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8530 Shatterbox 

Page 5 of 28 

SPEX SamplePrep LLC                                   January 2010 

 

3.0 UNPACKING 

 

The 8530 Shatterbox mechanism and its cabinet are shipped assembled, and carefully packed 
to avoid damage during shipping. Any visible damage to the shipping container should 
immediately be reported to the carrier. If there is no visible damage, remove all packing 
documents from the exterior of the box, and after completion of your inspection, file in your 
records.  
 
Before unpacking the 8530 Shatterbox, place the shipping carton upright and as close as 
possible to the mills intended location. Open the top of the shipping box. Remove the top and 
body of the carton. Note that if the tape holding the carton’s bottom piece together is slit on 
one side, that flap can be folded down and the Shatterbox rolled off after unlocking the casters.  
 
A plug-in line cord, an extra set of 51793 drive belts, an extra set of fuses, and a 31688 Friction 
Disc are included with your new Shatterbox. One Friction Disc (a circle of thin rubber matting) 
should always be kept in the recess off the capsule container, to cushion the grinding container, 
reduce the noise of the grinding, and prevent unnecessary and rapid wear of the clamp and 
capsule retainer. 
 
Move the mill to the location where it is likely to stay, lock the casters, and open the lid. Please 
note that the Shatterbox should always be installed and operated on a level surface. Check the 
power switch, which is on the back of the cabinet, next to the electrical inlet (Diagram C, Item 
48); this switch should be in the off position (the 0 should be pushed in) when the power cord is 
first attached. Look for any hidden damage that may have occurred during shipping. 
 
The 8530 Shatterbox comes fully assembled. However, 

before plugging the Shatterbox in and 

using the controls for the very first time, first inspect the drive mechanism to make sure it is 
properly linked and aligned

. The Shatterbox was tested before shipment, but there are four 

flexible belts connecting two drive arms, one on the motor and one on the capsule retainer. 
The belts can become dislodged during shipping.  

If the Shatterbox is run with the drive 

mechanism uncoupled or misaligned, damage can result

 
To inspect the drive mechanism, remove the access panel on the back of the case. (Note that in 
general this panel should not be removed without unplugging the power cord.) Check the belt 
linkage between the arm on the motor and the arm on the rotating funnel on the bottom of the 
capsule assembly. The two arms should be parallel and unbent, connected by four belts (O-
rings) in a diamond pattern that overlaps at the corners (Diagram B, item 34). (The coupling arm 
is attached to the top of the motor shaft. The eccentric arm is attached to the bottom of the 
rotating funnel.)  Spin the arms by hand; the motor arm and the funnel arm should rotate 
together smoothly. 
 
If the drive belts have come off, replace them as pictured in Diagram B: in a diamond pattern, 
two belts up and two belts down.    Spin the arms by hand. 
 

Summary of Contents for ENCLOSED SHATTERBOX 8530

Page 1: ...erty St Metuchen NJ 08840 732 623 0465 www spexsampleprep com 8530 ENCLOSED SHATTERBOX OPERATING MANUAL For 8530 115 and 8530 230 Shatterbox with Serial Numbers 07000 and higher this manual is Part No...

Page 2: ...5 1 Grinding Containers 13 6 0 Maintenance 17 6 1 Shatterbox Part Numbers 17 6 2 Cleaning the Shatterbox 17 6 3 Replacing Drive Belts 17 6 4 Clamp Mechanism Maintenance and Replacement 18 6 5 Tighten...

Page 3: ...ntainers are available in hardened steel tungsten carbide alumina ceramic and zirconia ceramic The full range of Shatterbox grinding containers is described in detail in the SPEX Handbook of Sample Pr...

Page 4: ...7 7 two prong plug supplied NOTE Operator is responsible for supplying alternate line cord plug if required Fuses 115V 60Hz version 10 amp slow blow fuse in inlet module 230V 50Hz version 5 amp slow...

Page 5: ...ace Check the power switch which is on the back of the cabinet next to the electrical inlet Diagram C Item 48 this switch should be in the off position the 0 should be pushed in when the power cord is...

Page 6: ...arms properly separated tighten the setscrews use a 1 8 Allen wrench As re installing the access panel note the electrical inlet on off switch and the fuse holder on the left side of the access panel...

