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M88-E01072

7 - 1

7. Calibration

Prior to calibration, the system must be aligned
using the scintillation detector.

Each detector and the associated electronics
are unique. A calibration process is used in con-
junction with standard reference materials to
determine a zero offset for the resolution in
degrees. This value represents the angular dif-
ference between the zero angle of 2-theta and
the zero channel of the PSD. The calibration
program will refine the values and record them
in the Configuration program.

7.1

Positional Calibration

1.

Manually open all window slits as wide as
possible.

2.

Ensure that the proper K

β

filter is in place.

3.

Make sure that no Debye slit is in place.

4.

Ensure that the reference material is
mounted (quartz or NIST 1976) in the sam-
ple stage.

5.

Set the goniometer to the parameters in
Table 7.1 or Table 7.2 using DIFFRAC

plus

COMMANDER.

NOTE: Do not close DIFFRAC

plus

COM-

MANDER. Instead, minimize the window.

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Содержание VANTEC-1

Страница 1: ...V NTEC 1 Detector USER MANUAL M88 E01072 5 05 BRUKER ADVANCED X RAY SOLUTIONS...

Страница 2: ......

Страница 3: ...V NTEC 1 Detector User Manual BRUKER ADVANCED X RAY SOLUTIONS M88 E01072 5 05...

Страница 4: ...ation and products protected by copyrights or patents and does not convey any license under the patent rights of Bruker AXS Inc nor the rights of others Bruker AXS Inc does not assume any liabilities...

Страница 5: ...1 3 System Description 3 1 3 1 The Detector 3 2 3 1 1 Detector Cables and Connectors 3 2 3 1 2 Environmental Ratings 3 5 3 2 The Detector Controller 3 5 3 2 1 Identifying Integrated and External FDC...

Страница 6: ...4 7 Installation of the detector controller using second generation indexer boards AIB2G 4 12 4 7 1 Requirements 4 12 4 7 2 Connection and Cable Wiring 4 13 4 7 3 Hardware Installation 4 14 4 7 4 Sof...

Страница 7: ...tector controllers with external FDC 6 9 6 5 2 For detector controllers with integrated FDC 6 9 6 5 3 Set Up Communication Parameters both FDC types 6 10 6 6 Factory Default Settings 6 11 7 Calibratio...

Страница 8: ...Openings 9 8 10 Preventive Maintenance and Troubleshooting 10 1 10 1 Cleaning the Diffraction System and Measuring Equipment 10 2 10 2 Replacing Fuses 10 3 10 3 Troubleshooting 10 4 10 4 Manual Config...

Страница 9: ...of danger The word Warning indicates that death severe personal injury or substantial property damage can result if proper precautions are not taken The word Caution indicates that minor personal inju...

Страница 10: ...erated and maintained as recommended by Bruker AXS Protection provided by this equipment may be impaired if it is used in a manner not specified by Bruker AXS 1 3 X ray Equipment X ray equipment produ...

Страница 11: ...upplied by several power supply lines The system and its components will be live until all power lines connected to the system are disconnected from the mains power supply The following warning symbol...

Страница 12: ...and national regulations 1 5 Proper Lifting Installation of the detector requires lifting of components that weigh up to 43 lbs 19 5 kg Whenever possible two or more people should lift objects togethe...

Страница 13: ...u investigations like recording an X ray movie of kinetic processes The active area of the detector is 50 mm by 16 mm along the scattering plane respectively per pendicular The simultaneously recorded...

Страница 14: ...ray emission lines from Cr through Mo the default is Cu The factory settings are optimized for Cu K The electronic energy window allows the opera tor to set a discriminator window optimized for the X...

Страница 15: ...controller FDC and the optics This section also contains information on the counterbalance and both integrated and external FDCs as these compo nents may vary depending on your configura tion The new...

