EYELA SD-1010 Instruction Manual Download Page 37

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2) Remove the evaporating tube from the main unit

evaporating tube installation part.

*Remove the outlet temperature sensor beforehand

from the sensor installation port on the branched
tube of the evaporating tube.

3) Disassemble and wash respective parts as

illustrated in the right figure.

*Use a neutral detergent to wash glass parts.

If they are dirty, immerse them in a neutral

detergent-diluted solution for about half a day
before washing them.

4) Assemble parts by reversing procedure.

Evaporating tube
mounting portion

Evaporator

Evaporating tube
receiving cradle

③

Pull out

②

Rotate

Rectification board

Evaporator

Cyclone

Separable seal packing

Packing (SC)

Connecting tube

Separable clamp (

75)

Code No.

Part name

Remarks

180370

Rectification board

180000

Evaporator

147840

Upper connection packing

146760

Collecting flask cap

199050

Lower connecting packing

146750

Separator, powder
collection container

116510

Separable clamp (

75)

180020

Connecting tube

116530

Separable seal packing

180010

Cyclone

180190

Packing (SC)

-32-

①

Loosen

Upper connecting packing

Powder collection container

Separator

Lower
connecting
packing

Collecting flask
Cap

Summary of Contents for SD-1010

Page 1: ...s designed to use this unit safely with the best performance Keep this instruction manual beside the unit Important Read carefully the chapter For safety operation before operating this unit SD 1010 Instruction Manual Spray Dryer Spray Dryer ...

Page 2: ... glass component used may get broken if mishandled potentially leading to an unexpected injury or accident We investigate enough possible hazards during the operation however it is very difficult for us to find every hazardous occasion Therefore this manual cannot describe all hazardous operations However if you carry out the handling method described in this manual you can operate and work more s...

Page 3: ... Be careful to use the unit referring warning messages When the warning label is worn and hardly show the message change it with a new one Please order us a new label Explosion Do not use this unit to dry any explosive materials such as organic solvent Warning Burning Do not touch evaporator or cyclone while drying samples Caution ...

Page 4: ...static electricity 13 5 1 6 Attaching silicone tubing 14 5 1 7 Connecting power cord 15 5 1 8 Connecting exhaust hose 15 5 1 9 Connecting air tubing 16 5 1 10 Connecting recorder cable 16 5 1 11 Replacing cap for nozzle 17 5 1 12 Installing agitator 18 5 2 Operation 5 2 1 Preparing sample and distilled water 19 5 2 2 Operation 20 5 2 3 Cleaning spray nozzle 24 5 2 4 Collection of fine powder 25 5 ...

Page 5: ...order 2m 3 12 Sensor for outlet temperature 1 13 Evaporator set 1 14 Cyclone set 1 15 Collection bottle set 2 16 Instruction Manual 1 17 Warranty 1 This unit is packed in 2 cartons which are main unit and accessory parts Check quantities referring to the below table P a c k i n g 2 Rectification board 3 Exhaust hose cuffs 4 Stainless steel diamond clamp 5 Air tube connector 6 Air tube 7 Stirring b...

Page 6: ...e pay attention to safety as this product becomes hot Warning Caution 1 Evaporator Cyclone In his unit samples are sprayed through a nozzle and dry by headed air to make dried fine particle Outline 2 Do not use flammable materials such as organic solvent Do not use this unit to dry flammable materials such as organic solvent This unit has a built in heater so it may ignite Dangerous 2 1 Applicatio...

Page 7: ...temp recorder output 0 10mV at50 250 C Drying air volume output 0 10mV at0 1m3 min Composition Heater 3kW Delivery pump Tube pump Spray nozzle Twin fluid nozzle nozzle hole diameter 0 71 mm in inside diameter Nozzle diameter changeable option Spray air pump Spray air compressor option Evaporating tube cyclone Powder collection container separator Hard glass Sample agitator motor magnet DC brushles...

Page 8: ...onnecting tube Duct Sensor for outlet temperature Protection cover Blower exhaust port Maintenance port Inside Inlet filter Caster Adjuster Maintenance port Inside Outlet filter Cooling fan for control part Cooling fan for main unit For cooling blower Air intake Outside air inlet Silicon tube Connection collar ...

Page 9: ...put terminals Operation lamp of over temperature protector Reset switch of over temperature protector Power switch Ground terminal Air connecting port Electrical leakage breaker Power cord Top face of operating portion Right side of operating portion Lower right side of housing 4 Operating panel Screw cover ...

Page 10: ...3 Temp control and blower operation lamp To control temperature It illuminates when the blower is in operation 14 SET key To determine setting values for temperature control and various parameters 15 UP key To change setting values for temperature control and various parameters 16 DOWN key To change setting values for temperature control and various parameters 17 Heater alarm lamp It illuminates w...

