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Agilent 1290 Infinity Binary Pump User Manual

5

How to Optimize the Performance of Your Module

Using Solvent Calibration Tables

Using Solvent Calibration Tables

Importing Solvent Calibration Tables

RC.NET based Agilent graphical user interfaces (ChemStation, EZChrom Elite, 
OpenLab etc.) include data for most commonly used solvents in HPLC. This 
data contains solvent properties and is used for optimum pump control in 
order to ensure best flow and composition accuracy.

If your solvent is not included to the software, please check the Agilent web 
site 

http://www.chem.agilent.com/en-US/Support/Downloads/firmware/Pages/LC
.aspx

 for additional libraries (registration required), which also provides 

updates and optimized data.

If your solvent is neither available in the user interface nor in the library, 
please use generic solvents. "Generic aequeous" gives good results for most 
solvent mixtures with at least 50 % water, which have similar properties as 
pure water. For other solvents with high organic percentage, "Generic organic" 
gives a good approximation.

Importing Solvent Calibration in ChemStation

1

Go to menu 

Instrument > Instrument configuration

.

2

In the 

Instrument Configuration

 screen choose your module and click 

Configure

.

3

Click 

Configure Solvent Type Catalogs

.

4

In 

Solvent Type Catalogs

 click 

Import

.

5

Navigate to the location of the solvent calibration table and click 

Open

.

6

The new solvent will now appear in the 

Solvent Type Catalogs

.

7

The imported solvent is now available for selection as a solvent type, see 

Table 5

 on page 50.

Содержание Infinity Binary Pump VL 1290

Страница 1: ...Agilent Technologies Agilent 1290 Infinity Binary Pump VL User Manual...

Страница 2: ...rms the warranty terms in the sep arate agreement shall control Technology Licenses The hardware and or software described in this document are furnished under a license and may be used or copied only...

Страница 3: ...nformation about the preferred stack setup for your system and the installation of your Agilent 1290 Infinity Binary Pump 4 Using the Pump This chapter explains the operational parameters of the Agile...

Страница 4: ...d Materials for Maintenance This chapter provides information on parts for maintenance 11 Identifying Cables This chapter summarizes information on all cables 12 Hardware Information This chapter desc...

Страница 5: ...iguration 26 Removing the Transport Foam 31 Installing the Pump 32 Flow connections to the pump 35 Installation of seal wash option 39 4 Using the Pump 41 Preparing the Binary Pump 42 Algae Growth in...

Страница 6: ...ce 110 Warnings and Cautions 112 Overview of Maintenance 113 Cleaning the Module 114 Installing Fittings and Capillaries 115 Replacing the Shutoff Valve Panel 116 Replacing the Pressure Sensor 118 Rep...

Страница 7: ...1 Pump Head Assembly Parts 172 Primary Pump Head Parts 174 Secondary Pump Head Parts 178 Purge Valve 182 Cover Parts 183 Leak Parts 184 Fuses 184 Accessory Kit 185 Others 186 11 Identifying Cables 189...

Страница 8: ...ion 228 Dynamic Host Configuration Protocol DHCP 232 Link configuration selection 236 Automatic configuration with Bootp 237 Manual Configuration 247 PC and User Interface Software Setup Setup 253 14...

Страница 9: ...inity Binary Pump User Manual Agilent Technologies 1 Introduction Features 10 Overview of the Binary Pump 11 Pump Principle 12 This chapter gives an introduction to the pump instrument overview and in...

Страница 10: ...performance with a minimum of delay volume Automatic purge function for ease of use and unattended preparation of the system Auto tuning of the delivery cycle for compensation of elasticity and dead v...

Страница 11: ...tability especially at low flow rates for maximum detector sensitivity The flow path of the pump has been optimized for minimal delay of gradients Typical applications are high throughput methods with...

Страница 12: ...sure up to 1200 bar Each channel comprises a pump assembly including independent pump drive for each piston pump head inlet valve outlet valve solvent heat exchanger and an outlet filter The two chann...

Страница 13: ...ally for composition accuracy across pressure it is vital for the compensation algorithm to use the right solvent properties The density of the solvents is increased under the influence of pressure an...

Страница 14: ...ossible to compensate for minor leaks in primary pump chamber inlet valve and seal without the performance of the pump being affected To increase the robustness of the pump it uses a fast defill funct...

Страница 15: ...er Manual Agilent Technologies 2 Site Requirements and Specifications Site Requirements 16 Physical Specifications 19 Specifications 20 This chapter provides information on environmental requirements...

Страница 16: ...c fuses are implemented in the power supply WARNING Module is partially energized when switched off as long as the power cord is plugged in Repair work at the module can lead to personal injuries e g...

Страница 17: ...e easily reached and unplugged Provide sufficient space behind the power socket of the instrument to unplug the cable WARNING Absence of ground connection or use of unspecified power cord The absence...

Страница 18: ...weight of all modules The module should be operated in a horizontal position Condensation WARNING Unintended use of supplied power cords Using power cords for unintended purposes can lead to personal...

Страница 19: ...17 inches Line voltage 100 240 VAC 10 Wide ranging capability Line frequency 50 or 60 Hz 5 Power consumption 350 VA 270 W 922 BTU Maximum Ambient operating temperature 4 55 C 41 131 F Ambient non ope...

Страница 20: ...low accuracy 1 or 10 l min whatever is greater Pumping degassed H2O at 10 MPa 100 bar Pressure operating range Operating pressure range 120 MPa 1200 bar up to 2 ml min Pressure pulsation 1 amplitude o...

Страница 21: ...02 01 SP1 or above Local control Agilent Instant Pilot G4208A B 02 08 or above Communications Controller area network CAN RS232C APG remote ready start stop and shutdown signals LAN Safety and mainte...

Страница 22: ...22 Agilent 1290 Infinity Binary Pump User Manual 2 Site Requirements and Specifications Specifications...

Страница 23: ...k Configuration 26 One Stack Configuration 26 Two Stack Configuration 29 Removing the Transport Foam 31 Installing the Pump 32 Flow connections to the pump 35 Installation of seal wash option 39 This...

Страница 24: ...form your service representative that the instrument may have been damaged during shipment CAUTION Defective on arrival problems If there are signs of damage please do not attempt to install the modul...

Страница 25: ...art lists in Parts and Materials for Maintenance on page 167 Please report any missing or damaged parts to your local Agilent Technologies sales and service office Table 3 Binary Pump Checklist Descri...

Страница 26: ...ystem flow path ensuring minimum delay volume For other possible configurations please refer to the Agilent 1290 Infinity System Manual One Stack Configuration Ensure optimum performance by installing...

Страница 27: ...User Manual 27 Installing the Module 3 Optimizing the Stack Configuration Figure 2 Recommended stack configuration for 1290 Infinity with binary pump front view 9ZiZXidg 6jidhVbeaZg Ejbe HdakZci XVW c...

Страница 28: ...l 3 Installing the Module Optimizing the Stack Configuration Figure 3 Recommended stack configuration 1290 Infinity with binary pump rear view 68 EdlZg A6C id A8 8 ZbHiVi dc 86C 7jh XVWaZ 6cVad YZiZXi...

