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8-7
MAINTENANCE, PERIPHERALS
8.1.6
Burette Preparation (Filling with Titrant)
Before starting a titration, the burette must be properly filled with titrant in order to obtain an
accurate and repeatable result. To fill the burette, follow the next steps and recommenda-
tions:
• If necessary, clean the burette and make sure it is empty and dry.
• From the main screen press
.
• Highlight
Prime Burette option and press
.
• Enter the number of times the burette needs to be rinsed (minimum three rinses are
recommended allowing air bubbles to be evacuated).
• Press
.
• Insert the aspiration tube into the titrant bottle only when the piston is going down
and has reached about ¼ from the top.
To avoid the presence of air bubbles inside the burette, make sure to have continuous liquid
flow inside the burette and a little air just above the liquid level during the first filling is
normal. The next filling will evacuate all of the air, no air will be left in the valve.
Sometimes during this process, slight finger tapping on the tubes is helpful to remove any
residual air bubbles from the tubes.
Summary of Contents for HI 903
Page 1: ...1 QUICK START GUIDE HI 903 KARL FISCHER VOLUMETRIC TITRATOR Revision 1 0 ...
Page 4: ...4 QUICK START GUIDE ...
Page 7: ...7 QUICK START GUIDE TITRATOR CONNECTIONS Front View Rear View ...
Page 18: ...18 QUICK START GUIDE QS 903 02 11 ...
Page 19: ...1 INSTRUCTION MANUAL HI 903 KARL FISCHER VOLUMETRIC TITRATOR Revision 1 00 ...
Page 22: ......
Page 24: ...1 2 INTRODUCTION ...
Page 26: ...2 2 SETUP ...
Page 30: ...2 6 SETUP 2 3 2 Titrator Rear View 2 3 3 Titrator Left side View ...
Page 40: ...2 16 SETUP ...
Page 42: ...3 2 USER INTERFACE ...
Page 50: ......
Page 52: ...4 2 GENERAL OPTIONS ...
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Page 92: ......
Page 94: ...6 2 TITRA TITRA TITRA TITRA TITRATION TION TION TION TION ...
Page 106: ...6 14 TITRA TITRA TITRA TITRA TITRATION TION TION TION TION ...
Page 118: ...8 2 MAINTENANCE PERIPHERALS ...
Page 147: ...A1 1 APPENDIX 1 Appendix 1 Contents A1 TECHNICAL SPECIFICATIONS A1 3 ...
Page 148: ...A1 2 APPENDIX 1 ...
Page 152: ......
Page 155: ...A3 1 APPENDIX 3 Appendix 3 Accesories A3 TITRATOR COMPONENTS A3 3 ...
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Page 159: ...1 GENERAL APPLICATIONS BROCHURE HI 903 KARL FISCHER VOLUMETRIC TITRATOR Revision 1 00 ...
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Page 192: ...2 TITRATION THEORY ...
Page 194: ...4 TITRATION THEORY ...
Page 206: ...16 TITRATION THEORY A B Figure 8 Potential glass electrode mV C ...