Bruker VANTEC-1, Руководство пользователя

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VÅNTEC-1 Detector User Manual Calibration
M88-E01072 7 - 7
2. Use the Browse button to locate the RAW
file saved during the calib.job measurement
(see Figure 7.4).
Figure 7.4 - Locate the RAW file
3. Press Apply to analyze the calibration and
set the resolution and offset of the detector.
4. Ensure that the mode zero offset value is
approximately -5 to -8. Resolution should be
approximately .007.
5. Recalibrate if the standard deviation is
greater than 0.05°. Continue on to the next
step when you have reached a standard
deviation of less than 0.05° (i.e., zero offset
is approximately -5 to -8 and standard devi-
ation is less than 0.05).
6. After changing the detector parameters,
save and download the new configuration.
The calibration is now complete.
After analyzing the calibration file and prior to
executing a measurement, optimize the detector
optics using the Calculate Geometry menu in
the VÅNTEC-1 Setup menu (see “Calculate the
Optimum Secondary Slit Openings” in Section
9.7).
NOTE: Whenever changes have been made in
Config, remember to restart the Measurement
server!