Agilent Technologies G7116A User Manual Download Page 162

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Agilent InfinityLab LC Series Multicolumn Thermostats User Manual

162

Parts and Materials for Maintenance

Accessories and Consumables

InfinityLab Quick Turn Fitting Replacement Bio-compatible Capillaries

NOTE

Bio-compatible MP35N capillaries are color-coded and have an orange stripe in

addition to color-coding of capillary internal diameters (0.075 mm - black,

0.12 mm - red, 0.17 mm - green, 0.25 mm - blue).

p/n

Description

5500-1589

Quick Turn Capillary MP35N 0.075 mm x 105 mm

5500-1590

Quick Turn Capillary MP35N 0.075 mm x 150 mm

5500-1591

Quick Turn Capillary MP35N 0.075 mm x 250 mm

5500-1592

Quick Turn Capillary MP35N 0.075 mm x 500 mm

5500-1593

Quick Turn Capillary MP35N 0.12 mm x 105 mm

5500-1594

Quick Turn Capillary MP35N 0.12 mm x 150 mm

5500-1595

Quick Turn Capillary MP35N 0.12 mm x 200 mm

5500-1596

Quick Turn Capillary MP35N 0.12 mm x 280 mm

5500-1597

Quick Turn Capillary MP35N 0.12 mm x 400 mm

5500-1598

Quick Turn Capillary MP35N 0.12 mm x 500 mm

5500-1599

Quick Turn Capillary MP35N 0.17 mm x 105 mm

5500-1600

Quick Turn Capillary MP35N 0.17 mm x 150 mm

5500-1601

Quick Turn Capillary MP35N 0.17 mm x 200 mm

5500-1602

Quick Turn Capillary MP35N 0.17 mm x 280 mm

5500-1603

Quick Turn Capillary MP35N 0.17 mm x 400 mm

5500-1604

Quick Turn Capillary MP35N 0.17 mm x 500 mm

5500-1605

Quick Turn Capillary MP35N 0.17 mm x 700 mm

Summary of Contents for G7116A

Page 1: ...Multicolumn Thermostats Agilent InfinityLab LC Series User Manual Agilent InfinityLab LC Series Multicolumn Thermostats User Manual...

Page 2: ...overing the material in this document that conflict with these terms the warranty terms in the separate agreement shall control Technology Licenses The hardware and or software described in this docum...

Page 3: ...mental requirements physical and performance specifications 3 Using the Module This chapter gives instructions on how to use the module 4 Preparing the Module This chapter provides information on how...

Page 4: ...f the MCT 10 Parts and Materials for Maintenance This chapter provides information on parts for maintenance 11 Identifying Cables This chapter provides information on cables used with the Agilent Infi...

Page 5: ...23 2 Site Requirements and Specifications 28 Site Requirements 29 Physical Specifications 32 Performance Specifications 34 Valve Specifications 38 Extended Specifications 41 3 Using the Module 42 Mag...

Page 6: ...tware 104 7 Error Information 105 What Are Error Messages 106 General Error Messages 107 MCT Error Messages 113 8 Test Functions and Calibrations 119 Tests and Calibrations in Agilent Lab Advisor 120...

Page 7: ...166 Remote Cables 168 CAN LAN Cables 172 RS 232 Cables 173 USB 174 12 Hardware Information 175 Firmware Description 176 Electrical Connections 179 Interfaces 182 2 bit Configuration Switch 189 Instrum...

Page 8: ...ction G7116B with G4239C 15 Multicolumn Selection G7116A with G4237A 16 Method Development 17 Typical Applications 18 Dual column selection 2 position 6 port or 2 position 10 port valves 19 Sample enr...

Page 9: ...apability provides high flexibility for optimized speed and enhanced selectivity of LC separations Exchangeable ultra high pressure valves enable a wide range of applications such as column selection...

Page 10: ...ty provides robust and reliable separations for maximum application flexibility Exchangeable high pressure valves enable a wide range of applications such as column selection of up to four columns sam...

Page 11: ...InfinityLab Quick Connect Heat Exchangers for precolumn solvent thermostatting which contribute volumes of only 3 1 6 or 1 L for optimized low dispersion Maximum application flexibility through Pelti...