Страница 29: ...p and thermostat at the bottom of each stack and avoids high stacks Some users prefer the lower height of this arrangement even without the autosampler thermostat A slightly longer capillary is requir...

Страница 30: ...the Module Optimizing the Stack Configuration Figure 5 Recommended two stack configuration for 1290 Infinity with binary pump rear view 86C 7jh XVWaZ id chiVci E adi 6cVad YZiZXidg h cVa dei dcVa 86C...

Страница 31: ...nfinity Binary Pump User Manual 31 Installing the Module 3 Removing the Transport Foam Removing the Transport Foam 1 Open the front cover of the module 2 Carfully remove the protective foam 3 Close th...

Страница 32: ...a horizontal position 2 Ensure the power switch on the front of the module is OFF switch stands out Figure 6 Front of Binary Pump Parts required Description 1 Pump 1 Power cord 1 Agilent Control Soft...

Страница 33: ...ZmiZgcVa 86C kVakZh NOTE In an Agilent 1290 Infinity System the individual modules are connected by CAN cables An Agilent 1200 Series Instant Pilot can be connected to the CAN bus of any module Connec...

Страница 34: ...wer left hand side of the module The power button stays pressed in and the status LED should be green NOTE When the line power button stands out and the green light is off the module is turned off NOT...

Страница 35: ...pump The pump is shipped with tubing and capillary connections installed between solvent selection valve degassing unit pump heads pressure sensor purge valve and Jet Weaver This section describes the...

Страница 36: ...system WARNING Toxic flammable and hazardous solvents samples and reagents The handling of solvents samples and reagents can hold health and safety risks When working with these substances observe app...

Страница 37: ...ry Pump 3 Put the four bottles into the solvent cabinet and screw a bottle head assembly onto each bottle 4 Install the shutoff valve panel at the top left corner of the instrument 5 Connect the solve...

Страница 38: ...y Binary Pump 7 Connect the outlet of the Jet Weaver to the autosampler 8 Connect Waste tubes G4220 67000 to the purge valve outlets at ports 5 and 6 9 Connect the corrugated waste tube to the outlet...

Страница 39: ...mended when using buffers or other non volatile solvents or additives that could deposit on pistons and seals It is used for regularly cleaning these parts automatically 1 Place a wash solvent reservo...

Страница 40: ...40 Agilent 1290 Infinity Binary Pump User Manual 3 Installing the Module Installation of seal wash option...

Страница 41: ...and or Reduce the Algae Problem 43 Setting up the Pump with the Instrument Control Interface 44 Overview 44 Instrument Configuration 45 The Pump User Interface Dashboard Panel 46 Control Settings 48...

Страница 42: ...the channels Prevent blocking of solvent inlet filters never use the pump without solvent inlet filters Growth of algae should be avoided see Algae Growth in HPLC Systems on page 43 Check pump outlet...

Страница 43: ...osition or gradient problems or a complete failure of the pump Small pore high pressure solvent filters usually placed before the injector to plug resulting in high system pressure PTFE frits blockage...

Страница 44: ...erface Setting up the Pump with the Instrument Control Interface Overview Parameters described in following sections is offered by the instrument control interface and can usually be accessed through...

Страница 45: ...ump configuration parameters are in two sections Communication Options Communication The parameters in this dialog box are detected automatically during autoconfiguration Device name Type ID Serial nu...

Страница 46: ...area when the solvent level falls below the specified volume the area turns yellow when the bottle is empty the area turns red Clicking on the solvent bottle displays the Bottle Fillings dialog box T...

Страница 47: ...els are shown in the graphic Control Displays the pump s Control dialog box Method Displays the pump s Method Setup dialog box Set Error Method Sets the method that is loaded if an error occurs to the...

Страница 48: ...eriodically Periodic Off no seal wash is used Single wash the seal will be purged for a specified time Periodic a periodic wash will be applied for a defined period in minutes The option is available...

Страница 49: ...o start priming Off to turn priming off The Prime function is helpful for filling empty solvent lines or if air has entered the pump heads The module draws solvent at high speed with all four pump dri...

Страница 50: ...e of solvent B to any value from 0 through 100 Solvent A always delivers the remaining volume 100 B The solvent B check boxes allow you to turn the solvent B channels on checked or off cleared When th...

Страница 51: ...aximum pressure limit at which the pump will switch itself off protecting the analytical system against over pressure Min is the minimum limit at which the pump will switch itself off for example if a...

Страница 52: ...he values for Channel B are set to the same as those for Channel A This is done to avoid floating disturbances affecting instrument performance Compressibility The compressibility of the mobile phase...

Страница 53: ...e occur linearly from either time zero or the time of the last defined change other parameters change instantaneously at the time defined in the timetable Show Advanced Timetable toggles the timetable...

Страница 54: ...for Different Purposes Activity Solvent Comments After an installation When switching between reverse phase and normal phase both times Isopropanol Isopropanol Best solvent to flush air out of the sy...

Страница 55: ...oth channels 2 Turn on the Prime function 3 Purge the system with 10 ml composition 50 50 and for 10 min 4 Attach a column suitable for isopropanol and set the Max pressure limit to the limit of the c...

Страница 56: ...low path Consider specifications for the pH range given for different materials like flow cells valve materials etc and recommendations in subsequent sections Materials in Flow Path Following material...

Страница 57: ...impurities like metal ions complexing agents oxygen etc Apart from pure chemical corrosion other effects like electro corrosion electrostatic charging especially for non conductive organic solvents s...

Страница 58: ...nds for yellow piston and wash seals which are used in 1290 Infinity pumps and for normal phase applications in 1260 Infinity pumps Polyethylene has a good stability for most common inorganic solvents...

Страница 59: ...Halogenated solvents or mixtures which form radicals and or acids for example 2 CHCl3 O2 2 COCl2 2 HCl This reaction in which stainless steel probably acts as a catalyst occurs quickly with dried chl...

Страница 60: ...regia Zirconium Oxide ZrO2 Zirconium Oxide is inert to almost all common acids bases and solvents There are no documented incompatibilities for HPLC applications Platinum Iridium Platinum Iridium is...

Страница 61: ...he Performance of Your Module Delay Volume and Extra Column Volume 62 Delay Volume 62 How to Configure the Optimum Delay Volume 63 How to Achieve Higher Resolution 65 Using Solvent Calibration Tables...

Страница 62: ...that in every HPLC system there is an additional isocratic segment in the gradient profile at the start of every run Usually the gradient profile is reported in terms of the mixture settings at the p...

Страница 63: ...acid TFA in the analysis of proteins and peptides The effect can be mitigated by increasing the mixer volume The following different Jet Weaver configurations are available The Jet Weaver 35 L 100 L G...

Страница 64: ...w cell Absorption fluctuations can then show up as baseline noise also referred to as mixing noise Applications like impurity quantitation or lowest level compound detection require minimizing this no...

