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Sartorius MA37, Operating Instructions Manual

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44

Calibration and Adjustment

Operating Instructions Moisture Analyzer MA37

Viewing the Calibration Report

 

Calibration/Adjustment

MA performance test
Weighing system adjustment
Calibration report

 

t

  To view the most recent calibration reports: Go to the 

Calibration/Adjustment

 

menu and select the 

Calibration report

 submenu .

Here you can select the most recent reports for the MA performance tests  
or weighing system adjustments and then access the most recent calibration 
reports, which are sorted by date . 
Up to 99 entries per day are saved . Calibration reports older than 30 days are 
deleted .

 

y

  Menu Calibration report . 

Example of a Calibration Report:

--------------------
2014-07-29     12:02
    Sartorius
Mod.          MA37-1
SerNo.    0031710609
BAC:        00-53-01
APC:        01-80-01
DOC:        07-40-03
--------------------
2014-07-29 

     12:02

External calibration
Start: manually
Set   +   50.000 g
Dev   -    0.002 g
External adjustment
Dev        0.000 g
Temp  +     23.7  

°

C

--------------------
Name:

--------------------

Calibration Report

MA performance test
Weighing system adjustment

Summary of Contents for MA37

Page 1: ...Operating Instructions Sartorius Moisture Analyzer Model MA37 Electronic Moisture Analyzer 98648 019 93 98648 019 93 ...

Page 2: ...g the Settings 26 List of Available Settings 27 Moisture Analysis 33 Viewing and Changing Method Parameters 33 Performing the Moisture Analysis 35 MA Performance Test 39 Starting the Performance Test 39 Performance Test Measurement Not Successfully Completed 41 Performance Test Successfully Completed 41 Calibration and Adjustment 42 Viewing the Calibration Report 44 Weighing 45 ISO GLP compliant P...

Page 3: ...anation of Symbols The following symbols are used in this manual Useful information and tips Hot surface Warning Risk of severe burns Note regarding device operation When individual buttons are displayed they should be pressed The following symbols are used in these instructions t Indicates a required action y Describes what happens after you have performed a particular step Perform steps in the s...

Page 4: ...tmospheres Materials liable to catch fire or explode may not be used as samples for moisture analysis Before initial startup ensure that the voltage rating printed on the manufacturer s ID label of the analyzer matches the voltage of the local AC power Installation Instructions Danger of severe personal injury or property damage due to faulty analyzer components Do not operate the analyzer if the ...

Page 5: ...pes of samples use a drying temperature that is low enough to prevent a fire or explosion from occurring If in doubt carry out a careful risk analysis Wear safety glasses Always work with small sample quantities Never leave the analyzer unattended in these cases No modifications are permitted to the analyzer Symbols Used on the Device When setting up the moisture analyzer leave enough space to pre...

Page 6: ...tances escaping under high pressure Safety Gloves Wear suitable safety gloves when handling chemicals or hazardous substances Check that the gloves are not worn and do not have any holes or tears before putting them on Intended Use The moisture analyzer can be used for quick and reliable determination of the moisture content of materials of liquid pasty and solid substances using the thermogravime...

Page 7: ... module 2 Heating element 3 Disposable sample pan 4 Pan support 5 Sample chamber bottom 6 Locking socket bayonet 7 Process status light 8 Unlocking handle for heating module 9 Power socket for country specific power cable 10 Fastening point for an optional Kensington key lock 11 Leveling feet 12 USB port for mini AB 13 Display and control unit touch screen 14 Temperature sensor ...

Page 8: ...location guarantees accuracy and reliability Ensure that the following ambient conditions are met Set up the analyzer on a stable even surface that is not exposed to vibrations e g weighing stone Maintain free access to the analyzer at all times Make sure to choose a place where excessive heat cannot build up Leave enough space between it and materials that are affected by heat Choose a location t...

Page 9: ...assembled at the factory Compensating for Unevenness of the Setup Surface t Twist the leveling feet until any slight unevenness in the setup surface is rectified and the analyzer is stable Anti theft Locking Device To protect against theft the analyzer has a fastening point for a security lock if required t A Kensington key lock can be installed at the fastening point on the back of the analyzer i...

Page 10: ...please inform the nearest Sartorius representative or your dealer The power must be connected in accordance with the regulations applicable in your country In order to connect the equipment to the power supply protection class 1 use a correctly installed wall outlet with a protective grounding conductor PE and a fuse of a maximum 16 A The power plug or another suitable disconnecting device for the...