Страница 16: ...1 1 Detector Cables and Connectors The back cover has six cable connectors One connector for the preamplifiers low voltage power supply Two cables for the detector s high voltage supply Three signal o...

Страница 17: ...Usable wavelength range From Cr K up to Mo K factory set default for Cu K Gas fill 3 04 bar 3040 hPa 3 ATM non polymerizing Xe CO2 gas no external gas supply required Radiation hardness 1012 counts m...

Страница 18: ...x 19 in W x 16 25 in D 10 lbs 90 mm H x 480 mm W x 410 mm D 4 5 kg Length of cables between the detector and the controller chassis unit 16 4 ft 5 m Disconnect device IEC 320 connector plug on power...

Страница 19: ...ower supply for the detector preamplifiers the Constant Fraction Discriminator CFD boards the Time to Digital Converter TDC boards and all electronic assemblies All of these units are placed within th...

Страница 20: ...st slot on the right hand side of the detector controller s rear panel contains both a DB9 male connector and a DB25 male connector Figure 3 2 Figure 3 2 External FDC identification Integrated FDC The...

Страница 21: ...k Adapter CFD LV Power Supply 24V LV Power Supply 7 5V PCI Back Plane TDC SBC FDC LV Power Supply LV Power Supply 7 5V LV Power Supply 12V Remote Control HV Filter 2 HV Filter 1 HV Power Supply 1 HV P...

Страница 22: ...er Manual 3 8 M88 E01072 Figure 3 5 Detector controller outside front Illuminated high voltage enable push button switch Fan filters LED Indicators Alarm Red System activity Green blinking HV OK Yello...

Страница 23: ...Manual System Description M88 E01072 3 9 Figure 3 6 Detector controller outside back Grid HV Power receptacle Low voltage connector Ch 1 Ch 5 Data I O COMM 2 COMM 1 LAN Anode HV Ch 2 CFD Out Motor cl...

Страница 24: ...mputer s diffractometer control data connection chain Features LCD display 132 x 39 mm Two serial interfaces Integrated multi channel analyzer 19 unit Online display of the measured 2 theta dia gram o...

Страница 25: ...front display of the FDC will graphically show a selected subset of the measuring channels and three values Figure 3 8 FDC display for fast diffraction locked coupled mode Y scale in counts 2 theta v...

Страница 26: ...2 5 4 0 optional and window opening scales The K filter and Debye slits have notches which fix the slit in position when properly inserted The anti scatter slit assembly length used depends on the me...

Страница 27: ...mpo nents see Appendix B for part numbers 1 Detector window slits 2 Debye slits optional 3 K filter 4 Anti scatter slits near sample window slits 5 Soller slits 6 Window opening scales Figure 3 10 Det...

Страница 28: ...ident angles The beam stop has three directions of move ment 1 Selects an adapter for the beam height default height is 150 mm 2 Adjusts beam stop for 401 435 and 500 mm circles 3 Adjusts beam stop up...

Страница 29: ...n is to reduce primary air scatter which influences the background of the diffraction pattern usually at lower angles The air scatter screen can be attached to the primary optics The air scatter scree...

Страница 30: ...sity standard like NIST SRM1976 Corundum plate or NIST SRM640c Silicon pow der filled in capillaries NOTE The radial Soller slit cannot be used with Bragg Brentano focusing geometry due to differ ence...

Страница 31: ...V NTEC 1 Detector User Manual System Description M88 E01072 3 17 Figure 3 15 Transmission ray tracing 2 Tangent Axis Radial Axis...

Страница 32: ...alance is based on the weight of the detector and optics the measuring circle diameter and the height of the sample stage In order to ensure proper weight distribu tion please use the tables below to...

Страница 33: ...V NTEC 1 Detector User Manual System Description M88 E01072 3 19 Figure 3 17 Counterbalance positions...

Страница 34: ...System Description V NTEC 1 Detector User Manual 3 20 M88 E01072...