Страница 65: ...st significant effect on resolution is the selectivity and practically varying this term involves changing the type of stationary phase C18 C8 phenyl nitrile etc the mobile phase and temperature to ma...

Страница 66: ...lectivity certainly for small molecules less than about 500 Da The viscosity can be reduced by increasing the temperature but it should be remembered that this can change the selectivity of the separa...

Страница 67: ...gher flow rate and a smaller volume column This equation also shows how to speed up an existing gradient if the flow is doubled but the gradient time is halved k remains constant and the separation lo...

Страница 68: ...ired which also provides updates and optimized data If your solvent is neither available in the user interface nor in the library please use generic solvents Generic aequeous gives good results for mo...

Страница 69: ...oting and Diagnostics Overview of the Module s Indicators and Test Functions 70 Status indicators 71 Power Supply Indicator 71 Module Status Indicator 72 Available Tests vs User Interfaces 73 Agilent...

Страница 70: ...anical or hydraulic failure the module generates an error message in the user interface For each message a short description of the failure a list of probable causes of the problem and a list of sugge...

Страница 71: ...d on the front of the module The lower left indicates the power supply status the upper right indicates the module status Figure 10 Location of Status Indicators Power Supply Indicator The power suppl...

Страница 72: ...atus indicator is red An error condition indicates the module has detected an internal problem which affects correct operation of the module Usually an error condition requires attention e g leak defe...

Страница 73: ...face the available tests and the screens reports may vary see chapter Test Functions and Calibrations Preferred tool should be the Agilent Lab Advisor software see Agilent Lab Advisor Software on page...

Страница 74: ...gnostic capabilities calibration procedures and maintenance routines for all the maintenance routines The Agilent Lab Advisor software also allows users to monitor the status of their LC instruments T...

Страница 75: ...pen Cover 83 Cover Violation 84 Pump Error Messages 85 Pressure of binary pump above upper limit 85 Pressure below lower limit 86 Target pressure not reached for binary pump degasser 86 Degasser s pre...

Страница 76: ...ver 94 Drive position limit 94 Insufficient power of drive encoder LED 94 Drive encoder error 95 Writing the purge valve tag failed 95 Current of primary pump drive too high 96 Current of secondary pu...

Страница 77: ...e user interface when an electronic mechanical or hydraulic flow path failure occurs which requires attention before the analysis can be continued for example repair or exchange of consumables is nece...

Страница 78: ...Probable cause Suggested actions 1 The analysis was completed successfully and the timeout function switched off the module as requested Check the logbook for the occurrence and source of a not ready...

Страница 79: ...inute the error message is generated Probable cause Suggested actions 1 Leak detected in another module with a CAN connection to the system Fix the leak in the external instrument before restarting th...

Страница 80: ...ture A leak is detected when solvent cools the leak sensor causing the leak sensor current to change within defined limits If the current increases above the upper limit the error message is generated...

Страница 81: ...en circuit The resistance across the temperature compensation sensor NTC on the main board is dependent on ambient temperature The change in resistance is used by the leak circuit to compensate for am...

Страница 82: ...Failed Error ID 0068 The cooling fan in the module has failed The hall sensor on the fan shaft is used by the main board to monitor the fan speed If the fan speed falls below a certain limit for a ce...

Страница 83: ...ccurs the leak sensor is cooled by the solvent This changes the resistance of the leak sensor which is sensed by the leak sensor circuit on the main board Open Cover Error ID 0205 The top foam has bee...

Страница 84: ...in place If the foam is removed while the lamps are on or if an attempt is made to switch on for example the lamps with the foam removed the lamps are switched off and the error message is generated P...

Страница 85: ...re has exceeded the upper pressure limit Parameter Measured pressure Probable cause Suggested actions 1 Blockage in flow path after the pressure sensor Check for blockages in the LC system e g purge v...

Страница 86: ...has not been reached within the expected time Parameter Pressure in mbar Probable cause Suggested actions 1 Leak Check for leaks 2 Bottle empty Check bottle filling 3 Wrong solvent viscosity Check so...

Страница 87: ...ve 0 for channel A 1 for channel B With Solvent Selection Valve 2 for channel A1 3 for channel B1 4 for channel A2 5 for channel B2 Probable cause Suggested actions 1 Leak in degasser chamber or degas...

Страница 88: ...the limit while the pump runs in pressure controlled mode e g during a pressure test Parameter None Probable cause Suggested actions 1 The waste container is full Empty waste container 2 Inappropriat...

Страница 89: ...405 Writing the pump encoder tag has failed Parameter 1 4 referring to pump drive Probable cause Suggested actions 1 Pump has been shut down Restart pump Probable cause Suggested actions 1 Defect conn...

Страница 90: ...p drive Drive Encoder failed Error ID 22408 Drive encoder failed during pump drive calibration Probable cause Suggested actions 1 Blockage of the pump drive Drive encoder failed Please contact your Ag...

Страница 91: ...too high Parameter 1 4 referring to pump drive Probable cause Suggested actions 1 Blockage of system before pressure sensor Check for blockage of e g outlet valve filter frit purge valve heat exchang...

Страница 92: ...encoder Error ID 22414 Defect connection between main board and pump drive encoder Parameter 1 4 referring to pump drive Probable cause Suggested actions 1 Valve defect Replace the solvent selection v...

Страница 93: ...valve tag failed Parameter None Probable cause Suggested actions 1 Defect encoder Please contact your Agilent service representative Probable cause Suggested actions 1 Purge valve drive mechanically b...

Страница 94: ...referring to pump drive Insufficient power of drive encoder LED Error ID 22426 Insufficient power of drive encoder LED Parameter 1 4 referring to pump drive Probable cause Suggested actions 1 Pump dr...

Страница 95: ...to pump drive Writing the purge valve tag failed Error ID 22431 Writing the purge valve tag failed Parameter None Probable cause Suggested actions 1 Pump drive encoder is defect Please contact your Ag...

Страница 96: ...e cause Suggested actions 1 Blockage of flow path between primary pump head and pressure sensor e g of the heat exchanger Check for blockages in flow path Please contact your Agilent service represent...

Страница 97: ...e error Error ID 22438 22439 The pump drive failed during calibration Parameter 1 4 referring to pump drive Probable cause Suggested actions 1 Wrong valve head installed Check or replace purge valve h...

Страница 98: ...e Pressure sensor calibration wrong or missing Error ID 22443 Pressure sensor calibration wrong or missing Parameter None Probable cause Suggested actions 1 Pump drive motor is mechanically blocked Pl...

Страница 99: ...D 22499 The seal wash pump has not been detected while being configured or detected before Probable cause Suggested actions 1 Defect cable connection to seal wash pump Check cable connection 2 Defect...

Страница 100: ...100 Agilent 1290 Infinity Binary Pump User Manual 7 Error Information Pump Error Messages...

Страница 101: ...nual Agilent Technologies 8 Test Functions and Calibrations Introduction 102 System Pressure Test 103 System Pressure Test Evaluation 104 Pump Head Leak Test 105 Pump Head Leak Test Evaluation 107 Thi...

