TABLE OF CONTENT
1
Technical Specifications of the Titrator TitroLine® 5000 ................................... 81
1.1
Summary ................................................................................................................................. 81
1.2
Specifications Titrator TitroLine
®
5000 .................................................................................... 82
1.3
Warning and safety information .............................................................................................. 84
2
Unpacking and First Operation ............................................................................ 85
2.1
Unpacking and First Operation of the titrator .......................................................................... 85
2.2
Connection and installing of Piston Burette and magnetic stirrer TM 50 ................................ 85
2.3
Connecting the Titrator - Combination with Accessories and Additional Devices .................. 86
2.3.1
Back panel of the titrator TitroLine® 5000 .............................................................................. 86
2.3.2
Connection ports of the TitroLine® 5000 . Connection of Electrodes ..................................... 86
2.3.3
Connecting a printer ................................................................................................................ 86
2.3.4
Connecting a USB device (manual controller, keyboard, memory device, hub) .................... 86
2.3.5
Connection of analytical balances ........................................................................................... 86
2.4
Setting the Language of the Country ...................................................................................... 87
2.5
Dosing unit and Accessories ................................................................................................... 89
2.6
Initial Filling and Rinsing ......................................................................................................... 90
3
Working with the Titrator TitroLine
®
5000 ........................................................... 92
3.1
Front Keyboard ........................................................................................................................ 92
3.2
Display ..................................................................................................................................... 92
3.3
Manual controller “mouse“ ...................................................................................................... 93
3.4
External PC Keyboard ............................................................................................................. 93
3.5
Menu Structure ........................................................................................................................ 94
3.6
Main Menu ............................................................................................................................... 96
3.6.1
Automatic Titration .................................................................................................................. 96
3.6.2
Calibration (CAL menu) ........................................................................................................... 98
3.6.3
Manual Titration ..................................................................................................................... 101
3.6.4
Dosage .................................................................................................................................. 103
4
Method Parameters ............................................................................................. 105
4.1
Method editing and new method ........................................................................................... 105
4.2
Default methods .................................................................................................................... 106
4.3
Copy Methods ....................................................................................................................... 106
4.4
Delete Methods ..................................................................................................................... 107
4.5
Print method .......................................................................................................................... 107
4.6
Change Method Parameters ................................................................................................. 107
4.6.1
Method type ........................................................................................................................... 108
4.6.2
Titration mode ....................................................................................................................... 108
4.6.3
Result .................................................................................................................................... 110
4.6.4
Titration parameters .............................................................................................................. 119
4.6.5
‘End-point titration’ Titration parameters ............................................................................... 127
4.6.6
Dosing parameter .................................................................................................................. 128
4.6.7
Sample identification ............................................................................................................. 129
4.6.8
Documentation ...................................................................................................................... 130
5
System settings ................................................................................................... 131
5.1
Calibration settings ................................................................................................................ 131
5.2
Reagents
– Dosing unit ......................................................................................................... 133
5.2.1
Replacing the dosing unit ...................................................................................................... 133
5.2.2
Replacing the titration solution .............................................................................................. 138
5.3
Globale Memory .................................................................................................................... 138
5.4
RS232 Settings ..................................................................................................................... 139
5.5
Connection of Printers ........................................................................................................... 141
5.6
Stirrer ..................................................................................................................................... 142
5.7
Date and Time ....................................................................................................................... 142
5.8
RESET .................................................................................................................................. 143
5.9
Device Information ................................................................................................................ 143
5.10
System Tone ......................................................................................................................... 144
5.11
Data exchange ...................................................................................................................... 144
5.12
Software Update .................................................................................................................... 146