Страница 35: ...erminals components and multiple power supply lines may be live It is not sufficient to just press the D8 enclosure s Power OFF button O or the on off power switch on the V NTEC 1 controller The mains...

Страница 36: ...when practical for return shipping 4 3 Baseline Data Before making any installation or calibrations to the diffractometer run and save a standard Bragg Brentano scintillation scan using the set tings...

Страница 37: ...detector controllers with internal FDC see Section 3 2 1 for identifi cation See Section 4 6 for detector installation with A1B2G index board D8 controllers installed after March 2005 Use the followi...

Страница 38: ...ed to accommodate the FDC controller 2 Relocate the existing rails A in Figure 4 1 for adequate airflow 3 Mount the rails so there is a minimum space of 1 between the detector and FDC control lers 4 M...

Страница 39: ...henever possible place the V NTEC 1 controller above the D8 controller electronics see Figure 4 2 for proper location in the D8 Allow at least 1 of open area around the top bottom and back of the unit...

Страница 40: ...from SCOM 2 of the FDC controller to COM 1 on top of the D8 controller All connectors have a positive lock to ensure proper connection 2 Connect the BNC type connector from CH 1 of the V NTEC 1 contr...

Страница 41: ...rates the major detector system components and the cabling for communication Figure 4 3 Configuration setup D8 Controller COM 1 COM 2 Control PC LAN 1 LAN 2 User s LAN OPTIONAL VANTEC 1 Controller COM...

Страница 42: ...olutely necessary to switch off the external mains supply before opening the housings It is not sufficient to just press the on off power switch on the V NTEC 1 controller The mains supply must be swi...

Страница 43: ...le A17 D42 must be connected between the 9 pin STEP DIR port on the rear of the detector controller see Figure 4 5 and either For D8 systems the X5 9 pin port on the B104 2 axis indexer board or For D...

Страница 44: ...al 4 10 M88 E01072 Figure 4 6 Wiring of V NTEC 1 detector controller with integrated FDC User s LAN OPTIONAL COM 1 COM 2 LAN LAN 1 LAN 2 COM 1 COM 2 V NTEC 1 Co ntroller Control PC D8 D4 Controller cr...

Страница 45: ...ufacturer for details Removal of retaining screws may be required Some models have plastic snaps at the cor ners or edges of the case Release the cover with a squeeze or pull 4 Select an open expansio...

Страница 46: ...r computer and allow it to boot up normally 8 To complete the installation go to Section 6 4 7 Installation of the detector con troller using second generation indexer boards AIB2G The cabling and con...

Страница 47: ...e X5 9 pin socket on the B231 2 axis indexer board or For D4 systems the socket on the bracket X11 of the B232 4 axis indexer board NOTE The clock signal cable can be one of two cables one straight an...

Страница 48: ...Controller Rack NOTE Never mix old and new Axis Indexer Boards The boards may be rendered inoperable as a result When using the B104 or B105 Axis Indexer Boards connect the motor clock cable and inde...

Страница 49: ...the motor and encoder cables as shown in Table 4 1 Table 4 1 Motor and encoder cable connection for a D8 system Switch on the D8 D4 system Source Theta Theta Theta 2Theta Cable Connection on B231 Th T...

Страница 50: ...systems without 21 CFR Part 11 software the system can be set to configure itself auto matically with regard to the source for the Clock Signal 1 Open the Configuration software and select the V ntec...

Страница 51: ...ed installation for the Clock Signal is recommended see Section 4 7 5 1 Make sure that the Automatic Drive Config uration is disabled by unchecking the check box in Figure 4 12 2 Select Advanced Board...

Страница 52: ...sending the clock signals this motor axis has to be chosen From Figure 4 13 the Axis must be Driver 1 Set Register to Signal Status Register and Bit to bit 11 Motor Clock Bit 3 Figure 4 15 Motorized D...

