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Measuring system XS22-E2010  

2 Overview 

 

XS22_E2010 

2  Overview of the measuring system 

The measuring system serves the measuring of the oxygen partial pressure 
in  vacuum.  It  consists  of  a  probe  and  an  integrated  control  and  signal 
processing electronics and an integrated control and evaluation electronics 
(E2010). The probe can be directly installed in vacuum systems.  

The electronic unit E2010, developed for panel mounting, provides the power 
supply  for  ZIROX®  sensors,  evaluates  signals  and  displays  measuring 
results in the form of a standard signal (4-20 mA) for process control. 

The electronics realizes the following functions: 

  Power supply and control of sensor heating 

  Processing of the thermoelectric and cell voltage of the probe to the 

oxygen concentration  

  Output of the oxygen concentration as a standard signal 

  Calibration 

  Reference air supply by internal pump (option) 

The probe is provided with a KF40-flange. Others on request. 

Because of its specially  adapted construction for vacuum applications, the 
probe  is  not  suitable  for  measurements  of  oxygen  concentrations  in  the 
percentage range. The relative error under normal pressure is > 20%.  

The probe must not be used in gases with high thermal conductivity (e.g. H

2,

 

He, NH

3

) at ambient pressure.  

The sensor element of the vacuum probe consists of a partially closed solid 
electrolyte tube. The reference electrode and a resistance heater are located 
inside the tube. The measuring electrode outside the solid electrolyte tube 
contains  a  thermocouple  for  the  temperature  regulation  of  the  sensor 
element.  The  protective  tube  as  part  of  the  probe  is  required  for  the 
symmetric creation of a heating field and serves the protection of the sensor 
from  parasitic  coating.  Without  a  protective  tube,  the  required  probe 
temperature  cannot  be  reached  and  the  thermal  asymmetry  increases 
significantly. 

Unlike probes, which are used under normal pressure, the vacuum probe is 
not calibration-free. Reasons are the inside heater of the sensor tube used 
in  this  probe  and  the  energy  removal  of  the  heated  sensor  element 
depending  on  the  pressure  and  the  ambient  gases.  Due  to  the  lack  of 
isothermal  electrodes,  the  validity  of  the  Nernst  equation  is  not  given. 
Usually,  running  the  production  unit  with  empirically  determined  sensor 
signals  is  sufficient  for  the  process  management.  The  calibration  by  the 
manufacturer  is  conducted  under  normal  pressure  as  a  calibration  of  the 
asymmetry voltage (zero-point-calibration). 

 

In operating status the ceramic front heats up to a temperature of 

about 700 °C. Burn hazard! 

danger

 

Summary of Contents for XS22

Page 1: ...rg 21 D 17489 Greifswald 49 0 3834 8309 00 Fax 29 E mail info zirox de ZIROX Oxygen Measuring Technology Measuring System Vacuum probe XS22 Electronic unit E2010 for oxygen measurements in vacuum appl...

Page 2: ...2 XS22_E2010...

Page 3: ...n 13 5 1 Installation 13 5 2 Reference air supply for ZIROX probes 13 5 3 Probe mounting 13 5 4 Waiting for operating state 13 6 Parametrization 14 6 1 Menu operation an example 14 6 2 Display 14 6 3...

Page 4: ...4 XS22_E2010...

Page 5: ...nly be ensured if the contents of this manual are known Therefore all chapters of this manual must be read carefully prior to operating the VMS Pages charts and figures are numbered consecutively 1 2...

Page 6: ...pical examples are Measurings in vacuum processes PVC CVD other plasma processes Measurings in process gases conducted under non standard pressure e g surface treatment processes Measurings in science...

Page 7: ...gases with high thermal conductivity e g H2 He NH3 at ambient pressure The sensor element of the vacuum probe consists of a partially closed solid electrolyte tube The reference electrode and a resis...

Page 8: ...at flange Diameter of the probe 16 mm Length of the probe 140 300 mm User specific Thermocouple Type B Heater voltage 24 V Approx 30 W Adjusted 17 W Heater resistance 20 Installation requirements DN2...

Page 9: ...ee IP 30 Front IP52 Working temperature 0 40 C Storage temperature 0 50 C Set temperature 700 C Display Double spaced LCD display 2 x 16 digits Input signal Sensor and thermoelectric Output signal 4 2...

Page 10: ...on and operation of E2010 4 1 Front keys The display and the keys for parametrization are located on the front Menu key scroll or select the requested parameter ENTER key activate or enter adjusted pa...

Page 11: ...and outputs are located on the rear Figure 3 Rear view E2010 with connections Terminal strip X1 probe connections Terminal strip X2 Power supply output signal Pin Description Cable 1 AINCOM brown 2 V...

Page 12: ...06 105 ppm O2 Oxygen concentration in ppm A1CR A1xxx xCR A120 9 20 9 mV Cell voltage in mV A2CR A2xxx xCR A2749 9 749 9 C Measuring temperature in C The parameters are set by the keys of the front cov...

Page 13: ...the manufacturer After starting the system E2010 with connected sensor the reference air flow must be checked by an inserted flow meter 5 10 l h resp approx 100 200ml min and if applicable adjusted v...

Page 14: ...er 4 1 With help of both keys an offset calibration zero point calibration in clean air and a span gas calibration is possible The complete menu is shown schematically in figure 4 p 18 The sensor can...

Page 15: ...ng parameters are adjustable in the menu SETTINGS OUTPUT VALUE Valid for display and analog output Vol O2 Vol ppm O2 mbar O2 atm O2 Vz mV OUTPUT VALUE log 10 linear for Vz linear only OUTPUT 4 20 mA C...

Page 16: ...the measuring gas With the zero calibration the working point in ambient air is calibrated with 20 64 vol O2 6 5 Span gas calibration After calling the SPAN GAS concentration in the calibration menu...

Page 17: ...Measuring system XS22 E2010 6 Parametrization 17 XS22_E2010 6 8 Menu navigation of calibration diagram Fig 4 Diagram offset and span gas calibration...

Page 18: ...atus 18 XS22_E2010 7 Status display error messages No Display LED red LED green 1 OK off on 2 Limit value on on 3 Probe temperature 700 C flashing off 4 Thermocouple broken 5 System error In status 3...

Page 19: ...causes Fault clearance Red LED off no supply voltage No supply voltage at the probe Check power supply Internal fuse switched off Send probe to service Green LED off no ready signal Probe is too coole...

Page 20: ...20 XS22_E2010...

Page 21: ...al pressure of oxygen at reference electrode pO2 measuring gas partial pressure of oxygen at measuring electrode After inserting the known values of the natural constants the following applies 42 46 e...

Page 22: ...different pumps over the pressures measured in a higher pressure range with a capacity meter in the medium pressure range with the Pirani device and in the lower pressure range at a cold cathode The j...

Page 23: ...icient to determine the probe signals empirically in a successful trial The operating mode has to be set up so as to receive the requested probe signal Due to different parameter impacts on the raw si...

Page 24: ...24 XS22_E2010...

Page 25: ...ot permitted either A connection of ZIROX and non ZIROX products voids any warranty claims Warranty and warranty claims are only accepted if they are in accordance with the General Sales and Delivery...

Page 26: ...26 XS22_E2010...

Page 27: ...Measuring system XS22 E2010 11 Declaration of conformity 27 XS22_E2010 11 Declaration of conformity...

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