Страница 102: ...Interfaces and available test functions Interface Comment Available Function Agilent Instrument Utilities Maintenance tests available System pressure test Agilent Lab Advisor All tests are available S...

Страница 103: ...ting the pressure at which the test is performed The leak rate of high pressure parts is not always a linear function and therefore it is recommended to perform the test at a pressure that corresponds...

Страница 104: ...lank nut you are using is in a good condition and properly tightened 2 Pump leakages Perform the Pump Head Leak test 3 Loose or leaky fittings Tighten the fittings or replace capillaries 4 Autosampler...

Страница 105: ...ston and thereby the parts between the outlet ball valve and the purge valve are tested for leak tightness The test allows for setting the pressure at which the test is performed The leak rate of high...

Страница 106: ...nctions and Calibrations Pump Head Leak Test 1 Run the Pump Head Leak Test with the recommended user interface for further information see Online Help of user interface Figure 13 Pump Head Leak Test R...

Страница 107: ...s not pressurized for better chance of success Re run test 3 Damaged pump seals or pistons Exchange the pump head or pump seals NOTE A wrongly installed pump seal will reduce the life time of the pump...

Страница 108: ...108 Agilent 1290 Infinity Binary Pump User Manual 8 Test Functions and Calibrations Pump Head Leak Test...

Страница 109: ...25 Changing configuration or replacing the Jet Weaver 127 Replacing the Seal Wash Pump 130 Releasing a Stuck Inlet Valve 131 Replacing the Pump Heads 134 Disassembling the Pump Head 139 Disassembling...

Страница 110: ...ty Binary Pump These parts can be accessed from the front simple repairs and don t require to remove the pump from the system stack Figure 15 Maintenance Parts Figure 16 on page 111 shows the flow con...

Страница 111: ...enance 9 Introduction to Maintenance Figure 16 Flow Connections gdb hdakZci gZhZgkd gh EgZhhjgZ hZchdg Id VjidhVbeaZg B mZg Eg bVgn ejbe ZVY Eg bVgn ejbe ZVY HZXdcYVgn ejbe ZVY HZXdcYVgn ejbe ZVY 9Z V...

Страница 112: ...the module can lead to personal injuries e g shock hazard when the cover is opened Do not remove the cover of the module Only certified persons are authorized to carry out repairs inside the module W...

Страница 113: ...ity Binary Pump User Manual 113 Maintenance 9 Overview of Maintenance Overview of Maintenance The following pages describe maintenance simple repairs of the module that can be carried out without open...

Страница 114: ...an use a soft cloth slightly dampened with water or a solution of water and mild detergent WARNING Liquid dripping into the electronic compartment of your module can cause shock hazard and damage the...

Страница 115: ...dures for example goggles safety gloves and protective clothing when opening flow path CAUTION Deformation of fittings and seals Liquid drops under high pressure up to 1200 bar act like solid parts Ti...

Страница 116: ...ired p n Description 1 5067 4124 Shutoff valve 1 G4220 40004 Shutoff valve panel 2 G4220 60035 Tubing kit 140 mm SSV to shutoff valve or degassing unit 2 tubes Preparations In order to avoid leaks rem...

Страница 117: ...al 117 Maintenance 9 Replacing the Shutoff Valve Panel 3 Remove the shutoff valve panel by pulling it downwards 4 After replacing the panel or after completion of other maintenance re install the pane...

Страница 118: ...pen 1 4 5 16 inch Screwdriver Parts required p n Description 1 G4220 60001 Pressure sensor 1200 bar Preparations Turn off pump flow switch off pump NOTE This procedure describes how to replace the pre...

Страница 119: ...sensor for about 2 cm Then unscrew the cable from the pressure sensor 4 Connect the new pressure sensor to the pressure sensor connector 5 Fix the pressure sensor to the instrument chassis 6 Connect t...

Страница 120: ...n Wrench 14 mm G4220 20012 Torque wrench 2 25 Nm Parts required p n Description G4220 60022 Inlet valve primary pump head CAUTION Potential damage of inlet valve Overtightening the valve will damage i...

Страница 121: ...acing the Inlet valve 3 With a 14 mm wrench unscrew the inlet valve and remove it 4 Install inlet valve and tighten it at 10 Nm with a torque wrench 14 mm 5 Attach the inlet tubing at the inlet valve...

Страница 122: ...ed p n Description Wrench 14 mm G4220 20012 Torque wrench 2 25 Nm G4220 20014 2 5 mm Hex Bit Parts required p n Description G4220 60028 Outlet valve 1290 Infinity Pump primary pump head G4220 20020 In...

Страница 123: ...e replaced separately as needed 4 Unscrew the outlet valve with a 14 mm wrench 5 Insert the outlet valve into the pump head Using a torque wrench set 10 Nm and close the outlet valve 6 Insert the heat...

Страница 124: ...124 Agilent 1290 Infinity Binary Pump User Manual 9 Maintenance Replacing the Outlet valve 7 Open the shut off valves and purge the system to remove air...

Страница 125: ...th the solvent selection valve Parts required p n Description 1 G4280 60029 Solvent selection valve 4 G4220 60035 Tubing kit 140 mm SSV to shutoff valve or degassing unit 2 tubes 1 Close shut off valv...

Страница 126: ...ection Valve SSV 3 Remove the connector by pushing up the small clip at the bottom of the connector 4 Install a new SSV by inserting the connector and clipping the SSV panel to the module top panel Th...

Страница 127: ...or optimizing the pump configuration to mixing performance or low delay volumes fast gradients see chapter Optimizing Performance Tools required p n Description 8710 0510 inch wrench 3 mm hex key Part...

Страница 128: ...tandard Jet Weaver Jet Weaver 35 L 100 L G4220 60006 has a front and a rear side with different internal volumes 35 100 L that are optimized for a low delay volume or best mixing performance Please re...

Страница 129: ...Jet Weaver 3 Install new Jet Weaver or flip the Jet Weaver for backside 4 Reinstall the capillary connections The inlet at the bottom of the Jet Weaver is connected to the central port of the pump val...

Страница 130: ...Parts required p n Description 5042 8507 Peristaltic Pump for Seal Wash Preparations Remove the shutoff valve panel Replacing the Shutoff Valve Panel on page 116 and flow connections from and to the...

Страница 131: ...f pump is not generating pressure after being turned off for an extended period of time NOTE Before the system is turned off for an extended period of time it should be flushed with at least 10 IPA to...

Страница 132: ...let Valve 3 Attach a Luer lock syringe with adapter to the tubing and fill it with solvent 4 Reconnect tubing to inlet valve 5 Unscrew tubing at degassing unit and attach the syringe to it 6 Push solv...

Страница 133: ...ser Manual 133 Maintenance 9 Releasing a Stuck Inlet Valve 7 Detach the syringe and reconnect the tubing into the degassing unit 8 Reinstall the capillary connection to the High Pressure Filter Assemb...

Страница 134: ...inary Pump has two pump assemblies for two solvent channels A and B which both consist of two pump drives and pump heads The solvent enters each pump through the primary pump head is transferred to th...