Страница 53: ...ct Advanced Board Setup Two Axis Indexer Boards Ensure that physical drive 1 is connected to logical axis THETA and physical drive 2 is connected to logical axis 2THETA see Figure 4 17 Figure 4 17 Adv...

Страница 54: ...e settings for 2Theta The param eters for Sources for AxisOUT have to look like Figure 4 19 NOTE Do not worry about the fact that the set tings for 2Theta show no settings for Register and Bit Figure...

Страница 55: ...es of freedom 2 DOF If this is not the case follow the steps indicated below Move the detector to different measuring circles to suit the installation 1 Move the 2 theta drive to a position where the...

Страница 56: ...n for the D8 ADVANCE V NTEC 1 Detector User Manual 4 22 M88 E01072 3 Use Figure 4 22 to set the predefined mea suring circle on the theta and 2 theta tracks Figure 4 22 Predefined measuring circle dia...

Страница 57: ...If not already attached attach the detector to the 2 DOF mount with the detector mounting screws shown in Fig ure 4 21 and Figure 4 24 4 2 Place the detector on the track Slide it down to the pinned p...

Страница 58: ...beam stop assembly to the goni ometer see Figure 4 26 3 1 Use the mounting pin to position the beam stop assembly 3 2 Insert and tighten the mounting screw 4 Mount the beam stop in one of the followi...

Страница 59: ...paper 4 1 Lower the room lights or cabinet lamps to make the beam visible 4 2 If necessary raise the kV mA to make the beam clearer 5 Lower the knife edge until the flux is clearly distinguished on th...

Страница 60: ...t the final settings with an intensity standard like the NIST SRM1976 Corundum plate Use a procedure similar to that in the Instrument Verifi cation Booklet M88 Zxx041 for final documenta tion of the...

Страница 61: ...V NTEC 1 Detector User Manual Hardware Installation for the D8 ADVANCE M88 E01072 4 27 Figure 4 28 Air scatter screen exploded view Tilt 2 3 4 5 6 1 Translation...

Страница 62: ...standard reference material SRM like the NIST 1976 corundum plate See the Instrument Verification Booklet M88 Zxx041 for additional system parame ters 2 For the tilt and translation adjustments use a...

Страница 63: ...V NTEC 1 Detector User Manual Hardware Installation for the D8 ADVANCE M88 E01072 4 29 Figure 4 29 Alignment of the paddle using the fluorescent screen Tilt adjustment Paddle 2 mm gap...

Страница 64: ...er Manual 4 30 M88 E01072 Figure 4 30 Translation adjustment Do not use smaller primary angles tube angle or sample than 0 theta in order to avoid a collision between the air scatter screen and sample...

Страница 65: ...et Allen key set Mount the radial Soller slit 1 Take off the k filter 2 Attach the radial Soller slit onto the V N TEC 1 optics block using the two anti scat ter slit screw holes shown in Figure 3 9 3...

Страница 66: ...Table 8 1 with SRM1976 or powder in capillaries to define the intensity distribution also see the Instrument Verifi cation Booklet M88 Zxx041 2 Install the radial Soller slit see Figure 4 31 3 Run a...

Страница 67: ...ts The detector mount and the cabling through the enclosure are also different 5 1 Servicing Precautions When the equipment is connected to the mains supply some terminals components and multiple powe...

Страница 68: ...e the packaging for return shipping 5 3 Baseline Data Before doing any installations or calibrations on the diffractometer run and save a standard Bragg Brentano scintillation scan using the set tings...

Страница 69: ...ximity to the generator This may induce electronic noise in the detector electronics Use care when moving the detector head to avoid mechanical shock to the assembly See Table A 3 in Appendix A for th...

Страница 70: ...6 Mount the controllers into the rack and con nect the components as shown in Figure 4 3 The cabling of the V NTEC 1 inside the radia tion safety box is shown in Figure 5 2 through Figure 5 4 Figure...