Page 7: ...S CLAMP A CONTAINER IN PLACE WHEN RUNNING THE SHATTERBOX 2 DO NOT OVERTIGHTEN THE CLAMP 3 DO NOT OPEN THE LID UNTIL THE LID LATCH IS DISENGAGED 4 ALWAYS UNPLUG THE MILL BEFORE OPENING THE CABINET ACCE...

Page 8: ...ertightening the clamp can damage it Such damage is not covered by the warranty The different parts of the clamp are illustrated in Diagram A To use the clamp first swing the clamp arm to the left sid...

Page 9: ...will light up The timer can now be programmed Pressing this switch to the off position 0 will switch off power to the mill 4 5 2 Digital Timer The timer includes a minutes seconds numerical display p...

Page 10: ...ts 2 55 2 50 2 45 etc Every time power is turned off and back on the timer will revert to the 3 00 default setting To keep another timer setting leave the power on If power is not interrupted the time...

Page 11: ...stay latched After 5 seconds the original timer setting will re appear and the lid latch will release To have the mill pause during a run and retain the timer setting push the pause button The motor...

Page 12: ...lement s from the container Clamp the container into the capsule retainer Make sure that the friction disc is properly placed and the grinding container is firmly seated If the clamp is properly adjus...

Page 13: ...f and tungsten carbide for the small amounts of Ti Ta and Nb present Performance is also important the denser the grinding container material the more rapid the grinding Tungsten carbide is the denses...

Page 14: ...a Large 8521 Large Hardened Steel grinding container with puck and ring Typical sample capacity 60 100 grams sample volume range 30 120 ml The sample volume ranges given above are estimates not absolu...

Page 15: ...amp causing damage to both the mill and container 5 1 4 Emptying and Cleaning the Grinding Container The grinding container is usually emptied by brushing out the ground sample Typically a technician...

Page 16: ...ner it will get Particle size can almost always be lowered further by reducing the sample size or lengthening the grinding time or both Dry grinding is relatively efficient for most brittle materials...

Page 17: ...hly Diagram A Item 13 Clean off any excess dust or dirt from the outer segments of the clamp with special attention being placed on the hinge sections and on the roller It may be necessary to oil the...

Page 18: ...p levers are replaced in a similar way by pushing the pin out of the yoke removing the old arm or lever replacing it re inserting the pin and holding the pin in place with a C clip 6 5 Tightening or R...

Page 19: ...the door on the fuse compartment by gently prying it open at the top and flipping it down Use a small screwdriver to gently pry the red fuse holder out of the compartment as shown in Figure 3 Remove t...

Page 20: ...uter Dimensions dia x height 17 5 x 8cm Weight 12 5kg Recommended Load 20 60ml Complete with Dish Lid Ring Puck Gasket 8505 Alumina Ceramic Grinding Container Outer Dimensions dia x height 15 2 x 8cm...

Page 21: ...lete with Dish Lid Puck Gasket 8507R Rack Holds one or three 8507 or 8508 grinding containers Rack base assembly and lid included rack with three grinding containers lifts easily in and out of Shatter...

Page 22: ...of 28 SPEX SamplePrep LLC January 2010 This page contains restricted content To download the full unabridged version of this manual please visit our website at www spexsampleprep com or call Customer...

Page 23: ...of 28 SPEX SamplePrep LLC January 2010 This page contains restricted content To download the full unabridged version of this manual please visit our website at www spexsampleprep com or call Customer...

Page 24: ...of 28 SPEX SamplePrep LLC January 2010 This page contains restricted content To download the full unabridged version of this manual please visit our website at www spexsampleprep com or call Customer...

Page 25: ...of 28 SPEX SamplePrep LLC January 2010 This page contains restricted content To download the full unabridged version of this manual please visit our website at www spexsampleprep com or call Customer...

Page 26: ...of 28 SPEX SamplePrep LLC January 2010 This page contains restricted content To download the full unabridged version of this manual please visit our website at www spexsampleprep com or call Customer...

Page 27: ...of 28 SPEX SamplePrep LLC January 2010 This page contains restricted content To download the full unabridged version of this manual please visit our website at www spexsampleprep com or call Customer...

Page 28: ...site www spexsampleprep com E mail sampleprep spexcsp com In Europe please contact our European Headquarters at SPEX CertiPrep Ltd 2 Dalston Gardens Stanmore Middlesex HA7 1BQ United Kingdom Tel 44 0...

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