Страница 135: ...mp Head Assembly Channel B right without Seal Wash Option Preparations Switch off pump at the main power switch Remove the front cover CAUTION Limitation of life time The pump head assembly is an exch...

Страница 136: ...hing off the pump bring it to the maintenance position NOTE This procedure describes the replacement of the left pump head assembly Similarly the right pump head assembly can be replaced One pump head...

Страница 137: ...the primary pump head inlet Remove the capillary connection at the top of the secondary pump head to the pump valve If installed remove the tubings of the seal wash option DO NOT REMOVE the capillary...

Страница 138: ...crews step by step not screw by screw 7 Install flow connections Connect the degassing unit outlet to the inlet of the primary pump head and the outlet of the secondary pump head to the inlet of the p...

Страница 139: ...Pump Heads on page 134 steps 1 4 NOTE This procedure describes replacements for the pump heads of channel A Replacement for channel B can be done accordingly The primary pump head does not have a heat...

Страница 140: ...which is a very hard and resistant material but it is sensitive to shearing forces from the side Do not try to remove the pump piston from the rear Do not use the piston for removing pump seals 1 Rem...

Страница 141: ...ng pump chamber housing with pump seal and seal holder If the seal wash option is installed also remove the support ring with wash seal and gasket 4 Remove the piston from the piston housing by pushin...

Страница 142: ...n seals NOTE Damaged pistons cause micro leaks and will decrease the lifetime of the seals 6 Use the soft plastic side of the insert tool for removing the pump seal from the pump chamber housing NOTE...

Страница 143: ...very hard and resistant material but it is sensitive to shearing forces from the side Do not try to remove the pump piston from the rear Do not use the piston for removing pump seals 1 Remove the fil...

Страница 144: ...the piston housing by pushing it to the rear then pull it out from the rear 5 Check the pump pistons for scratches grooves and dents when changing the piston seals NOTE Damaged pistons cause micro lea...

Страница 145: ...1290 Infinity Binary Pump User Manual 145 Maintenance 9 Disassembling the Secondary Pump Head 7 If the wash seal shall be replaced by a new one use the steel side of the insert tool for removing it Wa...

Страница 146: ...ter in square to hex 01018 23702 Insert tool Parts required p n Description 0905 1420 PE seals pack of 2 0905 1718 Wash Seal PE 5062 2484 Gasket seal wash pack of 6 CAUTION Limited life time of the pu...

Страница 147: ...g the pump drive in default position will damage the pump head assembly Bring the pump drive to the maintenance position NOTE This procedure describes how to assemble the secondary pump head using the...

Страница 148: ...any case avoid doing so If the backup seal by accident has been removed from the seal holder insert it in the correct orientation as shown below Please ensure that the cut end faces the seal holder 4...

Страница 149: ...he pump head correctly 6 Assemble the pump head by putting the pump chamber housing on top of the support ring Insert and tighten the two pump head screws NOTE Do NOT install the inlet and outlet valv...

Страница 150: ...alignment piston of the pump head alignment tool 9 Insert the pump head to the pump head alignment tool There are openings for the seal wash support ring and heat exchanger of the secondary pump head...

Страница 151: ...ositions and close the pump head tightly 13 Open the 3 screws which have closed the pump head alignment tool and take out the aligned pump head In case the pump head sticks inside the alignment tool y...

Страница 152: ...pump head assemble and install the high pressure filter assembly using the torque wrench 14 mm hex wrench set to 16 Nm 16 Remove the alignment piston 17 Insert the pump piston 18 Insert both pump head...

Страница 153: ...ition using the Lab Advisor user interface see Disassembling the Pump Head on page 139 Both pump drives must be retracted 21 Install the pump head assembly by fixing the 4 screws using a 4 mm hex key...

Страница 154: ...l damage of valve head or malfunction of valve When the pump is switched on the valve tag is accessed read write and used for correctly positioning the valve If the valve head is replaced while the pu...

Страница 155: ...ve Head 1 Remove all capillary connections Then unscrew the black union nut and remove the head of the purge valve by pulling it to the front 2 Put the new valve head onto the valve drive such that th...

Страница 156: ...ead of channel B Port 2 is connected to the outlet of the pressure sensor Port 3 is connected to the inlet of the pressure sensor Port 4 is connected the outlet of the secondary pump head of channel A...

Страница 157: ...ch 2 25 Nm G4220 20015 Adapter in square to hex 14 mm Hex bit Parts required p n Description 1 01018 22707 PTFE frits pack of 5 1 5067 4728 Seal cap CAUTION Leakage or damaged connection Opening the o...

Страница 158: ...ection from the outlet of the secondary pump head 2 Use a 14 mm hex wrench for opening the filter assembly of the secondary pump head 3 Replace the filter frit and seal cap as desired Please note the...

Страница 159: ...on the module cover First tighten these screws and then tighten the upper screws When This rail is needed for the installation of external valves Tools required Description Pozidrive screwdriver 1 Par...

Страница 160: ...2110 1004 Fuse 10 A t Preparations Switch off the instrument and unplug the main power cable WARNING Fire hazard Using wrong fuses can result in fire hazard For continued protection against fire hazar...

Страница 161: ...e 9 Replacing the Main Power Fuses 1 Use a screwdriver for removing the main fuse carrier from the compartment next to the main power plug Remove the fuse from the carrier 2 Install the new fuse 10A t...

Страница 162: ...r this module When The installation of newer firmware might be necessary if a newer version solves problems of older versions or to keep all systems on the same validated revision The installation of...

Страница 163: ...nel solvent selection valve degassing unit and pump inlets Switch the solvent selection valve if applicable When If the module shall be transported or shipped Parts required p n Description 1 9301 041...

Страница 164: ...mp Module for Transport 2 Remove tubing and capillary connections to other modules and the solvent cabinet Remove tubing plugs Zi LZVkZg DjiaZi id 6jidhVbeaZg 6 6 7 7 caZi 6jidbVi X HZVa LVh dei dcVa...

Страница 165: ...e for Transport 3 Remove the shutoff valve panel by pulling it downwards 4 You may keep internal tubing and capillary connections 5 Remove cable connections to other modules Remove the module from the...

Страница 166: ...ng the Pump Module for Transport 6 Carefully insert the Protective Foam to the front part of the instrument Do not damage any tubing or capillary connections 7 Close the front cover 8 For transport or...

Страница 167: ...of Maintenance Parts 168 Capillaries 169 Solvent Cabinet Kit 170 Seal Wash Option 171 Pump Head Assembly Parts 172 Primary Pump Head Parts 174 Secondary Pump Head Parts 178 Purge Valve 182 Cover Part...

Страница 168: ...valve G4220 60006 Jet Weaver 35 L 100 L G4220 60012 Jet Weaver 380 L OPTIONAL G4220 60001 Pressure sensor 1200 bar G4220 60200 Pump Head Assembly Channel A left with Seal Wash Option G4220 60210 Pump...

Страница 169: ...rts and Materials for Maintenance 10 Capillaries Capillaries p n Description 5067 4655 Capillaries to pump head assemblies channel A and B 2x G4220 87000 Capillary SST Valve to Jet Weaver 300 mm x 0 1...