Страница 71: ...he detector to the detector mount with two M3 countersunk screws and two M5 Allen screws see Figure 5 5 8 Mount the high voltage cables to the strain relief see Figure 5 6 Attach the other cables to t...

Страница 72: ...ine and all side and back panels 2 Mount the special handles for the front panel Turn the safety key to position 1 Open the front panel 3 Remove the scintillation counter propor tional counter Ca chan...

Страница 73: ...e groove ring NOTE Do not lose the T nut in the groove put a tissue into the groove to prevent this Figure 5 8 Mount the primary beam stop 8 Screw the alignment screw completely out see Figure 5 9 Put...

Страница 74: ...uator in the extreme high position of the alignment screw Figure 5 10 Mounting of the actuator bracket for beam stop collision switch 10 Mount the collision switch to the detector mount Place the colo...

Страница 75: ...collision switch to the detector mount 13 Test the collision switch by holding up the beam stop while moving down the detector 2 theta The instrument must stop moving and display the error theta and 2...

Страница 76: ...Hardware Installation for the D4 ENDEAVOR V NTEC 1 Detector User Manual 5 10 M88 E01072...

Страница 77: ...n program is used to set the parameters Perform the follow ing steps to configure the system see Figure 4 3 for the cabling scheme for an internal FDC Figure 4 6 for the cabling scheme for an inte gra...

Страница 78: ...into a free PCI slot in the PC 1 1 To install the network card see Section 4 6 2 Restart the computer 3 Windows should recognize the new hard ware If it asks for a diskette that contains the network a...

Страница 79: ...l appear see Fig ure 6 2 Figure 6 2 Internet Protocol TCP IP Properties 4 5 Select the Use the following IP address radio button and enter 192 168 23 1 for the IP address and 255 255 255 0 for the Sub...

Страница 80: ...n 1 Open the Configuration program Con fig exe located in the C Diffplus directory 1 1 From the main Config menu select the Detectors menu see Figure 6 3 1 2 Check the Position Sensitive Detec tor che...

Страница 81: ...Software Configuration From Config 1 The FDC type has to be set to internal In fact the settings of the Fast Diffraction Controller at the subfolder Computer Ports will be inaccessible see Figure 6 9...

Страница 82: ...Geometry Angle to 12 3 3 Set FDC type to Internal for detector controllers with an internal FDC See Section 3 2 1 for identification 3 4 Select FDC type to Socabim for detec tor controllers with an ex...

Страница 83: ...n program must be completed prior to saving and downloading the configura tion file 1 Go to Advanced Board Setup PSD Con troller 1 1 In Communication Topology select Network and press the button Defau...

Страница 84: ...7 2 1 In IP Setup select the Static Address Assignment radio button 2 2 Enter the Host IP Address 192 168 23 2 and the Netmask 255 255 255 0 Do not change any other values 2 3 Under Services check the...

Страница 85: ...onfiguration 6 5 1 For detector controllers with external FDC 1 In Config go to Computer Ports see Figure 6 8 Figure 6 8 Computer port configuration 6 5 2 For detector controllers with inte grated FDC...

Страница 86: ...1 3 Click OK and close the window Figure 6 10 Diffractometer Settings pop up window 2 In Computer Ports select Settings under PSD Controller 2 1 In the pop up window under TCP IP enter the IP address...

Страница 87: ...ur V NTEC 1 has an inte grated FDC refer to Figure 4 6 7 Click OK to download 6 6 Factory Default Settings 1 Import the default detector settings see Fig ure 6 13 1 1 In the Configuration menu select...

Страница 88: ...r User Manual 6 12 M88 E01072 2 Select V NTEC 1 Setup see Figure 6 14 2 1 Set the Geometry Angle to 12 2 2 The starting values for Resolution and Zero Offset should be 0 008 and 6 5 respectively 2 3 C...

