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ORACLE

Rapid NMR Fat Analyzer

Manual

Summary of Contents for ORACLE

Page 1: ...ORACLE Rapid NMR Fat Analyzer Manual...

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Page 3: ...MART 6 Connection 29 Sample Preparation Sampling 34 Preparation 34 Weight 34 Glass Fiber Pads 34 Trac Film 34 Sample Preparation using the ORACLE Station Sample Preparation using the ORACLE Station 36...

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Page 5: ...cks The SMART 6 is equipped with three safety interlocks which prevent the instrument from producing microwave power if the cover is open Do not place any object between the SMART 6 cavity and the cov...

Page 6: ...erformed only by those highly trained in repair and maintenance of high voltage and microwave power systems Samples that can be considered flammable corrosive poisonous or explosive must be discussed...

Page 7: ...The ORACLE consists of an NMR magnet to perform the fat analysis an electronics box listed as processor box for controlling and storing system settings and data and may also include a SMART 6 Moistur...

Page 8: ...for faster process control and formulation changes The QuikPrep heater includes a sensor to immediately determine when a sample has been placed in the heating area ensuring each sample heats for the...

Page 9: ...ference by 90 down to 0 3 C as well as a newly designed heating component that better fits the ORACLE tubes Samples are typically conditioned for a minimum of 60 minutes at the preset temperature The...

Page 10: ...et and Processor box ORACLE NMR Magnet Quick Prep Touch Screen USB Ports Processor Box SMART 6 Only for SMART 6 users Printer optional Cavity Balance Pan Touch Screen Power Inlet Receptacle Exhaust Po...

Page 11: ...if applicable the ORACLE processor 37 lbs 17 kg and SMART 6 62 lbs 28 kg Does not have a steel iron top Materials such as wood plastic aluminum or non magnetic stainless steel are suitable surfaces E...

Page 12: ...bove Workbench Processor Box on Workbench beside Magnet Processor Box Under Workbench NOTE The processor box must be within 9 ft 3 m of the magnet 3 Remove the six screws from the sides of the magnet...

Page 13: ...tainer one on each side use the straps and carefully lift the magnet from the skid and place it on the workbench The magnet weighs approximately 120 pounds 55 kg 5 Unpack the power conditioner and pla...

Page 14: ...cord below is applicable to the U S only Power cords for instruments installed in other countries will be supplied based on electrical specifications for the applicable country 6 Plug the power cord...

Page 15: ...e used to confirm the ORACLE s functionality 1 Unbox the heater block and place it near the ORACLE either on a shelf or the benchtop 2 Plug the heater block into a standard wall outlet 3 Power the hea...

Page 16: ...o the power conditioner Wait until connecting all ORACLE cables to connect the SMART 6 to the ORACLE processor box via the supplied green Ethernet cable then pro ceed with powering the SMART 6 on 4 Fo...

Page 17: ...ct the SMB long cable to the processor box and the magnet as illustrated below 8 Connect the shim cable to the processor box as illustrated below 9 Connect the crossover CAT 5 Ethernet cable to the pr...

Page 18: ...ion 10 Connect the HDMI video cable to as illustrated below 11 Connect the Tx crossover cable to the processor box as illustrated below 12 Connect the USB cable to the ORACLE and to the processor box...

Page 19: ...second USB cable to the ORACLE and processor box as illustrated below 14 Connect the audio cable to the ORACLE and processor box as illustrated below 15 Use the 1 loom provided to wrap each cable goi...

Page 20: ...Conditioner then turn the green switch on the processor box to the ON position 17 SMART 6 Connection ONLY After following instructions to install the SMART 6 system in the SMART 6 manual do not plug t...

Page 21: ...con Description Icon Description Accept Delete Main Menu QuikPrep Temperature Back Edit Tag Next Repeat Sample Balance Connection Failing Value Passing Value SMART 6 Connection Cancel Magnet Temperatu...

Page 22: ...imal magnet temperature QuikPrep Temperature This icon displays the actual temperature and set temperature of the QuikPrep heater at the top of the magnet The icon will display a red bar up arrow when...