Page 12: ...tion InfinityLab Quick Connect Heat Exchanger easily installed for each column A bio inert heat exchanger is available for biological and extreme pH applications Maximum application flexibility throug...

Page 13: ...ure stability for the column This ensures that the column and the solvent flowing through it are almost at the same temperature The solvent cools down or heats up on its transfer from the Quick Connec...

Page 14: ...iple slightly different temperatures at different positions The actual temperature displayed on the user interface is always the temperature measured at the heating and cooling device The equilibratio...

Page 15: ...ages Increase productivity Higher instrument up time The valve facilitating quick changes allows the selection between up to eight different stationary phases for a variety of applications or the usag...

Page 16: ...g quick changes allows the selection between up to four different stationary phases for a variety of applications or the usage of identical stationary phases in columns with different dimensions for e...

Page 17: ...1 Introduction to the Multicolumn Thermostat Column Switching Valve Method Development Advantages Faster method development Automated method development possible Figure 6 Different chromatographic res...

Page 18: ...r valve position strongly depends on the combination of valve and module The software user interface always displays the correct situation A method modification or re plumbing of the connections is ty...

Page 19: ...ity Higher instrument up time The valve can select either column 1 or column 2 allowing quick changes between two different stationary phases for separation selectivity or immediate availability of a...

Page 20: ...ition 10 port valves Sample Enrichment Sample Cleanup Position 1 6 Pump A autosampler Waste Enrichment column Pump B Analytical detector column Position 1 2 Pump A autosampler Waste Enrichment column...

Page 21: ...ove the sample matrix in such applications as proteomics drug metabolism and environmental trace analysis The analytes are retained and concentrated onto the precolumn while the sample matrix is passe...

Page 22: ...Change 2 position 10 port valve enables the simultaneous analysis of one sample on one LC column while an extra regeneration pump flushes and equilibrates a second identical column At the end of the r...

Page 23: ...on the Internet All leak plane outlets are situated in a consistent position so that all Infinity and Infinity II modules can be stacked on top of each other Waste tubes are guided through a channel...

Page 24: ...gilent InfinityLab LC Series Multicolumn Thermostats User Manual 24 1 Introduction to the Multicolumn Thermostat Leak and Waste Handling Figure 7 Infinity II Leak Waste Concept Flex Bench installation...

Page 25: ...nt InfinityLab LC Series Multicolumn Thermostats User Manual 25 1 Introduction to the Multicolumn Thermostat Leak and Waste Handling Figure 8 Infinity II Single Stack Leak Waste Concept bench installa...

Page 26: ...Introduction to the Multicolumn Thermostat Leak and Waste Handling Figure 9 Infinity II Two Stack Leak Waste Concept bench installation The waste tube connected to the leak plane outlet on each of th...

Page 27: ...ports 5043 1221 for optimal and safe waste disposal If you decide to use your own waste solution make sure that the tubes don t immerse in the liquid Leak Sensor CAUTION Solvent incompatibility The s...

Page 28: ...cifications 32 Physical Specifications G7116B 32 Physical Specifications G7116A 33 Performance Specifications 34 Performance Specifications G7116B 34 Performance Specifications G7116A 36 Valve Specifi...

Page 29: ...esult if the devices are connected to a line voltage higher than specified Connect your instrument to the specified line voltage only WARNING Electrical shock hazard The module is partially energized...

Page 30: ...nded purposes can lead to personal injury or damage of electronic equipment Never use a power cord other than the one that Agilent shipped with this instrument Never use the power cords that Agilent T...

Page 31: ...ed to bear the weight of all modules The module should be operated in a horizontal position Condensation NOTE Agilent recommends that you install the HPLC instrument in the InfinityLab Flex Bench rack...

Page 32: ...es Width with column identification kit 472 mm G7116B may have a Column ID tag reader on both sides Line voltage 100 240 V 10 Wide ranging capability Line frequency 50 or 60 Hz 5 Power consumption 150...

Page 33: ...lumn identification kit 460 mm G7116A only has a Column ID tag reader on the left hand side Line voltage 100 240 V 10 Wide ranging capability Line frequency 50 or 60 Hz 5 Power consumption 150 VA 150...