Page 11: ...rating lamp It illuminates when the stirrer operates 27 Stirring speed control dial To control stirring speed 28 Flow rate control knob To control the flow rate of sample 29 Flow rate lock lever To fix the flow rate of sample 27 26 29 28 6 ...

Page 12: ...ks the outdoor air inlet Clean the exit filter or replace it 7 Alarm function Alarm name Alarm operation Alarm cause Temp alarm Temp Alarm Temp alarm lamp illuminates Inlet temperature is 10 C or higher for 3 minutes or longer time Sensor alarm _ _ _ blinks on the temperature indicator of which sensor alarm occurs Sensor input value is abnormal Outlet temp upper limit alarm Outlet temperature blin...

Page 13: ...rials pyrotechnic materials nearby Ambient temperature between5and35 C The part where no condensation is Places with little humidity where water drops do not reach Places with little dust Places not exposed to direct sunlight Well ventilated place A level stable and robust place Keep good ventilation space The following space See the left figure from the ceiling surface ceiling etc is required as ...

Page 14: ...to the casters and damage the unit in this case lift it up to move it 3 Once the installation place is determined push down and lock the stopper levers of the casters 4 Adjust the level of adjusters 4 using a wrench to place the unit horizontally Float the casters from the ground by lifting up the unit to fixate the unit Caster with stopper Adjuster The unit goes down The unit goes up 9 Lock Stopp...

Page 15: ...ctly Warning Warning Warning 1 Check the voltage phase and capacity of power to which the product model is connected Power to which the product is connected is as follows 2 No power plug is supplied Directly connect to the distribution board Do not connect power yet here Connect the ground wire of the power cord to the ground Product model Power necessary for connection Power Capacity SD 1010 AC22...

Page 16: ...unit During installation you may put the evaporating tube temporarily on the evaporating tube receiving cradle of the main unit When insertion becomes heavy tight replace O ring inside the main unit 3 After insertion into the main unit rotate the evaporating tube leftward at 45º A click on the evaporating tube mounting portion is clutched and the evaporating tube is temporarily fastened on the mai...

Page 17: ... of outlet temperature sensor to the connector on the main unit 2 Slightly loosen the cap on the sensor mounting port of the evaporating tube and insert the outlet temperature sensor 3 Make adjustments so that the tip of the outlet temperature sensor is positioned in the branched tube center of the evaporating tube and then fasten the cap to fix the sensor Be careful not to touch the cable of the ...

Page 18: ...pacity is not enough use an optional powder collection container 1 2 L Cyclone Evaporator Cap screw Upper connection packing Powder collection container 13 Separator Code No Part name Remarks 146750 Powder collection container 600mL Standard accessory 147940 Powder collection container 1 2L 5 1 5 Countermeasures against static electricity When spraying and drying a sample vulnerable to electrifica...

Page 19: ...in Length reaching sample container Length reaching pressure sensor approx 100 mm Pull Pull Pressure sensor Spray nozzle Silicon tube ID3 7 x OD6 1 mm 14 Code No Part name Qty 125510 Silicon tube 3 15 x 5 2 5m 125530 Silicon tube 3 7 6 1 5m 2 Set silicon cut in an appropriate length on the delivery pump main and fix the tube retainer 3 Push down the lever of tube retainer and fixate the tube 4 Sli...

Page 20: ...f electrical shock Never connect a ground wire to the gas piping or water piping to prevent an incident of electrical shock Connect a ground wire correctly Warning Warning 15 5 1 8 Connecting exhaust hose 1 Attach cuffs at both ends of exhaust hose 2 Attach exhaust hose to the blower exhaust port and fix it with stainless steel diamond clamp 3 Put another side of exhaust hose into a draft chamber ...

Page 21: ...by PISCO When you remove the air piping tube pull out the tube while pushing the rim of connecting port Air connecting port Air piping tube Push the rim Pull out tube How to remove tube 16 5 1 10 Connecting recorder cable Connecting to the recorder allows you to record data on the inlet temperature outlet temperature and dry air volume 1 Connect the banana plug side of cable for recorder supplied ...

Page 22: ...ks 120730 Liquid cap hole diameterφ0 71 2 Slurry concentration approx 5 30 Standard accessory 120750 Gas cap hole diameter φ1 75 180270 Needle for liquid cap for hole diameter φ0 71 120720 Liquid cap hole diameter φ0 51 2A Slurry concentration approx 5 Powder grain size is greater than nominal size 1 120750 Gas cap hole diameter φ1 75 Standard accessory 180260 Needle for liquid cap for needle hole...