Страница 170: ...y Pump includes the following parts 5065 9981 Solvent cabinet 1200 Infinity including all plastic parts 9301 1420 3x Solvent bottle transparent 9301 1450 Solvent bottle amber 5067 4124 4x Shutoff valv...

Страница 171: ...User Manual 171 Parts and Materials for Maintenance 10 Seal Wash Option Seal Wash Option Figure 18 Seal wash pump p n Description 5042 8507 Seal wash pump cartridge 5065 9978 Tubing 1 mm i d 3 mm o d...

Страница 172: ...172 Agilent 1290 Infinity Binary Pump User Manual 10 Parts and Materials for Maintenance Pump Head Assembly Parts Pump Head Assembly Parts Figure 19 Pump head assembly parts...

Страница 173: ...ts and Materials for Maintenance 10 Pump Head Assembly Parts Item p n Description 1 G4280 60026 High Pressure Filter Assembly secondary pump head 2 G4220 60028 Outlet valve 1290 Infinity Pump primary...

Страница 174: ...Pump User Manual 10 Parts and Materials for Maintenance Primary Pump Head Parts Primary Pump Head Parts Primary Pump Head With Seal Wash Binary Pump Figure 20 Primary pump head Binary Pump with seal w...

Страница 175: ...pump head 4 G4220 60028 Outlet valve 1290 Infinity Pump primary pump head 5 G4220 20020 Internal gold seal for 1290 Infinity outlet valve 6 0905 1420 PE seals pack of 2 7 G4220 60016 Seal holder inclu...

Страница 176: ...inity Binary Pump User Manual 10 Parts and Materials for Maintenance Primary Pump Head Parts Primary Pump Head Without Seal Wash Binary Pump Figure 21 Primary pump head Binary Pump without seal wash 1...

Страница 177: ...g order pump head 3 G4220 60022 Inlet valve primary pump head 4 G4220 60028 Outlet valve 1290 Infinity Pump primary pump head 5 G4220 20020 Internal gold seal for 1290 Infinity outlet valve 6 0905 142...

Страница 178: ...nual 10 Parts and Materials for Maintenance Secondary Pump Head Parts Secondary Pump Head Parts Secondary Pump Head With Seal Wash Binary Pump Figure 22 Secondary pump head Binary Pump with seal wash...

Страница 179: ...at Exchanger Screw 6 G4220 20001 Spacer Fitting 7 Pump Chamber Housing order pump head 8 0905 1420 PE seals pack of 2 9 G4220 60016 Seal holder including backup ring 10 5062 2484 Gasket seal wash pack...

Страница 180: ...ry Pump User Manual 10 Parts and Materials for Maintenance Secondary Pump Head Parts Secondary Pump Head Without Seal Wash Binary Pump Figure 23 Secondary pump head Binary Pump without seal wash 1 2 3...

Страница 181: ...er secondary pump head only Channel A 5 0515 5237 Heat Exchanger Screw 6 G4220 20001 Spacer Fitting 7 Pump Chamber Housing order pump head 8 0905 1420 PE seals pack of 2 9 G4220 60015 Support ring inc...

Страница 182: ...s and Materials for Maintenance Purge Valve Purge Valve Figure 24 Purge valve parts Item p n Description 5067 4119 Purge valve head 1 1535 4857 Stator screws 2 5068 0004 Purge Valve Stator 3 5068 0005...

Страница 183: ...er Parts Cover Parts Figure 25 Cover Parts Item p n Description 1 5067 4613 Cabinet Kit Side Covers left right Top Cover Tubing Plug Base Cover and Leak Seal 2 5042 9949 Tubing Plug Plastic 5042 9972...

Страница 184: ...nt 1290 Infinity Binary Pump User Manual 10 Parts and Materials for Maintenance Leak Parts Leak Parts Figure 26 Leak funnel Fuses p n Description 5041 8388 Leak funnel p n Description 2110 1004 2x Fus...

Страница 185: ...long T handle 9301 0411 Syringe Plastic 9301 1337 Syringe adapter 5067 4657 SST Capillary 300 x 0 17 mm Pump to Autosampler 5067 4658 SST Capillary 450 x 0 17 mm Pump to Thermostatted Autosampler 0100...

Страница 186: ...d items 1 4 Figure 27 Pump head alignment tool Item p n Description 5067 4699 1290 Infinity pump service kit 1 G4220 20012 Torque wrench 2 25 Nm 2 G4220 20013 4 mm hex bit 3 G4220 20014 2 5 mm Hex Bit...

Страница 187: ...ty Binary Pump User Manual 187 Parts and Materials for Maintenance 10 Others Figure 28 Replacement kit for 1290 Infinity pump head alignment tool piston handle Figure 29 HPLC System Tool Kit Alignment...

Страница 188: ...188 Agilent 1290 Infinity Binary Pump User Manual 10 Parts and Materials for Maintenance Others...

Страница 189: ...Manual Agilent Technologies 11 Identifying Cables Cable Overview 190 Analog cables 192 Remote Cables 194 BCD Cables 197 CAN LAN Cable 199 RS 232 Cable Kit 200 Agilent 1200 Module to Printer 201 This c...

Страница 190: ...t module to 3394 6 integrators 35900 60750 Agilent 35900A A D converter 01046 60105 Analog cable BNC to general purpose spade lugs p n Description 03394 60600 Agilent module to 3396A Series I integrat...

Страница 191: ...ble shielded 3 m for point to point connection 5023 0202 Twisted pair network cable shielded 7 m for point to point connection p n Description G1530 60600 RS 232 cable 2 m RS232 61601 RS 232 cable 2 5...

Страница 192: ...to Agilent modules The other end depends on the instrument to which connection is being made Agilent Module to 3394 6 Integrators Agilent Module to BNC Connector p n 35900 60750 Pin 3394 6 Pin Agilen...

Страница 193: ...1290 Infinity Binary Pump User Manual 193 Identifying Cables 11 Analog cables Agilent Module to General Purpose p n 01046 60105 Pin Pin Agilent module Signal Name 1 Not connected 2 Black Analog 3 Red...

Страница 194: ...Integrators Agilent Module to 3396 Series II 3395A Integrators Use the cable Agilent module to 3396A Series I integrators 03394 60600 and cut pin 5 on the integrator side Otherwise the integrator prin...

Страница 195: ...3395B Integrators p n 03396 61010 Pin 33XX Pin Agilent module Signal Name Active TTL 9 1 White Digital ground NC 2 Brown Prepare run Low 3 3 Gray Start Low NC 4 Blue Shut down Low NC 5 Pink Not conne...

Страница 196: ...2 Brown Prepare run Low 3 Gray 3 Gray Start Low 4 Blue 4 Blue Shut down Low 5 Pink 5 Pink Not connected 6 Yellow 6 Yellow Power on High 7 Red 7 Red Ready High 8 Green 8 Green Stop Low 9 Black 9 Black...