Page 34: ...onal flexibility 1 Temperature range 20 C below ambient minimum 4 C to 110 C 2 Temperature range increment Settable in steps of 0 1 C 2 Temperature stabil ity 0 03 C 2 Temperature accu racy 0 5 C with...

Page 35: ...nd side of module Instrument control LC and CE Drivers A 02 11 or above Agilent Instant Pilot G4208A B 02 19 or above InfinityLab LC Companion G7108A 1 1 or above Lab Advisor B 02 06 or above For deta...

Page 36: ...mm length plus InfinityLab Quick Connect fittings or pre column The number of pre column Quick Connect Heat Exchangers is scalable each column can be equipped with an individual heat exchanger for be...

Page 37: ...G7116A is a hosted module The LC stack needs to contain suitable host module or a LAN card for communication and control Maintenance and safety related fea tures Extensive diagnostics error detection...

Page 38: ...4 Position 10 Port Valve 800 bar Type Specification Maximum pressure 800 bar Typical application 4 column selection Port size Accepts M4 male threaded fittings Liquid contacts PEEK Stainless steel pH...

Page 39: ...240 2 Position 10 Port Valve 1300 bar Type Specification Maximum pressure 1300 bar Typical application Anything a 2 Position 6 Port valve can do plus alternating column regeneration Port size Accepts...

Page 40: ...pts M4 male threaded fittings Liquid contacts PEEK Stainless steel pH range 0 141 1 incompatible with some mineral acids For more information see Solvent Information Table 12 G4234A 5067 4284 6 Positi...

Page 41: ...with 3 L internal volume that is suitable for standard applications The G7116B MCT is delivered with Low Dispersion Quick Connect Heat Exchanger 0 12 mm with 1 6 L internal volume that is suitable for...

Page 42: ...on Lock and the Valve Dummy 55 Install the Valve Head and Connect Capillaries 57 Installing the capillaries 61 Install the Divider Assembly 63 Install the Thermal Equilibration Device 64 Installing an...

Page 43: ...Agilent InfinityLab LC Series Multicolumn Thermostats User Manual 43 3 Using the Module Magnets Magnets 1 Magnet in the front door of the Multicolumn Thermostat...

Page 44: ...Agilent InfinityLab LC Series Multicolumn Thermostats User Manual 44 3 Using the Module Turn on off Turn on off This procedure exemplarily shows an arbitrary LC stack configuration 1 2 Power switch On...

Page 45: ...Agilent InfinityLab LC Series Multicolumn Thermostats User Manual 45 3 Using the Module Turn on off 3 Turn instrument On Off with the control software 4 Power switch Off 5...

Page 46: ...of six possible module conditions Status indicators 1 Idle 2 Run mode 3 Not ready Waiting for a specific pre run condition to be reached or completed 4 Error mode interrupts the analysis and requires...

Page 47: ...Manual 47 3 Using the Module Open the Front Door Open the Front Door The front door opens in two angles 90 and 180 In the 90 position it can be used as a tray 1 Press the release button to open the fr...

Page 48: ...Thermostat MCT New design Quick Connect Heat Exchangers do not have twist lock clips on the front side of the heat exchanger Instead Quick Connect Heat Exchangers include two column holders to fix the...

Page 49: ...hanger Standard G7116 60021 Quick Connect Heat Exchanger Ultra Low Dispersion G7116 60031 Quick Connect Heat Exchanger High Flow 5067 5957 InfinityLab Quick Connect Assy ST 0 12 mm x 105 mm from heat...

Page 50: ...t Bio Heat Exchanger Standard Flow G7116 60081 Quick Connect Bio Heat Exchanger High Flow G7116 68003 Column Holder Lamella 2 pk 5500 1596 Quick Turn Capillary MP35N 0 12 mm x 280 mm 5067 5966 Infinit...

Page 51: ...lary to the outlet of the Quick Connect Heat Exchanger 4 Position the heat exchanger in the groove of the MCT heater block and prepare column holders to fix the heat exchanger 5 Turn column holders to...

Page 52: ...500 1191 InfinityLab Quick Turn Capillary ST 0 12 mm x 280 mm long socket from column to detector 5067 5966 InfinityLab Quick Turn Fitting column inlet 0100 1516 Finger tight fitting PEEK 2 pk column...

