processor (EPC-700) Connection ---------------- 47
15-2. Specifications ------------------------------------------------------------------------- 48
15-3. Sample Preparation ----------------------------------------------------------------- 49