Страница 197: ...ment to be connected to Agilent Module to General Purpose p n G1351 81600 Wire Color Pin Agilent module Signal Name BCD Digit Green 1 BCD 5 20 Violet 2 BCD 7 80 Blue 3 BCD 6 40 Yellow 4 BCD 4 10 Black...

Страница 198: ...ifying Cables BCD Cables Agilent Module to 3396 Integrators p n 03396 60560 Pin 3396 Pin Agilent module Signal Name BCD Digit 1 1 BCD 5 20 2 2 BCD 7 80 3 3 BCD 6 40 4 4 BCD 4 10 5 5 BCD0 1 6 6 BCD 3 8...

Страница 199: ...cted to Agilent modules CAN or LAN connectors CAN Cables LAN Cables p n Description 5181 1516 CAN cable Agilent module to module 0 5 m 5181 1519 CAN cable Agilent module to module 1 m p n Description...

Страница 200: ...0 RS 232 cable 2 m RS232 61601 RS 232 cable 2 5 m Instrument to PC 9 to 9 pin female This cable has special pin out and is not compatible with connecting printers and plotters It s also called Null Mo...

Страница 201: ...ntifying Cables 11 Agilent 1200 Module to Printer Agilent 1200 Module to Printer p n Description 5181 1529 Cable Printer Serial Parallel is a SUB D 9 pin female vs Centronics connector on the other en...

Страница 202: ...202 Agilent 1290 Infinity Binary Pump User Manual 11 Identifying Cables Agilent 1200 Module to Printer...

Страница 203: ...Description 204 Electrical Connections 207 Rear View of the Module 208 Interfaces 209 Overview Interfaces 212 Setting the 8 bit Configuration Switch 216 Special Settings 218 Instrument Layout 220 Ear...

Страница 204: ...perties are the complete communication capabilities CAN LAN and RS 232C memory management ability to update the firmware of the main system Main System Its properties are the complete communication ca...

Страница 205: ...r the G1315A B DAD R the firmware revision for example A for G1315B or B for the G1315C DAD VVV is the revision number for example 102 is revision 1 02 XXX is the build number of the firmware For inst...

Страница 206: ...heir initial firmware revision For example a G1315C DAD SL cannot be downgraded below firmware revision B 01 02 or to a A xx xx Some modules can be re branded e g G1314C to G1314B to allow operation i...

Страница 207: ...ware the RS 232C connector may be used to control the module from a computer through a RS 232C connection This connector is activated and can be configured with the configuration switch The power inpu...

Страница 208: ...Binary Pump User Manual 12 Hardware Information Electrical Connections Rear View of the Module Figure 31 Rear of Binary Pump 8dc jgVi dc hl iX 86C 7jh GH A6C 8dbeVXi aVh EdlZg eaj 6E GZbdiZ EdlZg hjee...

Страница 209: ...Pump G1312C Bin Pump VL 1376A Cap Pump G2226A Nano Pump G5611A Bio inert Quat Pump 2 Yes No Yes 1 Yes G4220A B Bin Pump G4204A Quat Pump 2 No Yes Yes No Yes CAN DC OUT for CAN slaves G1361A Prep Pump...

Страница 210: ...OZERO Others G1170A Valve Drive 2 No No No No No Requires a HOST module with on board LAN e g G4212A or G4220A with minimum firmware B 06 40 or C 06 40 or with additional G1369C LAN Card G1316A C TCC...

Страница 211: ...ules LAN connector as interface to the control software RS 232C as interface to a computer REMOTE connector as interface to other Agilent products Analog output connector s for signal output NOTE The...

Страница 212: ...dule from a computer through RS 232C connection using the appropriate software This connector can be configured with the configuration switch module at the rear of the module Refer to Communication Se...

Страница 213: ...gnal Output The analog signal output can be distributed to a recording device For details refer to the description of the module s main board Table 10 RS 232C Connection Table Pin Direction Function 1...

Страница 214: ...m s critical parts in case any module detects a serious problem To detect whether all participating modules are switched on or properly powered one line is defined to summarize the POWER ON state of a...

Страница 215: ...s activities 3 START L Request to start run timetable Receiver is any module performing run time controlled activities 4 SHUT DOWN L System has serious problem for example leak stops pump Receiver is...

Страница 216: ...col and instrument specific initialization procedures All modules with on board LAN e g G1315 65C D G1314D E F G4212A B G4220A B Default is ALL switches DOWN best settings Bootp mode for LAN and 19200...

Страница 217: ...SW 8 LAN 0 0 Link Configuration Init Mode Selection Auto negotiation 0 x x x x x 10 MBit half duplex 1 0 0 x x x 10 MBit full duplex 1 0 1 x x x 100 MBit half duplex 1 1 0 x x x 100 MBit full duplex 1...

Страница 218: ...he following switch settings and power the instrument up again the instrument firmware stays in the resident mode It is not operable as a module It only uses basic functions of the operating system fo...

Страница 219: ...itch settings and power the instrument up again a forced cold start has been completed CAUTION Loss of data Forced cold start erases all methods and data stored in the non volatile memory Exceptions a...

Страница 220: ...is then housed in a metal inner cabinet which is enclosed by a plastic external cabinet The advantages of this packaging technology are virtual elimination of fixing screws bolts or ties reducing the...

Страница 221: ...terface when the limit is exceeded Some counters can be reset to zero after the required maintenance procedure Using the EMF Counters The user settable EMF limits for the EMF Counters enable the early...

Страница 222: ...222 Agilent 1290 Infinity Binary Pump User Manual 12 Hardware Information Early Maintenance Feedback...

Страница 223: ...ootP Service 237 How BootP Service Works 238 Situation Cannot Establish LAN Communication 238 Installation of BootP Service 239 Two Methods to Determine the MAC Address 241 Assigning IP Addresses Usin...

Страница 224: ...ss Control address for further reference The MAC or hardware address of the LAN interfaces is a world wide unique identifier No other network device will have the same hardware address The MAC address...

Страница 225: ...ou Have to Do First 2 Connect the instrument s LAN interface see Figure 35 on page 225 to the PC network card using a crossover network cable point to point or a hub or switch using a standard LAN cab...

Страница 226: ...requesting the parameters from a network based DHCP Server using the so called Dynamic Host Configuration Protocol This mode requires a LAN onboard Module or a G1369C LAN Interface card see Setup DHCP...

Страница 227: ...n Switch The module is shipped with all switches set to OFF as shown above NOTE To perform any LAN configuration SW1 and SW2 must be set to OFF Table 15 Factory Default Settings Initialization Init Mo...

Страница 228: ...eters obtained become the active parameters immediately They are not stored to the non volatile memory of the module Therefore the parameters are lost with the next power cycle of the module Figure 37...

Страница 229: ...otp In this case he starts the Bootp Server temporarily powers on the module using the initialization mode Bootp Store waits for the Bootp cycle to be completed closes the Bootp Server and powers off...

Страница 230: ...zation mode Using Stored is selected the parameters are taken from the non volatile memory of the module The TCP IP connection will be established using these parameters The parameters were configured...