Page 53: ...ser Manual 53 3 Using the Module Exchange a Column Remove a column 1 Remove the column from the column holder 2 Disconnect the column outlet 3 Open the lever of the Quick Connect Fitting 4 Unscrew and...

Page 54: ...itting until it is finger tight 3 Close the lever to make a leak tight connection 4 Connect the capillary to detector to the column outlet When using the Quick Turn Fitting tighten the fitting until i...

Page 55: ...sure that the guide pin snaps into the groove of the valve drive thread Remove the Transportation Lock and the Valve Dummy The following procedure demonstrates the necessary steps for installing the...

Page 56: ...alve Heads 1 Switch off the module 2 When unscrewing the transportation lock push it back until the last screw is removed the valve rail is spring loaded 3 Press on the valve dummy 1 to release it 2 s...

Page 57: ...ins sensitive optical parts which need to be protected from dust and other pollution Pollution of these parts can impair the accurate selection of valve ports and therefore bias measurement results Al...

Page 58: ...ves on the valve drive s actuator axis Their match depends on the diameter of the pin and groove NOTE The tag reader reads the valve head properties from the valve head RFID tag during initialization...

Page 59: ...into the outside groove you have to turn the valve head until you feel that the two pins snap into the grooves Now you should feel additional resis tance from the valve drive while continuously turnin...

Page 60: ...Using the Module Installing Valve Heads 3 Install all required capillary connections to the valve 4 Push the valve head until it snaps in and stays in the rear position 5 Power on or power cycle your...

Page 61: ...ngs into ports 9 and 10 Figure 11 Rerouting of 2 position 10 port valve to match 2 position 6 port valve 1 Connect the capillaries going to a valve and fasten them immediately with a spanner 2 Startin...

Page 62: ...d modules autosampler detector additional pumps Fit all unused valve ports with blank nuts 8 Push the valve into the rear position 9 Place the capillaries that go to another module or waste into the c...

Page 63: ...eater element to separate these two temperature zones 1 Push the rear part of the Divider Assembly into position 1 and fix it with the screw 2 2 Install the valve head if used See Replace Valve Heads...

Page 64: ...uilibration Devices are installed at the same time 5 6 7 8 1 2 3 4 Tools required p n Description 5023 2502 Hex driver SW 6 35 slitted Preparations Install Quick Change Valve Head and columns accordin...

Page 65: ...of the capillary guidance remove the side covers of the InfinityLab Thermal Equilibration Devices that point towards the valve 5 Turn twist lock clips with the hex driver to fix the InfinityLab Therm...

Page 66: ...17 InfinityLab Column Identification Tag Preparations Power off the instrument CAUTION Electronic boards and components are sensitive to electrostatic discharge ESD ESD can damage electronic boards an...

Page 67: ...lders that may already be installed on the sides of the MCT cover 2 Unlock the left and right G7116B only side cover inserts by pushing them to the rear and put them aside 3 Identify the left and righ...

Page 68: ...the flex cable to the column ID module a Open the locking mechanism of the connector by lifting up the frame b Push in the cable with the contacts facing to the rear c Close the locking mechanism d V...

Page 69: ...olumn Thermostats User Manual 69 3 Using the Module Installing and Using Column ID Tags 7 Repeat steps 4 to 9 for the column ID module on the other side for G7116B on the right 8 Install the waste tub...

Page 70: ...column 2 Install the column in the column compartment see Exchange a Column on page 52 3 Plug the free end of the Column ID Tag into the adjacent socket in the column tag reader unit NOTE It is impor...

Page 71: ...ed with the column These fields are read only from the perspective of the user meaning that their content cannot be manually edited or erased For pre labeled Agilent columns the static fields are pre...

Page 72: ...rom a database an existing catalog or inventory or the Agilent columns guide This option is available only for the OpenLab CDS ChemStation C 01 07 SR2 or higher When plugging a new tag into the tag re...

Page 73: ...a line above the currently selected line or the Append button to add a line to the end of the table The new line contains a copy of the information in the template line 4 Click the Edit button to disp...

Page 74: ...ut the columns attached to each position in the column compartment The information in the Column Assignment dialog box is in three sections 1 The Plumbing section contains a table where you can specif...

