Labconco CentriVap 74600-00 User Manual Download Page 15

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Product Service Domestic 1-800-522-7658, International 816-333-8811

Chapter 3: Getting Started

Catalog #

Product Description

78100-00

CentriVap Concentrator – 115V

78100-10

CentriVap Concentrator – 230V

78100-02

CentriVap Concentrator with Heat Boost – 115V

78100-03

CentriVap Concentrator with Heat Boost – 230V

Plus the Following:
Part #

Component Description

74614-00 User’s

Manual

13345-00

13341-00

Power Cord – 115V

Power Cord – 230V

78286-06 Tubing
14888-00 Clamp

(2)

Catalog #

Product Description

78110-00

CentriVap Cold Trap – 115V

78110-01

CentriVap Cold Trap – 230V

Plus the Following:
Part #

Component Description

74614-00 User’s

Manual

13345-00

13341-00

Power Cord – 115V

Power Cord – 230V

74646-00 Wire

Assembly

78286-06 Tubing
14888-00 Clamp

(2)

79814-00

Insulation – Cover

78735-00 Cover

Assembly

Catalog #

Product Description

74600-00

CentriVap Cold Trap – 115V

74600-01

CentriVap Cold Trap – 230V

Plus the Following:
Part #

Component Description

74614-00 User’s

Manual

13345-00

13341-00

Power Cord – 115V

Power Cord – 230V

74646-00 Wire

Assembly

78286-06 Tubing
14888-00 Clamp

(2)

79814-00

Insulation – Cover

78735-00 Cover

Assembly

Concentrator

Cold Trap

Summary of Contents for CentriVap 74600-00

Page 1: ...40 00 79840 01 74750 00 74750 01 User s Manual LABCONCO CORPORATION 8811 PROSPECT AVENUE KANSAS CITY MO 64132 2696 800 821 5525 816 333 8811 FAX 816 363 0130 E MAIL labconco labconco com HOME PAGE www...

Page 2: ...aler who sold you the product If the cause is determined to be a manufacturing fault the dealer or Labconco Corporation will repair or replace all defective parts to restore the unit to operation Unde...

Page 3: ...ep 8 CHAPTER 3 GETTING STARTED 9 Unpacking Your CentriVap 10 CentriVap Components 10 Setting Up Your CentriVap 13 Emergency Access Into the Chamber 13 Component Orientation Hose Connections 13 Exhaust...

Page 4: ...talling a Secondary Chemical Trap 30 Installing a CentriZap Strobe Light 32 Installing a Glass Trap in the Cold Trap 33 CHAPTER 7 TROUBLESHOOTING 35 APPENDIX A CENTRIVAP COMPONENTS 39 APPENDIX B CENTR...

Page 5: ...small as a few microliters The Concentrator is equipped with a 300 watt heater to speed evaporation by warming the chamber during processing A timed outlet for the vacuum pump connection delays the st...

Page 6: ...nance and making minor modifications to your CentriVap are also included Chapter 1 Introduction provides a brief overview of the CentriVap explains the organization of the manual and defines the typog...

Page 7: ...s of all of the accessories available for your CentriVap Typographical Conventions Recognizing the following typographical conventions will help you understand and use this manual Book chapter and sec...

Page 8: ...ll your CentriVap and make all of the necessary connections For information on the operational characteristics of your CentriVap go to Chapter 4 Using Your CentriVap If your CentriVap is installed and...

Page 9: ...and of solid construction In addition an exhaust means must be provided An electrical source must be located near the installation site Carefully read this chapter to learn the electrical supply requi...

Page 10: ...require an 8 Amp circuit breaker or fuse rated at 230V 50 60 Hz 115V models are equipped with a 15 Amp NEMA 5 15P plug 230V models are not equipped with a plug It will be necessary to install a plug...

Page 11: ...um pumps used with 115V models should be equipped with a 115V 15 Amp NEMA 5 15P plug Vacuum pumps used with 230V models should be equipped with a reverse IEC 320 plug This will allow the vacuum pump t...

Page 12: ...al components within the CentriVap are made from stainless steel or aluminum and can be degraded if exposed to acids Before evaporating acids be sure to contact Labconco A moisture trap solvent trap a...

Page 13: ...ctrical supply source to your CentriVap properly exhaust your CentriVap safely use solvents with your CentriVap The CentriVap Concentrator weighs over 42 lbs 19 Kg The carton allows for lifting with a...

Page 14: ...P WAS DAMAGED IN TRANSIT YOU MUST FILE A CLAIM DIRECTLY WITH THE FREIGHT CARRIER LABCONCO CORPORATION AND ITS DEALERS ARE NOT RESPONSIBLE FOR SHIPPING DAMAGE Do not discard the carton or packing mater...

Page 15: ...g Product Description 78110 00 CentriVap Cold Trap 115V 78110 01 CentriVap Cold Trap 230V Plus the Following Part Component Description 74614 00 User s Manual 13345 00 13341 00 Power Cord 115V or Powe...