Страница 231: ...then close the session select the initialization mode Using Stored power on again and establish the TCP IP connection using the new parameters When the module is wired to the PC directly e g using a c...

Страница 232: ...G1369C LAN Interface Card 1120 1220 LC System When the initialization mode DHCP is selected the card tries to download the parameters from a DHCP Server The parameters obtained become the active para...

Страница 233: ...may take some time until the DHCP server has updated the DNS server with the hostname information 2 It may be necessary to fully qualify the hostname with the DNS suffix e g 0030d3177321 country compa...

Страница 234: ...t the MAC address can be found under Details in the LAN section Figure 42 LAN Setting on Instant Pilot 2 Set the Configuration Switch to DHCP either on the G1369C LAN Interface Card or the main board...

Страница 235: ...Control Software e g Agilent ChemStation LabAdvisor Firmware Update Tool and use MAC address as host name e g 0030d3177321 The LC system should become visible in the control software see Note in secti...

Страница 236: ...e itself for 10 or 100 Mbps half duplex operation For example when connected to a non negotiating 10 Mbps hub the LAN interface will be automatically set to operate at 10 Mbps half duplex If the modul...

Страница 237: ...dresses for Agilent instruments on a LAN The BootP service must be running TCP IP network protocol and cannot run a DHCP server NOTE All examples shown in this chapter will not work in your environmen...

Страница 238: ...powered on Powering down the instrument causes it to lose its IP address so the Agilent BootP Service must be running every time the instrument powers up If the Agilent BootP Service runs in the backg...

Страница 239: ...tomatically click Cancel to stop it 4 Open Windows Explorer 5 Go to the BootP directory on the Agilent ChemStation DVD and double click BootPPackage msi 6 If necessary click the Agilent BootP Service...

Страница 240: ...be used The default subnet mask is 255 255 255 0 The default gateway is 192 168 254 11 13 On the BootP Settings screen click OK The Agilent BootP Service Setup screen indicates completion 14 Click Fi...

Страница 241: ...each device that requests configuration information from BootP 3 Click OK to save the values or Cancel to discard them The editing ends 4 After each modification of the BootP settings i e EditBootPSe...

Страница 242: ...will not be updated if it is open The contents will be similar to the following 3 Record the hardware MAC address for example 0010835675AC 4 The Error means the MAC address has not been assigned an IP...

Страница 243: ...e all instruments have been added The Do you want to log BootP requests box must be unchecked when you have finished configuring instruments otherwise the log file will quickly fill up disk space 3 Cl...

Страница 244: ...e EditBootPSettings a stop or start of the BootP service is required for the BootP service to accept changes See Stopping the Agilent BootP Service on page 245 or Restarting the Agilent BootP Service...

Страница 245: ...atically when your PC reboots To change Agilent BootP Service settings you must stop the service make the changes and then restart the service Stopping the Agilent BootP Service 1 From the Windows con...

Страница 246: ...In the Edit BootP Addresses screen press Add to create a new entry or select an existing line from the table and press Modify or Delete to change the IP address comment subnet mask for example in the...

Страница 247: ...tile memory of the module It never affects the currently active parameters Therefore manual configuration can be done at any time A power cycle is mandatory to make the stored parameters become the ac...

Страница 248: ...g on Windows START button and select Run Type cmd and press OK 2 Type the following at the system DOS prompt c telnet IP address or c telnet host name Figure 49 Telnet Starting a session where IP addr...

Страница 249: ...ress Enter where parameter refers to the configuration parameter you are defining and value refers to the definitions you are assigning to that parameter Each parameter entry is followed by a carriage...

Страница 250: ...e information about the LAN interface MAC address initialization mode Initialization mode is Using Stored active TCP IP settings TCP IP status here ready connected to PC with controller software e g A...

Страница 251: ...ng the configuration parameters type exit and press Enter to exit with storing parameters Figure 54 Closing the Telnet Session NOTE If the Initialization Mode Switch is changed now to Using Stored mod...

Страница 252: ...he module to the network the Instant Pilot G4208A can be used 1 From the Welcome screen press the More button 2 Select Configure 3 Press the DAD button 4 Scroll down to the LAN settings Figure 55 Inst...

Страница 253: ...tup PC Setup for Local Configuration This procedure describes the change of the TCP IP settings on your PC to match the module s default parameters in a local configuration see also Initialization mod...

Страница 254: ...finity Binary Pump User Manual 13 LAN Configuration PC and User Interface Software Setup Setup User Interface Software Setup Install you user interface software according the provided User Interface S...

Страница 255: ...es 14 Appendix General Safety Information 256 The Waste Electrical and Electronic Equipment WEEE Directive 2002 96 EC 259 Radio Interference 260 Sound Emission 261 Agilent Technologies on Internet 262...

Страница 256: ...erminal Indicates eye damage may result from directly viewing the light produced by the deuterium lamp used in this product The apparatus is marked with this symbol when hot surfaces are available and...

Страница 257: ...y the following must be observed Do not remove instrument covers when operating Before the instrument is switched on all protective earth terminals extension cords auto transformers and devices connec...

Страница 258: ...components with power cable connected Do not operate the instrument in the presence of flammable gases or fumes Operation of any electrical instrument in such an environment constitutes a definite sa...

Страница 259: ...all Electric and Electronic appliances from 13 August 2005 NOTE This product complies with the WEEE Directive 2002 96 EC marking requirements The affixed label indicates that you must not discard thi...

Страница 260: ...t Technologies to ensure proper functionality and compliance with safety or EMC regulations Test and Measurement If test and measurement equipment is operated with equipment unscreened cables and or u...

Страница 261: ...ration This statement is provided to comply with the requirements of the German Sound Emission Directive of 18 January 1991 This product has a sound pressure emission at the operator position 70 dB So...

Страница 262: ...y Binary Pump User Manual 14 Appendix Agilent Technologies on Internet Agilent Technologies on Internet For the latest information on products and services visit our worldwide web site on the Internet...

Страница 263: ...0 cables analog 190 BCD 190 CAN 191 LAN 191 overview 190 remote 190 RS 232 191 CAN cable 199 capillaries 115 cleaning 114 compensation sensor open 81 compensation sensor short 82 condensation 18 confi...

Страница 264: ...ad leak test 107 purge valve failed 93 reading of purge valve tag failed 93 reading the pump encoder tag failed 89 remote timeout 79 seal wash pump was missing when tried to turn on 99 shutdown 79 sol...

Страница 265: ...ed 25 missing 25 PC and User Interface Software Setup 253 performance specifications 20 performance Optimization 61 physical specifications 19 power considerations 16 power consumption 19 power cords...

Страница 266: ...ndicator 72 System pressure test error message 104 system setup and installation optimizing stack configuration 26 T target pressure not reached for binary pump degasser 86 TCP IP parameter configurat...

Страница 267: ...Agilent 1290 Infinity Binary Pump User Manual 267 Index...

Страница 268: ...m Agilent Technologies In This Book This manual contains technical reference information about the Agilent 1290 Infinity Binary Pump G4220B introduction and specifications installation using and optim...

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