Страница 89: ...ro angle of 2 theta and the zero channel of the PSD The calibration program will refine the values and record them in the Configuration program 7 1 Positional Calibration 1 Manually open all window sl...

Страница 90: ...llation step sec Cr 20 03 20 03 20 03 40 06 0 3 0 6 V 35 45 006 30 002 Co 15 52 15 52 15 52 31 04 0 3 0 6 Fe 35 45 006 30 002 Cu 13 32 13 32 13 32 26 64 0 3 0 6 Ni 40 40 006 30 002 Goniometer Divergen...

Страница 91: ...he new menu files Click OK see Figure 7 1 Figure 7 1 Wizard File New 4 To create the DQL file input the calibration parameters and click OK The number of positions must be nine or greater When ever po...

Страница 92: ...Calibration V NTEC 1 Detector User Manual 7 4 M88 E01072 Figure 7 2 Create the DQL file Example shown is for Corundum sample and Cu radiation...

Страница 93: ...5 7 2 2 Collect Data 1 Open DIFFRACplus COMMANDER 2 Select the Jobs tab and create a job using the Calib DQL file 3 Name the RAW file Calib raw 4 Press Start Job and wait for the job to fin ish NOTE I...

Страница 94: ...Detector User Manual 7 6 M88 E01072 7 2 3 Analyze Data 1 After creating Calib raw select Analyze Calibration in the Configuration program under the V NTEC 1 Setup menu see Fig ure 7 3 Figure 7 3 Anal...

Страница 95: ...is greater than 0 05 Continue on to the next step when you have reached a standard deviation of less than 0 05 i e zero offset is approximately 5 to 8 and standard devi ation is less than 0 05 6 After...

Страница 96: ...Calibration V NTEC 1 Detector User Manual 7 8 M88 E01072...

Страница 97: ...2 DOF mount by running repeated PSD fixed scans of NIST SRM 1976 or Quartz For a quick assess ment of the alignment compare the intensities of the main 104 peak to the valley between K 1 and K 2 see...

Страница 98: ...he ratio of the intensity of the main peak to the valley between the K 1 and K 2 peaks see Figure 8 1 NOTE The increment is dependent on PSD Calib and the measuring diameter Figure 8 1 Measure the int...

Страница 99: ...he baseline scan If the ratio increases continue to adjust in the direction first attempted If the ratio decreases reverse the direction of movement and repeat step 3 until the maximum ratio is achiev...

Страница 100: ...other measuring circle If specifications are not met repeat Section 8 1 Table 8 2 FWHM specifications for Cu radiation 1 Start EVA and load the RAW data to evalu ate 2 Open the EVA toolbox press F2 or...

Страница 101: ...Alignment is complete when FWHM matches the specifications in Table 8 2 Figure 8 4 EVA toolbox 5 After completing the alignment of the mount repeat the calibration described in Section 7 NOTE The prim...

Страница 102: ...Alignment V NTEC 1 Detector User Manual 8 6 M88 E01072...

Страница 103: ...TEC 1 controller requires one hour to warm up for optimal results 9 1 V NTEC 1 Power Up Procedure 1 Press the I O button on the front of the V N TEC 1 controller to apply mains power The I O button il...

Страница 104: ...to stop power to the control electronics high volt age generator and the V NTEC 1 control ler and FDC if present when the controllers are connected to X602 4 Before switching off the diffraction syst...

Страница 105: ...rgency situations and not for normal shutdown of the diffractome ter system The Stop button will not turn off the three AC outlets X601 that are located on the mains distribution panel Devices connect...

Страница 106: ...h the access panel removed firmly grasp the power cord of the detector con troller at the strain relief and pull the cord from the controller 5 The power cord is connected to X601 on the left side of...

Страница 107: ...xx060 This section gives an overview of the system operation and collection of data To open the XRD COMMANDER program 1 Locate the C diffplus directory 2 Double click on the XRDCMD icon There may be i...