Page 16: ...tem 115V 79830 01 Acid System 230V Plus the Following Part Component Description 78100 00 78100 01 CentriVap Concentrator 115V or CentriVap Concentrator 230V 78110 00 78110 01 CentriVap Cold Trap 115V...

Page 17: ...power disruption If it is necessary to open the lid when there is no electrical power connected to the CentriVap insert a small screwdriver or similar instrument into the small round hole on the left...

Page 18: ...ttach the other end of this hose to one of the barb fittings on the Cold Trap Cover Assembly Clamp securely with the clamps supplied Attach another hose to the remaining barb fitting on the Cold Trap...

Page 19: ...ceptacle on the back of the CentriVap Concentrator and plug the other end into a suitable power receptacle Plug the power cord into the receptacle on the back of the CentriVap Cold Trap and plug the o...

Page 20: ...ld be used in a prudent manner using good laboratory practices It has been designed for use with compounds as described in the United States National Electrical Code Class I Group D The heater may be...

Page 21: ...zardous solvents within 12 inches 300 mm of the CentriVap Several components of the CentriVap which are located inside the chamber are made of stainless steel which can be attacked by acids Use of aci...

Page 22: ...to load and operate your CentriVap proceed to Chapter 4 Using Your CentriVap To make a modification to the configuration of your CentriVap proceed to Chapter 6 Modifying your CentriVap To perform addi...

Page 23: ...chapter to learn how to set operating parameters operate the controls properly select and position glassware inside your CentriVap understand the display interrupt a cycle after it has begun Do not u...

Page 24: ...uld be filled no more than approximately half full Select the size of the sample tube so it is compatible with the rotor and the desired sample size Tubes should not be loose in the rotor Rotors are a...

Page 25: ...r off prior to stopping the entire system enter a set time into the memory at the HEATER TIME When the programmed time expires the heater will turn off but the rotation and vacuum will continue until...

Page 26: ...ton 3 Run Stop Button Used to start or stop a run 4 Preheat Button Used to turn on the heater to preheat the chamber prior to loading samples 5 Increase Button When pressed the last selected set point...

Page 27: ...essed Select existing program Operating parameters can be stored in memory so protocols can be repeated Nine programs can be stored To select a program press the set point SELECT button until arrows p...

Page 28: ...y without alarming at the end of a time period press the increase button until the display says ON The last entered set point is stored in memory If during a run the STOP button is pressed the timers...

Page 29: ...STOP in the display changes to R RUN The program on the display alternately displays R or the number of the program that is running If you intend to run program 1 2 or 3 simply press PROG 1 PROG 2 or...

Page 30: ...urned on the CentriVap returns to the same mode RUN or STOP that it was in when the power was turned off If the CentriVap was in the RUN mode when the power was turned off when the power is turned on...

Page 31: ...nge or chamois and a mild non abrasive soap or detergent 3 Check oil level of the vacuum pump if applicable It should be between MIN and MAX If the oil level is less than an inch 25 4 mm above MIN add...

Page 32: ...eventually deteriorate and require replacement The effective life of rubber parts depends upon both their usage and the surrounding environment Check all rubber hoses and gaskets and replace any that...

Page 33: ...ain added chemical resistance You may wish to add a secondary trap to trap vapors exhausted from the vacuum pump To observe the samples while they are processing an optional strobe light may be instal...

Page 34: ...s Attach the bracket to the side of the Cold Trap housing using the screws provided Attach the hose from the Cold Trap Lid Assembly to the out connector of the canister housing Connect another hose fr...

Page 35: ...tridge is used to trap radioactive waste When the media in the insert has changed color discard the insert and replace it with a new insert For the radiochemical trap insert no color indicator exists...

Page 36: ...rovided Plug the connector on the strobe light harness into the receptacle on the back of the CentriVap marked STROBE OUTLET Peel the protective backing off the enclosed Velcro and attach it to the ba...

Page 37: ...on the center tube of the Glass Trap and clamp securely Attach the hose from the vacuum pump or Secondary Trap to the other barb fitting on the Glass Trap and clamp securely Place the Glass Trap insid...

Page 38: ...hen problems are sensed by the internal self check routine DISPLAY ERROR CODE CAUSE CORRECTIVE ACTION HEAT SENSOR Sensor failure Replace sensor assembly Connection failure Repair connection CLOSE LID...

Page 39: ...od Evaporation rate is reduced Heater inoperable Contact Labconco Vacuum pump failure Check pump Obstruction in hose Remove obstruction or replace hose Lack of adequate vacuum See below No vacuum poor...

Page 40: ...ected Cold Trap is not ON Check to make sure switch is ON and condensing unit fan is moving air out of the rear of the cabinet Cold Trap does not cool down Turn vacuum pump OFF and allow Cold Trap to...

Page 41: ...A AP PP PE EN ND DI IX X A A C CE EN NT TR RI IV VA AP P C CO OM MP PO ON NE EN NT TS S The following pages list components that are available for your CentriVap The parts shown are the most common r...