Page 11: ... installed and used in accordance with the instructions may cause harmful interference to radio communications However there is no guarantee that interference will not occur in a particular installation If this equipment does cause harmful interference to radio or television reception which can be determined by turning the equipment off and on the user is encouraged to try to correct the interfere...

Page 12: ...isture Analyzer MA37 Transporting the Analyzer Moving the Analyzer in the Lab Avoid shocks and vibrations t Never lift and carry the analyzer by its heating module t Hold the analyzer under the housing lift it up carefully and carry it to its new location ...

Page 13: ...istered during the drying routine These methods include oven drying infrared drying and microwave drying All three of these methods are thermogravimetric When deductive methods are used the moisture content is indirectly determined A physical property related to the moisture in the substance is measured e g conductivity These methods include capacitive and spectroscopic processes Thermogravimetry ...

Page 14: ...s may be used that generate heat The heat generated may result in a loss of moisture prior to the measurement Perform initial analysis of a new substance to test how the IR rays are absorbed by the sample and converted into heat A printout of the intermediate values of the drying process provides information on this at an early stage Due to the fact that the supply of IR rays results in intensive ...

Page 15: ...iterion for example with a different loss rate per 24 s Change the switch off criterion if required Increase end point recognition Set the parameter to 2 mg 24 s or 1 mg 24 s Decrease end point recognition Set the parameter to 10 mg 24 s or 20 mg 24 s Preparing the Sample Select a sample t t Select a representative part of the whole substance as a sample Choose a representative number of individua...

Page 16: ... for grinding the sample Use a disposable sample pan t t Use only Sartorius disposable sample pans inner diameter of 90 mm Reusing sample pans leads to poor repeatability of results After cleaning sample residues can still remain on the pan Residues from cleaning agents can evaporate during the next moisture analysis Scratches and grooves made during cleaning result in damage that forms points of ...

Page 17: ...o not reflect Considerably more convenient than the sea sand method When drying samples containing sugar a crust or skin can form and seal the surface A glass fiber filter is particularly useful in such cases The moisture can evaporate downwards through the surface of the filter Crust skin formation can be prevented or limited by placing the glass fiber filter on top of the sample t t Cover solid ...

Page 18: ... for applying a sample to the analyzer not as a starting condition can be entered by the user The tolerance range can be freely selected e g 0 5 g Print Lines When print lines are activated 1 or 2 lines with 20 characters each additional information about the method entered by the user appears on the report and printout Filter The user has the option of selecting between 0 1 or 2 filters During ta...

Page 19: ... The analysis ends as soon as the weight loss per the set interval is lower than a user defined threshold set in milligrams The weight loss is entered by the user Semi automatic percentage The analysis ends as soon as the weight loss in percent is lower than a user defined threshold set in percent The percentage is entered by the user Time The analysis ends as soon as the specified time has elapse...

Page 20: ...o standby select the menu key at the bottom left of the main screen on the display y y The menu is displayed t t Select the j button in the menu y y The moisture analyzer switches to standby mode t t To switch the moisture analyzer on again Select j on the display The moisture analyzer starts in the method most recently used before the analyzer was last switched off Moisture in M Start new measure...

Page 21: ...y y The Settings window appears t t Select Language or the top entry in the list y y The Language settings window appears t t Select the desired language such as Deutsch German t t Select l to confirm y y The display changes directly to the desired language t t Select o to return to the menu Moisture in M Standard drying 105 C Standby temperature Initial weight End Fully automatic Target value No ...

Page 22: ... such as ballpoint pens can damage the device The touch screen should only be operated by lightly pressing it using the tips of your fingers You can also operate the touch screen when wearing lab gloves Moisture in M Start new measurement Standard End autom 105 C Wednesday 2014 01 08 16 50 5 1 2 3 4 1 Current date and time 2 Selected result display for the method 3 Operate method such as start moi...

Page 23: ...lect the menu key at the bottom left of the display y y The menu opens Moisture in M Standard drying 105 C Standby temperature Initial weight End Fully automatic Target value No automatic printout 1 3 5 4 2 1 Method with current parameters 2 Back to the main screen 3 Setup menu Open system settings see page 26 4 Change method parameters 5 Switch moisture analyzer to standby mode ...

Page 24: ... l Entering Text and Characters A keyboard will appear when you have to enter text and characters t t Select the individual characters one after the other The entered text appears at the top of the display If you hold down a character for longer the special versions of that character umlauts accent marks and special characters appear t t Use the Shift key to switch the keyboard display between upp...

Page 25: ...er on the display and drag it slowly either up or down y y The entries on the display move in the corresponding direction While you are scrolling a gray scroll bar appears on the right of the display indicating where you are in the list of options t t Tap the desired entry to select it Settings Signals Date and time Device information Calibration Adjustment Printout Settings Signals Calibration Ad...