Page 23: ...e screw to secure the cover 3 Tighten the agitator installation pole on the pole installation screw 4 Mount the agitator drive on the agitator installation pole 5 Place the agitator operating portion on the upper part of the main See and follow the Installation Manual of the small agitator SPZ 2000 when using it Code No Part name Remarks 275200 Agitator installation pole 124560 ZC clamp 260530 Sma...

Page 24: ...ng left in the container A hot plate unit that can heat sample and keep it warm is made available as an option Pre heating of sample and maintenance of sample temperature during spray drying can prevent sample from crystallizing The use of the outside temperature sensor can control sample temperature A hot plate unit 220V can be custom made When some troubles occur stop operating immediately When ...

Page 25: ...e screw head of the protection cover convex part to the hook hole in the lower portion of the front panel to lock 3 Rotate the agitator speed adjusting knob to adjust the agitation speed of sample The agitator operation lamp illuminates during agitation Protection cover Close Front panel Screw head Protection cover convex part Stirring speed control dial Stirrer operating lamp Rotation speed rises...

Page 26: ...l temperature alarm works and all operations excluding agitation stop The heater alarm lamp illuminates Buzzer keeps ringing for 30 sec If during heating the current flown into the heater lowers below the standard the abnormal heater alarm works and all operations excluding agitation stop The heater alarm lamp illuminates Buzzer keeps ringing for 30 sec If dry air volume is insufficient the overhe...

Page 27: ...intake key Spray air supply lamp illuminates and supply of spray air starts 8 Rotate the spray pressure adjusting knob while checking the value in the spray pressure display and adjust the spray pressure The spray pressure adjusting knob has a locking mechanism When adjusting pressure lightly pull the knob to unlock before operating it The setting range of spray pressure is 20 250 kPa Operate the ...

Page 28: ...the outlet temperature display and adjust the outlet temperature 11 Once the temperature reaches the desired outlet temperature put down the delivery volume fixing knob on the Lock side and fix the knob Adjust the outlet temperature in the range not exceeding 100ºC If the outlet temperature goes up to 100ºC the outlet temperature upper limit alarm works and the value in the outlet temperature disp...

Page 29: ...f the jet cleaner When adjustments were made to shorten the operation interval and if the adjusted time exceeds the current accumulated time the jet cleaner works on the spot Press the jet cleaner manual operation key and the jet cleaner can be operated in an optional timing If the spray condition does not improve after the use of the jet cleaner press down the needle knob of the upper portion of ...

Page 30: ...powder collection container into the cyclone from below 5 3End of operation When sample in the sample container runs out promptly refill it with next sample or stop the operation of the unit according to the following steps 1 Pour and deliver 100 mL of distilled water in the empty sample container and wash the silicon tube and spray nozzle 2 Adjust the interval timer adjusting knob to the OFF posi...

Page 31: ...OFF position The agitator operation lamp goes out and agitation of sample stops 7 Turn off power switch leakage breaker in this order at the right side of the unit Power supply to the unit stops and all displays on the operating panel go out Temp control and blower operation lamp Temperature controller blower RUN STOP key Stirring speed control dial Stirrer operating lamp 26 Spraying air supply la...

Page 32: ...op operation immediately and call service The dry air volume blower air volume is not adjustable The blower does not start operating Press and hold Temp Controller Blower RUN STOP key for 1 sec You intend to enter an air volume exceeding the set air volume range 0 2 0 75 m3 min Adjust to an air volume within the set air volume range The inlet filter and outlet filter are clogged Clean and replace ...

Page 33: ...clogging etc of the spray nozzle Press down the needle knob by two to three degrees Clean the nozzle tip from the nozzle cleaning port of the evaporating tube The warning buzzer sounded for 30 sec and the alarm lamp illuminated All but agitation stopped The temperature alarm lamp illuminates The inlet temperature kept 10ºC higher than the set value for more than 3 min due to failure of heater cont...

Page 34: ...method When cleaning or taking care of the product do not water directly inside the housing case or never use any cleanser polishing powder thinner oil kerosene acid and similar things Electrical shock or damage to the product may occur Caution Maintenance and Check up 7 7 1 Cleaning and care of product 29 Turn off power and the leakage breaker and further turn off the breaker on the distribution ...

Page 35: ...wer is not as desired even if you turn fully the drying air volume control dial clockwise clean the filter If dirt does not fall even after cleaning replace with a new filter 7 2 1 Cleaning or changing suction inlet filter 1 Open the maintenance port on the left side of unit 2 Remove the nut the holder and the packing 3 Detach the case cover and take out the element 4 Tap the element and spray air...

Page 36: ...by reversing procedure Code No Part name Remarks 179960 Air filter Maintenance port 7 3 Cleaning evaporating tube and cyclone Handle glass wares carefully When attaching and detaching the glass part please pay attention to handling so that it will not be damaged during cleaning Caution Cyclone Connector Packing SC Loosen Connection collar 1 Lift up the connecting collar and remove it from the cycl...