Page 42: ...Temp Speed Sensor 8 1 7479400 PCB 9 1 1289200 Relay Vacuum Pump 115V 9A 1 1289100 Relay Vacuum Pump 230V 10 1 7826000 Switch Latch 11 1 7478700 Solenoid Latch 12 1 7403701 Display 13 1 7455300 Label...

Page 43: ...41 Product Service Domestic 1 800 522 7658 International 816 333 8811 Appendix A CentriVap Components...

Page 44: ...Ground 8 1 1360500 Valve 9 1 7873500 Cover Assembly 10 2 1548603 Stem Adapter 11 2 1544501 Elbow 12 2 1548101 Stem 13 1 7981400 Insulation Lid Assembly 13A 1 7873200 Insulation Glass Trap 14 1 787150...

Page 45: ...43 Product Service Domestic 1 800 522 7658 International 816 333 8811 Appendix A CentriVap Components...

Page 46: ...imer 230V 7 1 7474500 Switch Pressure 8 1 1360500 Valve 9 1 7464600 Wire Assembly Ground 10 1 7873500 Cover Assembly 11 2 1548603 Stem Adapter 12 2 1544501 Elbow 13 2 1584101 Stem 14 1 7981400 Insulat...

Page 47: ...45 Product Service Domestic 1 800 522 7658 International 816 333 8811 Appendix A CentriVap Components...

Page 48: ...47 Product Service Domestic 1 800 522 7658 International 816 333 8811 A AP PP PE EN ND DI IX X B B C CE EN NT TR RI IV VA AP P D DI IM ME EN NS SI IO ON NS S CentriVap Concentrator...

Page 49: ...48 Product Service Domestic 1 800 522 7658 International 816 333 8811 Appendix B CentriVap Dimensions CentriVap Cold Trap 55 C Models 78110 00 78110 01...

Page 50: ...49 Product Service Domestic 1 800 522 7658 International 816 333 8811 Appendix B CentriVap Dimensions CentriVap Cold Trap 100 C Model 74600 00 74600 01...

Page 51: ...8100 00 excluding vacuum pump 3 1A Nominal amperage for 230V CentriVap Concentrator model 78100 01 excluding vacuum pump 1 6A Nominal amperage for 115V CentriVap Concentrator model 78100 02 excluding...

Page 52: ...y at 104 F 40 C Main supply voltage fluctuations not to exceed 10 of the nominal voltage Transient overvoltages according to Installation Categories II Overvoltage Categories per IEC 1010 Temporary vo...

Page 53: ...53 Product Service Domestic 1 800 522 7658 International 816 333 8811 Appendix C CentriVap Specifications Wiring Diagram Concentrator 115V Model...

Page 54: ...54 Product Service Domestic 1 800 522 7658 International 816 333 8811 Appendix C CentriVap Specifications Wiring Diagram Concentrator 230V Model...

Page 55: ...55 Product Service Domestic 1 800 522 7658 International 816 333 8811 Appendix C CentriVap Specifications Wiring Diagram Cold Trap 115V 230V Models Models 78110 00 78110 01...

Page 56: ...56 Product Service Domestic 1 800 522 7658 International 816 333 8811 Appendix C CentriVap Specifications Wiring Diagram Cold Trap 115V 230V Models Models 74600 00 74600 01...

Page 57: ...5 18 10 100 on Diaphragm 34 no 5 29 Acetonitrile bp 82 50 12 25 45 off Diaphragm 184 no 1 63 50 12 25 45 on Diaphragm 181 no 1 66 50 12 25 100 off Diaphragm 81 no 3 70 50 12 25 100 on Diaphragm 77 no...

Page 58: ...off Diaphragm 196 no 0 67 1 5 132 1 100 off Diaphragm 117 no 1 13 1 5 132 1 100 on Diaphragm 108 no 1 22 50 12 25 45 off rotary vane 1002 yes 0 30 50 12 25 100 off rotary vane 424 yes 0 70 50 12 25 1...

Page 59: ...A Holds 72 0 5 ml microcentrifuge tubes and 60 1 5 ml microcentrifuge tubes or 60 2 0 ml microcentrifuge tubes 74507 00 Rotor 1 5 ml Holds 132 1 5 ml microcentrifuge tubes or 132 2 0 ml microcentrifug...

Page 60: ...5 ml microcentrifuge tubes or 32 2 0 ml microcentrifuge tubes and 12 28 x 115 mm conical tubes or 12 28 x 135 mm conical tubes or 12 28 x 140 mm conical tubes 74619 00 Rotor 96 well plate Holds 4 Stan...

Page 61: ...single phase 2 4 amp operation 77394 03 Direct Drive Vacuum Pump 195 liters minute Same as 14677 00 except 220 208 230 VAC 50 60 Hz single phase 4 0 amp operation 79141 00 Diaphragm Vacuum Pump Corros...

Page 62: ...agm Vacuum Pump Corrosion resistant explosion proof motor 29 in Hg Vacuum 115V 60 Hz 5 8 amps single phase 88 liters minute 79249 01 Diaphragm Vacuum Pump Corrosion resistant explosion proof motor 29...

Page 63: ...63 Product Service Domestic 1 800 522 7658 International 816 333 8811...

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