Page 26: ...ce information Calibration Adjustment Printout y The Settings menu appears Settings Signals Date and time Device information Calibration Adjustment Printout t To scroll place your finger on the display and drag it slowly either up or down y The entries on the display move in the corresponding direction While you are scrolling a gray scroll bar appears on the right of the display indicating where y...

Page 27: ...format can be set here Under Date t To set the date select t enter the current date and confirm with l Under Date format t Select how the date is displayed and printed out DD MMM YYYY The date is displayed in the order of day month then year MMM DD YYYY The date is displayed in the order of month day then year YYYY MM DD ISO The date is displayed in the order of year month then day The time is alw...

Page 28: ...ports are saved per day Calibration reports that are at least 30 days old are deleted Printout You can configure the settings for printing and data output here Some of the settings depend on the configuration of the USB interface see Chapter USB Interface on page 30 Under Printout measurement t Select the settings for printing out the results on the connected lab printer Printout measurement The p...

Page 29: ...ce ID Batch ID function Sample ID function The identifiers for the printout can be defined here The Device ID identifier is entered here once The device ID can be a maximum of 14 characters long The Batch ID and Sample ID functions can be activated here The user must then enter the batch and sample IDs before each measurement routine Batch and sample IDs cannot exceed 20 characters Under Device ID...

Page 30: ...xt format Off Under Device Protocol t Select the data format for the transfer to the PC PC SBI Driver for PC required CDC Virtual Com Port The data is sent via SBI protocol using a virtual serial interface Additional information can be found in Chapter USB Interface section Direct Transfer of Data PC PC spreadsheet format The analyzer transmits the data via keyboard command keyboard emulation to t...

Page 31: ...e Protocol t Select the desired setting for the connection to the printer YDP30 YDP40 The connected printer is detected automatically and the connection is established Off The connection to the printer is deactivated 3 Connection to a Serial Printer or Another External Serial Device via a 9 pin Serial Interface USB Mini A to RS 232 Under Device Protocol t Select the desired setting for the connect...

Page 32: ...access Access code xxxxxx This function is used by the Sartorius Service Center and can only be accessed by authorized service technicians Reset All settings can be reset to the factory settings here t When the security prompt appears select Yes reset and confirm with l The moisture analyzer is reset and restarts ...

Page 33: ...death These samples must only be dried in a laboratory hood Corrosion due to aggressive vapors Substances that emit aggressive vapors when heated may cause condensation to form on cooler housing parts and lead to corrosion Use small sample quantities of these substances Viewing and Changing Method Parameters Moisture in M Start new measurement Standard Fully automatic 105 C Wednesday 2014 01 08 16...

Page 34: ... Moisture in M Target value Off y The current method parameters are displayed Customize parameters Heating program End Initial weight Result display Standard drying 105 C Fully automatic Off Moisture in M Target value Off t Select the parameter you wish to change such as Heating program Heating program Type Temperature C 110 85 125 Gentle drying Standard drying t Set the parameters to suit your re...

Page 35: ...s Moisture in M Start new measurement Standard Fully automatic 105 C Wednesday 2014 01 08 16 50 When all parameters have been set to suit your requirements you can start the moisture analysis Observe the following instructions in order to ensure successful measurement Wear gloves for each measurement so that the liquid in the sample is not influenced by handling Remove the sample directly from the...

Page 36: ...t Open the hood Fill in sample and close hood to start 0 000 g t Place the sample on the sample pan or filter s Fill in sample 1 929 g 2 000 y If you have activated the Initial weight option in the method parameters a target value display appears t Add the sample to the sample pan slowly When the sample quantity reaches the preset range the target value display turns green Close hood to start 1 92...

Page 37: ...ncel the moisture analysis before it is finished Select y When the moisture analysis is finished the moisture content of the sample is shown on the display The process status light on the analyzer flashes three times and then goes out 67 53 M Standard Fully automatic 110 C 11 18 min Measurement completed i OK New n 67 50 M If a target value is set the moisture content is displayed as a bar diagram...

Page 38: ...an analysis report can be found in Chapter ISO GLP compliant Printout Removing a Sample Danger of burns due to hot sample pan The sample and sample pan may be very hot Do not touch the sample pan Use sample tongs accessory to remove the sample Remove sample Remove old sample from sample chamber y When you have exited the measurement by selecting OK you can remove the sample from the moisture analy...

Page 39: ...tem adjustment Calibration report t Select MA performance test y The display switches to a view with three heating temperatures Please ensure that the device has not been heated for at least one hour before a performance test is carried out MA performance test The device is too warm for a performance test The device is still cooling down m t Select m to confirm the message and start the performanc...