Page 37: ...reversing procedure Evaporating tube mounting portion Evaporator Evaporating tube receiving cradle Pull out Rotate Rectification board Evaporator Cyclone Separable seal packing Packing SC Connecting tube Separable clamp φ75 Code No Part name Remarks 180370 Rectification board 180000 Evaporator 147840 Upper connection packing 146760 Collecting flask cap 199050 Lower connecting packing 146750 Separa...

Page 38: ...while pushing the rim of the connector 2 Pull out the spray nozzle upward from the main unit 3 Disassemble the spray nozzle and wash respective parts in an ultrasonic cleaner etc Disassemble with reference to Spray Nozzle Disassembly Diagram on page 34 Clean the inside wall of the inside tube the gas cap and the liquid cap especially carefully The inner wall of the inside tube should be washed wit...

Page 39: ...Gasket for field cap CP3612 TEF 6 Needle adapter CP6137 SS Use a wrench opposite side distance 21 mm etc 7 O ring CP7717 11 BU 8 Inside tube 9 Outside tube 10 Body adapter Use a wrench opposite side distance 21 mm etc 11 Body 12 Gasket for spray nozzle CP10439 TEF 13 Packing box Use a wrench opposite side distance 17mm etc No 13 to 19 will come off collectively 14 15 Packing screw 16 Spring 17 Nee...

Page 40: ...de distance 3 mm The hex bar wrench is not supplied 4 Remove the connector of cyclone and packing SC 5 After replacing parts assemble them according to the reverse sequence to disassembly 7 5 1 Replacing parts at the connection Evaporator Connector Ring spring Connector Slide Remove Fixing bolt Remove Remove Cyclone Connector Code No Part name Remarks 246810 Connecting screw CAP set Evaporator Cyc...

Page 41: ...ap screw from the glass part 3 After replacing parts assemble them according to the reverse sequence to disassembly 7 5 2 Replacing collection bottle fixing parts Cap screw Ring spring Slide Spread and pull out Cap screw Code No Part name Remarks 147820 Cap screw 147800 Ring spring ID φ30 Ring spring Remove 36 ...

Page 42: ...ainless steel Electric parts Glass epoxy rubber ABS polyproprene polyester resin Silicon PVC nylon steel material stainless steel aluminum nickel Non leaded solder copper Evaporator Glass stainless steel phenol resin silicon Cyclone Glass stainless steel phenol resin PTFE silicon Separator Powder collection container Glass MC nylon silicon To dispose of the product or parts dispose of them in acco...

Page 43: ...r it is broken down with reference to the page of Troubleshooting 2 If it is still not working right ask the company where you purchased it or the nearby service center for repair Please contact your nearest service center for repair Post sale service 9 38 ...

Page 44: ...terial Qty Code No Standards Material Qty 180370 1 180360 1 180350 φ6 1 Exhaust hose Cuff for duct Stirring bar Code No Standards Material Qty 179980 Nominal 50 mm 2 5m Code No Standards Material Qty Code No Standards Material Qty 179990 Nominal 50 mm 10m 180600 φ50 1 123840 TSB 40 5 Cable for recorder Evaporator Evaporating tube cap Code No Standards Material Qty Code No Standards Material Qty Co...

Page 45: ... packing Cyclone Packing SC Code No Standards Material Qty Code No Standards Material Qty Code No Standards Material Qty 116530 1 180010 1 180190 2 Air filter Piping duct Rubber tray Code No Standards Material Qty Code No Standards Material Qty Code No Standards Material Qty 179960 1 147880 5m 180610 1 Connecting screw CAP set Screw retainer Protection cover O ring containing Si oil Code No Produc...

Page 46: ...PF 1650 SS 5 147851 Gasket for field cap CP3612 TEF 2 6 180660 Needle adapter CP6137 SS 1 7 201400 O ring CP7717 11 BU 1 12 147852 Gasket for spray nozzle CP10439 TEF 1 17 180270 Needle for liquid cap for hole diameter φ0 71 Y14293 6 1 28 SS 1 180260 Needle for liquid cap for needle hole diameter φ0 51 Y14293 6 1 20 SS 180250 Needle for liquid cap for needle hole diameter φ0 41 Y14293 6 1 16 SS 41...

Page 47: ... 265680 1 114030 2 Container with drain port Two way cock set Holder for container with drain port Code No Standards Material Qty Code No Standards Material Qty Code No Standards Material Qty 275210 1 275220 1 275230 1 Small agitator ZC clamp Agitator installation pole Code No Model Material Qty Code No Standards Material Qty Code No Standards Material Qty 260530 SPZ 2000 1 124560 1 275200 1 ...

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