Page 75: ...n information is imported into the Column Tag Information table NOTE It may take several seconds before the information appears in the Column Tag Information table NOTE The characters semicolon single...

Page 76: ...information in the tag you can irrevocably seal the tag to set all static fields to read only Right click in the appropriate line in the Column Tag Information table and select Seal Column Tag from t...

Page 77: ...the column compartment the columns are color coded Place the mouse cursor over a column to display a tooltip of the column information from the column ID tag Click a column to highlight the column inf...

Page 78: ...ion s Method and Control view also allows you a quick view of the column ID tag information Figure 17 The dashboard panel of the column compartment Place the mouse cursor over the column ID tag icon t...

Page 79: ...onal columns The table includes not only the columns that are installed in the column thermostat device s but also the inventory of other available columns for example columns that have been used in t...

Page 80: ...ight of the table to show the full table Tag Status Shows the status of the column ID tag Empty The position is empty or has a column without a column ID tag A column with a column ID tag is installed...

Page 81: ...erature in C experienced by the column to date Dynamic Read Read MaximumTempera ture The safe maximum operating temperature of the column in C Static Read Write Minimum pH The minimum pH supported by...

Page 82: ...monitoring of Agilent Infinity II LC modules Excellent usability and ease of use through a user interface specifically tailored for mobile devices simple intuitive touch enabled and visual controllab...

Page 83: ...nd Waste Handling 84 Waste Concept 85 Solvent Information 86 Capillary Coding Guide 92 Syntax for Capillary Description 92 At a Glance Color Coding Keys 94 Install Capillary Connections 95 This chapte...

Page 84: ...s includes the solvent temperature in the sample compartment For the solvents methanol and ethanol keep the solvent temperature at least 25 C 45 F below the boiling point Do not operate the instrument...

Page 85: ...g the Module Leak and Waste Handling Waste Concept 1 Agilent recommends using the 6 L waste can with 1 Stay Safe cap GL45 with 4 ports 5043 1221 for optimal and safe waste disposal If you decide to us...

Page 86: ...xcellent robustness under typical HPLC conditions For any special condition please consult the material information section or contact Agilent Disclaimer Subsequent data was collected from external re...

Page 87: ...tration pH impurities stress surface finish and dissimilar metal contacts Polyphenylene Sulfide PPS Polyphenylene sulfide has outstanding stability even at elevated temperatures It is resistant to dil...

Page 88: ...f steel and ensures pressure stability up to 600 bar If in doubt consult the available literature about the chemical compatibility of PEEK Polyimide Agilent uses semi crystalline polyimide for rotor s...

Page 89: ...norganic acids like nitric acid sulfuric acid and organic solvents especially at higher temperatures replace if your chromatography method allows by phosphoric acid or phosphate buffer which are less...

Page 90: ...ion in anhydrous methanol which can be avoided by adding a small amount of water about 3 Slight corrosion is possible with ammonia 10 Diamond Like Carbon DLC Diamond Like Carbon is inert to almost all...

Page 91: ...opolymer tubings which are used in all Agilent degassers except G1322A G7122A are not compatible with fluorinated solvents like Freon Fluorinert or Vertrel They have limited life time in the presence...

Page 92: ...ble 13 Capillary coding guide Type The type gives some indication on the pri mary function like a loop or a connection capillary Material The material indicates which raw material is used Fitting left...

Page 93: ...tight V 1200 bar B Bio P PEEK I Intermedi ate 1 Fused silica in contact with solvent 2 Stainless steel coated PEEK Table 13 Capillary coding guide Type The type gives some indication on the pri mary...

Page 94: ...ng Internal diameter in mm Color code 0 015 Orange 0 025 Yellow 0 05 Beige 0 075 Black 0 075 MP35N Black with orange stripe 0 1 Purple 0 12 Red 0 12 MP35N Red with orange stripe 0 17 Green 0 17 MP35N...

Page 95: ...0 17 mm x 500 mm SI SI 5500 1246 Multisampler MCT Valve Heat Exchanger Capillary ST 0 17 mm x 400 mm SL SL 5500 1252 Vialsampler MCT Valve Heat Exchanger Capillary ST 0 17 mm x 105 mm SL SL 5500 1240...