Страница 108: ...show the actual settings for the current measurement Figure 9 2 The scan control area 2 Scan type Choose the scan type from the drop down menu You must select PSD as a detector type in the Details ta...

Страница 109: ...and the location of the K 1 peak In the case of Cu radia tion a Ni filter is included with the V NTEC 1 accessories Settings Quartz Standard Anode E KeV K 1 K 2 K 1 Beta Filter Cu 8 048 26 64 26 70 24...

Страница 110: ...the operation and use of the XRD COMMANDER measure ment software package refer to the DIFFRACplus COMMANDER User Manual M88 Exx060 9 7 Calculate the Optimum Secondary Slit Openings This section descr...

Страница 111: ...anti scatter slit is measured from the center of the goniometer to the edge of the slits The distance for the detector slit is measured from the reference mark on the detector to the edge of the detec...

Страница 112: ...width 4 Physically set the slit settings to the values determined in step 3 5 To implement the settings press the Apply button 6 Download the changes to the V NTEC 1 controller to make them effective...

Страница 113: ...e diffractometer measur ing equipment are maintenance free for the user However Bruker AXS recommends a yearly preventive maintenance inspection To schedule this inspection or for technical support co...

Страница 114: ...X ray window Never drill grind or sand beryllium unless you are a qualified individual using appropriate respiratory equipment and dust containment and collection apparatus Disposal of parts containin...

Страница 115: ...ure 10 1 NOTE Replace the fuse only with the specified replacement see Appendix B Do not substi tute a fuse with a different rating 4 Insert the new fuse into the holder Verify complete seating of the...

Страница 116: ...heck if the HV Enable button is illuminated 2 The High Voltage Enable button is not illuminated Press the High Voltage Enable button If the switch lights the high voltage is enabled If the switch is s...

Страница 117: ...TEC 1 detector see Section 7 5 There is poor instrument resolution FWHM is greater than 0 065 of the 104 reflection of NIST 1976 Repeat the alignment of the 2 DOF mount for the V NTEC 1 detector see S...

Страница 118: ...s in the screen shown in Fig ure 10 2 3 Select COM1 in the drop down list and press Continue Another window appears indicating that Config is now waiting for the controller to boot up Figure 10 3 Boot...

Страница 119: ...ges Non Ambient Chambers Reflectometry Sample Stage Flip Stick Centric Eulerian Cradle D4 Sample Stages 401 A17 D16 435 A17 D15 A17 D15 A17 D15 A17 D15 500 A17 D17 A17 D17 A17 D17 A17 D17 500 A17 D18...

Страница 120: ...er A17 D15 A17 D16 A17 D17 A17 D18 Name Radial Soller V NTEC 1 435 mm Radial Soller V NTEC 1 401 mm Radial Soller V NTEC 1 500 mm Radial Soller V NTEC 1 Push Plug Available Space to Sample Center 82 5...

Страница 121: ...tics Fixed Sample Stage Reflection Rotation Sample Stage Transmission Reflection mode Rotation Sample Stage Transmission Transmission mode Flip Stick 9 position D4 Sample Stage 401 Fixed or variable s...

Страница 122: ...Appendix A Configuration Tables V NTEC 1 Detector User Manual A 4 M88 E01072...

Страница 123: ...15 A 250 V 5 x 20 mm 072 000400 Fan 12 V Rotron 085 000200 Coaxial thin wire cable 085 006100 3 cond 8 2 cable 085 013500 Push button 0 1 switch 085 013800 Cable control to FDC 113 002400 Power supply...

Страница 124: ...00 Mount Assy D4 106mm PXC 1D 472 053700 LV Power Supply Chassis 672 012200 Detector assembly 672 012600 Controller 1D 7KP2912 8BA Fast Diffraction Controller 842 082100 V NTEC 1 Detector 1D A17B10 Op...

