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8-5
MAINTENANCE, PERIPHERALS
8.1.5
Cleaning the Burette
To clean the burette, follow these steps:
• If the burette is filled with titrant, remove the aspiration tube from the titrant bottle
and purge burette (
see Section 7.2.4, Purge Burette
).
• Insert the aspiration tube into the Karl Fischer solvent.
• Prime burette to fill the burette with solvent (use 2 rinses) (
see Section 7.2.1, Prime
Burette).
• During second refilling of the burette remove the aspiration tube from the solvent or
cleaning solution and allow the air to replace the liquid in the burette. This will clean
the aspiration tube.
If this simple cleaning procedure is not adequate, continue with these steps:
• Slide the burette out from the pump assembly.
• Remove the dispensing and aspiration tubes. Clean them separately or insert new
ones.
• Remove the protective cap from the bottom of the burette assembly by using the
special tool (HI900942).
• Remove the syringe from the burette assembly by unscrewing it with your fingers.
• Extract the piston from the syringe.
• Clean both the piston and the syringe with appropriate cleaning solution.
• Remove the excess liquid.
Summary of Contents for HI 903
Page 1: ...1 QUICK START GUIDE HI 903 KARL FISCHER VOLUMETRIC TITRATOR Revision 1 0 ...
Page 4: ...4 QUICK START GUIDE ...
Page 7: ...7 QUICK START GUIDE TITRATOR CONNECTIONS Front View Rear View ...
Page 18: ...18 QUICK START GUIDE QS 903 02 11 ...
Page 19: ...1 INSTRUCTION MANUAL HI 903 KARL FISCHER VOLUMETRIC TITRATOR Revision 1 00 ...
Page 22: ......
Page 24: ...1 2 INTRODUCTION ...
Page 26: ...2 2 SETUP ...
Page 30: ...2 6 SETUP 2 3 2 Titrator Rear View 2 3 3 Titrator Left side View ...
Page 40: ...2 16 SETUP ...
Page 42: ...3 2 USER INTERFACE ...
Page 50: ......
Page 52: ...4 2 GENERAL OPTIONS ...
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Page 92: ......
Page 94: ...6 2 TITRA TITRA TITRA TITRA TITRATION TION TION TION TION ...
Page 106: ...6 14 TITRA TITRA TITRA TITRA TITRATION TION TION TION TION ...
Page 118: ...8 2 MAINTENANCE PERIPHERALS ...
Page 147: ...A1 1 APPENDIX 1 Appendix 1 Contents A1 TECHNICAL SPECIFICATIONS A1 3 ...
Page 148: ...A1 2 APPENDIX 1 ...
Page 152: ......
Page 155: ...A3 1 APPENDIX 3 Appendix 3 Accesories A3 TITRATOR COMPONENTS A3 3 ...
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Page 159: ...1 GENERAL APPLICATIONS BROCHURE HI 903 KARL FISCHER VOLUMETRIC TITRATOR Revision 1 00 ...
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Page 192: ...2 TITRATION THEORY ...
Page 194: ...4 TITRATION THEORY ...
Page 206: ...16 TITRATION THEORY A B Figure 8 Potential glass electrode mV C ...