Page 23: ...em settings Depending on the user s access level some items ie maintenance might be grayed out Run The Run Screen allows users quick access to sample analysis at any time Simply choose the tab then cl...

Page 24: ...ic maintenance and system settings such as running diagnostics Guests can log in without a password and have the capability to run samples view results and export data Instruments The Instruments tab...

Page 25: ...ure total system functionality verified using Certified Reference Materials sealed check standard tubes and short and long term magnet stability The diagnostics tab allows the user to run a number of...

Page 26: ...ing data externally such as on a laptop or PC Users also have the option to transfer Diagnostic and Maintenance logs which can lead to faster service and minimize system downtime in the event of any i...

Page 27: ...Enter the Name and then decide the user privilege guest user and administrator 4 If user or administrator is selected then a password will be required 5 Select Save changes to add the new user Edit De...

Page 28: ...24 Manage Users 2 Select the account to be edited deleted Edit the name or privileges and select save Select Delete User followed by Delete...

Page 29: ...he Barcode Scanner icon then the Scanner button 1 Select the Barcode Scanner icon from the header icons A pop up will appear 2 Select Scanner button A new screen will appear 3 The user can manually en...

Page 30: ...used the One Time Pass please contact the Process Control Group at CEM Corporation System Setup 1 Once the ORACLE has been turned on and the software has appeared log in under the Administrator user...

Page 31: ...B is plugged into the ORACLE Processor Box highlight the USB drive listed in the window and select Import to complete the process 7 Once the Clone file has been imported select Auto Run to perform a f...

Page 32: ...4 separate stages with each stage noted The first two stages require the magnet to be empty of any tubes and the temperature conditioning and last two stages require the Normalization tube to be place...

Page 33: ...he current value for the given setting 4 3 Press the Scroll button to edit current value for a given setting if required 4 4 Press the Enter button to save the changes and return to the Interface conf...

Page 34: ...dministrator The pass word case sensitive is oracleadmin 2 Confirm the ORACLE software has connectivity to the coreboard This can be done by clicking on the Magnet Temperature icon along the top of th...

Page 35: ...E software 7 Another window will then appear Select the Start ORACLE button to activate the software 8 The ORACLE software will then reload and bring the user back to the login screen Log in again as...

Page 36: ...to continue with the remaining steps NOTE If the System Network icon has a red X over it then the Ethernet cable connecting the SMART 6 and ORACLE is not correctly plugged in or functioning properly...

Page 37: ...MART 6 icon at the top of the screen going white Alternatively the SMART 6 should now display a white ORACLE magnet icon If this icon doesn t appear or only appears grayed out please reconfirm all of...

Page 38: ...While sample size can vary from 1 0 grams to 5 0 grams depending on the type of product being tested repeatability within the same sample is important to avoid burning or under drying of a sample All...

Page 39: ...t pipette the product into the center of the top sample pad then cover the sample with the bottom sample pad to fully cover the product Then gently use the Sample Press to spread the sample thinly and...

Page 40: ...re that may cause interference during analysis 1 Remove and place one sheet of Trac Film on the platform of the ORACLE Station 2 Place the square pad and sample in the center of the Trac Film 3 Prepar...

Page 41: ...tioned in the appropriate analysis area Check to make sure the sample is not positioned beneath the bottom of the tube Sample Removal 1 After the analysis is complete press the sample pads out of the...

Page 42: ...f the samples that will be analyzed or use a separate balance to record the initial weights and manually input them into the ORACLE after the sample moisture is recorded Sample Preparation and Analysi...

Page 43: ...testing process 7 At this time the user can press the box containing the sample weight and the system will attempt to register the sample weight If using the balance choose Balance follow the instruc...

Page 44: ...ature factors This frequency lock is critical to achieving the absolute best results even in less than optimal situations 13 Then following the instructions on the screen remove the sample from the he...

Page 45: ...41 ORACLE Batch Testing with an Air or Vacuum Oven 14 After 35 seconds of analysis the ORACLE will display the final Fat result...

Page 46: ...nly be turned on and adjusted at the request of a CEM Applications Specialist The ORACLE settings are specific to the QuikPrep integrated heater at the top of the magnet The standard settings for most...