Page 40: ...Easy pad accessory and remove the pad t Remove the protective wrapping t Affix the pad to the center of the sample pan sticky side down Fill in reference sample and close hood to start 2 513 g t Place the ReproEasy pad reference sample accessory on the sample pan Close hood to start 6 721 g t Close the hood y The performance test starts automatically During the performance test the process status ...

Page 41: ...ay switches back to the menu If a fault has been detected MA performance test Device is not OK 5 MApi 10 MApi Temperature 70 C Please contact Sartorius service a y The message Device is not OK appears t Select m to confirm Contact Sartorius service if the message Device is not OK appears Performance Test Successfully Completed a l MA performance test Device is OK Result 10 MApi Temperature 70 C 3 ...

Page 42: ...tically adjusted When and How Often The moisture analyzer must be calibrated and adjusted for example When the ambient conditions have changed temperature humidity or air pressure When the moisture analyzer is set up in a different location or moved in its current location An external calibration weight is required for calibration and adjustment 100 g Please note the tolerance of the calibration w...

Page 43: ...y please zero the integrated balance y A message appears on the display prompting you to place the calibration weight 50 g on the analyzer t Place the calibration weight on the pan support y Calibration starts automatically When calibration is complete a report appears on the display The report gives the deviation detected during calibration You are asked whether the weighing system should be adju...

Page 44: ...for the MA performance tests or weighing system adjustments and then access the most recent calibration reports which are sorted by date Up to 99 entries per day are saved Calibration reports older than 30 days are deleted y Menu Calibration report Example of a Calibration Report 2014 07 29 12 02 Sartorius Mod MA37 1 SerNo 0031710609 BAC 00 53 01 APC 01 80 01 DOC 07 40 03 2014 07 29 12 02 External...

Page 45: ... information Calibration Adjustment Printout y The Settings menu appears Calibration Adjustment MA performance test Weighing system adjustment Calibration report t Go to Calibration Adjustment and select Weighing system adjustment t Select Weighing only 0 000 END Weighing only g y The weighing screen appears You can now use the moisture analyzer as a simple lab balance t To exit the weighing funct...

Page 46: ... number Software version number of the device BAC Software version number of the display APC Software version number of the heating module DOC Device ID with max 14 characters if activated under system settings GLP footer Field for signature Configuration To print out the ISO GLP report define the following system settings see Chapter System Settings section Printout t Activate ISO GLP compliant p...

Page 47: ... MA37 1 SerNo 0000037919 BAC 00 53 01 APC 01 80 01 DOC 07 40 03 Type Standard drying Temperature 40 C Standby Off Initial weight Off End Fully automatic Result display Moisture in M Target value Off No of filters 0 Start time 10 03 Start weight 4 564 g Measurement time 01 15 min Result 8 16 M Final weight 4 531 g End of analysis Name ...

Page 48: ...er YDP30 YDP40 Off Type A Mini A Type B Mini A RS 232 9 pin Sartorius order no YCC04 D09 Sartorius order no YCC03 D09 USB Host Master 1 2 3 USB Device Slave Serial device with 9 pin SUB D plug Printer equipment supplied Direct Transfer of Data PC Requirements PC with Windows 7 Windows 8 Vista Windows XP or 2000 operating system A to Mini B USB connection cable from PC to moisture analyzer Sartoriu...

Page 49: ...ure analyzer go to USB port and select Device Protocol Setting Options t To change the moisture analyzer to suit your PC settings define the following system settings you can find more information on this in Chapter System Settings USB Interface Choose the character to be used as a decimal point for the spreadsheet calculation Set the PC keyboard to English USA instead of Universal numbers lock on...

Page 50: ...uctions Moisture Analyzer MA37 When PC text format is set on the moisture analyzer e g with Microsoft Excel open t Activate the cursor in the PC application t Then select a or n on the moisture analyzer for the respective data output ...

Page 51: ...nect the peripheral device to the moisture analyzer using the Sartorius YCC03 D09 connection cable RS 232 9 pin PC compliant assignment t Define the desired settings See Chapter System Settings section USB Interface Interface Specification Data Output The print command can be triggered by selecting a Data Output Formats Values are always output with an ID if more than 22 parameters are set the val...

Page 52: ...elected use four characters to print out the units because no space is printed before a unit In a print interval however one line is generated with the following Five characters for a header One character for a space Nine characters for the values including signs One space Four characters for the units 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 N _ _ _ _ _ _ _ _ _ 6 7 8 7 _ g _ _ CR ...