Страница 125: ...radiation for V NTEC 1 default 0 5 A17B25 Soller slit 2 5 for V NTEC 1 A17B26 Soller slit 4 for V NTEC 1 A17B27 Air scatter screen 401 mm diameter A17B28 Air scatter screen 435 mm diameter A17B29 Air...

Страница 126: ...r 1 mm 4 mm And 8 mm A17D13 Set of K filters for V NTEC 1 Cr Co and Mo radiation A17D15 Radial Soller Slit for V NTEC 1 435 mm measurement circle A17D16 Radial Soller Slit for V NTEC 1 401 mm measurem...

Страница 127: ...C S3K C79298A3130A76 Cable Serial Communication Control PC to Detector Controller C79298A3220B240 TDC Signal Conditioning board C79298A3320B124 Remote Control board K340C9 Ethernet Crosslink cable 50...

Страница 128: ...Appendix B Spare Parts List V NTEC 1 Detector User Manual B 6 M88 E01072...

Страница 129: ...roller This section describes how to update the firmware on the detector control ler s Flash drive C 1 Setting up the HTTP connection To access the detector controller with a Web browser the user need...

Страница 130: ...Appendix C Updating the Detector Controller Firmware V NTEC 1 Detector User Manual C 2 M88 E01072 Figure C 1 Set up login and password...

Страница 131: ...er Add User menu 4 Click OK 5 Save and download the configuration From the menu bar at the top of the Diffractome ter Configuration window go to File Save and Download 6 A confirmation window appears...

Страница 132: ...or PC by typing the detector controller s IP address into the address field of your browser http 192 168 23 2 NOTE If you are using a local proxy server make sure the detector controller s IP address...

Страница 133: ...Enter Password 4 Initially the user name is user and the password is the corresponding password that was chosen in Section C 1 Enter the username and password and click OK 5 The detector controller me...

Страница 134: ...ould take about one minute 9 When finished a report about the installa tion process will be displayed 10 The update of the PSDWARE is now com plete 11 To activate the update reboot the detector contro...

Страница 135: ...ec onds and switching it on again After reboo ting the detector controller should be reachable with your Web browser at the same IP address 7 There are various services running on the system e g http...

Страница 136: ...Appendix C Updating the Detector Controller Firmware V NTEC 1 Detector User Manual C 8 M88 E01072...

Страница 137: ...M88 E01072 D 1 Appendix D EC Declaration of Conformity See the figure on the next page...

Страница 138: ...Appendix D EC Declaration of Conformity V NTEC 1 Detector User Manual D 2 M88 E01072...

Страница 139: ...Altitude 3 5 Analyze Data Calib raw 7 6 Anti scatter slit assembly length 3 12 measuring distance of 9 9 B Baseline Data 4 2 for D4 5 2 Beam Stop 3 14 adapter 3 14 collision switch 5 8 Installing on...

Страница 140: ...te System C 5 warm up time 9 1 Detector Mount cable strain relief 4 23 measuring circle radius 4 23 setscrew 4 21 Detector Optics 3 12 Detector overview 3 2 Detector Specifications 3 3 Detector Type i...

Страница 141: ...removing 1 3 I Integrated and External FDC configurations 3 5 intensity ratio between K alphas 8 2 IP addresses 6 3 6 8 6 10 C 4 exceptions C 4 IQ OQ PQ 8 5 K K beta Suppression filters 9 7 K beta su...

Страница 142: ...efinition 1 1 High voltage symbol 1 1 Note definition 1 1 proper lifting 1 4 Warning definition 1 1 Scan Continuous Step 9 6 Fixed PSD max length 9 6 Speed 9 6 Type 9 6 Scan Outside Software Limits 10...

Страница 143: ...ement 2 1 energy resolution 2 2 fixed PSD mode 2 1 Integrated vs external FDC 3 1 locked coupled mode 2 1 maximum local count rate 3 3 Optics 3 12 Positional Calibration 7 1 pressurization 3 2 W weigh...

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