Page 47: ...rporation Process Application Support 800 726 3331 8 After the sample has been added and properly spread center the pads on the balance pan gently close the SMART 6 cover and press the START button Th...

Page 48: ...t every sample will require cooling The amount of cooling will be initially determined during the method development of the SMART 6 moisture analysis 11 After the sample has been cooled the system wil...

Page 49: ...s present and begin heating the sample for a predetermined length of time 15 The ORACLE will then heat the sample accordingly before automatically dropping it into the magnet for fat analysis Please d...

Page 50: ...ACLE Testing with a SMART 6 NOTE The SMART 6 results screen shows fat solids and moisture results Simply use the arrows to the right and left of the result to scroll through Moisture Solids and Fat re...

Page 51: ...s based on the user the sample ID or tag or the time and date of analysis 1 Select the Main Menu icon followed by the Samples tab A list of every sample that has been analyzed on the ORACLE will appea...

Page 52: ...r High Throughput ORACLE users 1 1 Select the Main Menu icon followed by Settings 1 2 Under the Sample header scroll to reach LIMS output 1 3 Press the slider to turn the output option ON which will a...

Page 53: ...te USB 4 Select the appropriate results to export screen captures system data or sample results Screen Captures Tapping the bottom right corner of the ORACLE screen three times will take a screenshot...

Page 54: ...t your local CEM Service representative Daily Inspect the sample probe for excessive dust or loose sample If any sample has fallen into the probe please contact the local CEM service provider for clea...

Page 55: ...t the blue vent cover 3 Remove the filter 4 Using purified water or a pressurized air source clean off any dust that has built up on the filter 5 Return the filter to the processor box If using water...

Page 56: ...Run 4 The ORACLE software will walk the user through each procedure and instruct the user to remove or insert the oil standard tube 5 Every test result provides a value that is compared to the intern...

Page 57: ...h set of standards are designated with a serial number to ensure facilities with multiple standards do not accidentally use the incorrect standard to produce a false failure Ensure all four Standard t...

Page 58: ...Stability test measures the peak to peak difference of signal amplitude of a Normalization Standard over the course of approximately 4 hours The purpose of this test is to confirm the internal compone...

Page 59: ...automatically determine if a sample contains low levels of fat and optimize the signal to those levels This will increase analysis time by approximately 1 5 minutes and has shown to increase repeatabi...

Page 60: ...r record keeping System Time This is used to set the correct time for the ORACLE so it is accurately reflected in sample logs Volume This adjusts the volume of the speakers for videos and other audito...

Page 61: ...e and network settings This should only be accessed during system setup and at the request of a CEM trained specialist Note this is the location of the ORACLE IP Address that is used to pair the syste...

Page 62: ...Event Viewer The event viewer is used by CEM service and applications personnel to track and determine the possible cause of certain system issues Event Viewer should only be accessed at the request o...

Page 63: ...Processor 37 lbs 17 kg Ambient Air Temperature 15 C and 30 C For optimum stability and performance the ambient temperature should not vary more than 5 day The ORACLE should not be near areas with exc...

Page 64: ...ies of Purchaser To ensure warranty coverage the purchaser must Use the instrument according to directions Connect the instrument properly to a power supply of proper voltage Replace blown fuses Repla...

Page 65: ...of use of instrument or other incidental or consequential costs expenses or damages incurred by the purchaser or any other user This warranty is not transferable Purchaser s Rights under State Law Thi...

Page 66: ...ique de Saclay 4 rue Ren Razel 91892 ORSAY Cedex France Web Address http www cemfrance fr Email info fr cem com Germany CEM GmbH Phone 011 49 2842 9644 0 Fax 011 49 2842 9644 11 Address Carl Friedrich...

Page 67: ...nd Ltd Phone 353 0 1 885 1752 Address Sky Business Centre 9a Plato Business Park Damastown Dublin 15 Ireland Web Address http www cemmicrowave co uk Email info ireland cem com CEM Distributors For a c...

Page 68: ...rved This guide contains proprietary information which shall not be reproduced or transferred to other documents or disclosed to others without prior written permission of CEM Corporation CEM IFM and...

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