Page 53: ...errors only relevant functions keys are displayed depending on the situation This prevents most operating errors from occurring The following buttons are only available in specific circumstances A Only if there is a measured value in the zero setting range before external calibration adjustment D Only if there is a measured value larger or smaller than zero Error Messages during Operation Value is...

Page 54: ...elected temperature is too high and the sample is oxidized sample is boiling or burning and the splashes are continuously changing the weight Reduce drying temperature Lay glass fiber filter onto the sample Reduce the sample quantity or apply the sample more evenly Select a semi automatic switch off criterion or select timer mode Measurement time too long Increase temperature Reduce sample quantit...

Page 55: ...kaging from the Sartorius Service Center if necessary Avoid shocks and vibrations Prior to shipping switch the analyzer to standby mode see page 20 and then pull the plug t Remove the following parts from the analyzer Disposable sample pan Pan support t Place the analyzer in one side of the packaging t Place the other side of the packaging over the analyzer ...

Page 56: ...56 Shipping the Analyzer Operating Instructions Moisture Analyzer MA37 t Then put the packaged analyzer into the cardboard box and seal the box ...

Page 57: ...ius dealer to arrange for proper repairs Cleaning the Analyzer Cleaning the Control Panel Switch the display to standby mode to avoid modifying the settings for operation during cleaning t Select the menu key to switch to the method menu t If you then select j the display is switched off t To switch the display back on Select j at the bottom left of the display The moisture analyzer starts in the ...

Page 58: ...ing the Heating Module Danger of Burns The inner part of the heating module and parts of the sample chamber may be extremely hot Wait until the heating module has cooled completely Avoid touching the heating element To remove spray residues or deposits from the heating element use a weak solvent such as ethanol Unlocking the Heating Module 1 Open the heating module all the way 2 Pull the unlocking...

Page 59: ...washer 6 Once cleaning is complete reassemble the heating module and reinstall in the analyzer following the instructions in reverse order The heating module must snap into place on the analyzer Cleaning the Bottom of the Sample Chamber Danger of Burns Parts of the sample chamber may be extremely hot Wait until the bottom of the sample chamber has cooled completely Removing the Sample Chamber Bott...

Page 60: ...er MA37 2 Remove the Locking socket bayonet as in general view and sample chamber bottom from the analyzer and clean in a dishwasher 3 After cleaning fix the sample chamber bottom into place again on the analyzer using the Locking socket bayonet as in general view ...

Page 61: ...ispose of it separately from other unsorted municipal waste with the aim of recycling it For more information regarding disposal and recycling please contact our local service representatives Our partners listed on the following website will also be able to provide assistance within the EU 1 Go to http www sartorius com de 2 Select the Service menu item 3 Then select Information on Disposal 4 Addr...

Page 62: ...on 10 50 60 Hz Protection class and standards Protection class I as per EN 61010 1 IEC 61010 1 up to 3000 m above sea level IP20 as per EN 60529 IEC 60529 Power supply Using country specific power cable from Sartorius only Power consumption Max 640 W typically Ambient Conditions The specifications are valid for the following ambient conditions Environment For indoor use only Ambient temperature 10...

Page 63: ...fatty samples soft quality 200 pcs d 90 mm 6906941 External adjustment weight 50 g OIML class E2 with DKD certificate YCW452 AC 02 Tweezers 69MA0072 Printers and Communication Premium GLP lab printer Printer paper for GLP lab printer paper Continuous labels for GLP lab printer YDP30 69Y03285 69Y03286 Data cable for Mini USB USB A YCC04 D09 Data cable for Mini USB 9 pin RS 232 YCC03 D09 Spare Parts...

Page 64: ...64 Analyzer Dimensions Operating Instructions Moisture Analyzer MA37 Analyzer Dimensions MA37 All dimensions are given in millimeters ...

Page 65: ...65 Declaration of Conformity Operating Instructions Moisture Analyzer MA37 Declaration of Conformity ...

Page 66: ...66 Certificate of Compliance Operating Instructions Moisture Analyzer MA37 Certificate of Compliance ...

Page 67: ...67 Certificate of Compliance Operating Instructions Moisture Analyzer MA37 ...

Page 68: ...68 Operating Instructions Moisture Analyzer MA37 Certificate of Compliance ...

Page 69: ... Sartorius All rights reserved by Sartorius in accordance with copyright law The information and figures contained in these instructions correspond to the version date specified below Sartorius reserves the right to make changes to the technology features specifications and design of the equipment without notice Status October 2014 Sartorius Lab Instruments GmbH Co KG Goettingen Printed in the EU ...

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