Page 96: ...Quick Turn Capillary ST 0 12 mm x 280 mm long socket 5500 1191 Column MCT Valve Detector Waste accessory kit 5062 8535 VWD Waste Tube PTFE 0 7 mm x 5 m 1 6 mm od 5062 2462 DAD FLD Waste Analytical tu...

Page 97: ...ttle Head Assembly G7120 60007 Solvent Bottle Infinity II Pump Capillary MP35N 0 17 mm x 500 mm SI SI 5500 1419 Pump Multisampler Capillary MP35N 0 12 mm x 500 mm SI SI 5500 1279 Multisampler MCT Quic...

Page 98: ...nd of the tubing or capillary 3 Carefully slide the ferrule components on after the nut and then finger tighten the assembly while ensuring that the tubing is completely seated in the bottom of the en...

Page 99: ...the ferrule is correctly positioned on the tubing or capillary NOTE The first time that the swagelock fitting is used on a column or an injection valve the position of the ferrule is permanently set I...

Page 100: ...gilent InfinityLab LC Series Multicolumn Thermostats User Manual 100 5 Optimization Optimizing the Column Compartment 101 This chapter provides information on how to optimize the Multicolumn Thermosta...

Page 101: ...ables section for additional available heat exchangers with various internal volumes to address certain applications in terms of flow rates and dispersion volume optimization Keep the left and right h...

Page 102: ...ab LC Series Multicolumn Thermostats User Manual 102 6 Troubleshooting and Diagnostics Available Tests vs User Interfaces 103 Agilent Lab Advisor Software 104 Overview about the troubleshooting and di...

Page 103: ...g on the user interface the available tests and the screens reports may vary see chapter Test Functions and Calibrations Preferred tool should be the Agilent Lab Advisor software see Agilent Lab Advis...

Page 104: ...ed Lab Advisor Basic is included with every Agilent 1200 Infinity Series and Agilent InfinityLab LC Series instrument The Lab Advisor Advanced features can be unlocked by purchasing a license key and...

Page 105: ...Sensor Open 112 Compensation Sensor Short 112 MCT Error Messages 113 VALVE INIT FAILED 113 VALVE FAILED 114 VALVE TAG VIOLATION 114 WRONG VALVE 115 WAIT TIMEOUT 116 HEATEX OVERTEMP 116 UHX SENSOR ERRO...

Page 106: ...get a notification all LEDs get red and the run will be stopped Depending on the module type this stop is implemented differently For example for a pump the flow will be stopped for safety reasons For...

Page 107: ...uggested actions 1 The analysis was completed successfully and the timeout function switched off the module as requested Check the logbook for the occurrence and source of a not ready condition Restar...

Page 108: ...in another module with a CAN connection to the system Fix the leak in the external instrument before restarting the module 2 Leak detected in an external instrument with a remote connection to the sy...

Page 109: ...ystem configuration If one or more of the modules is no longer recognized as being connected to the system the error message is generated Probable cause Suggested actions 1 Not ready condition in one...

Page 110: ...ed by the leak algorithm to determine whether a leak is present When a leak occurs the leak sensor is cooled by the solvent This changes the resistance of the leak sensor which is sensed by the leak s...

Page 111: ...when solvent cools the leak sensor causing the leak sensor current to change within defined limits If the current increases above the upper limit the error message is generated Probable cause Suggeste...

Page 112: ...e power switch board in the module has failed open circuit The resistance across the temperature compensation sensor NTC on the power switch board is dependent on ambient temperature The change in res...

Page 113: ...reference index position An error is generated if the reference index cannot be found within a given time Probable cause Suggested actions 1 Defect in cable connection of valve drive con trol Please...

Page 114: ...a different valve head if possible Contact your Agilent service representative 2 Defective sensor on the valve drive motor Check valve head for correct installation Try to identify the source of trou...

Page 115: ...G4232D 5067 4240 2 position 10 port Valve 1300 bar G4231C 5067 4241 2 position 6 port Valve 1300 bar G4234A 5067 4284 6 position 14 port Valve 800 bar G4234C 5067 4273 6 position 14 port Valve 1300 b...

Page 116: ...Probable cause Suggested actions 1 Defective heater Contact your Agilent service representative 2 Defective mainboard Please contact your Agilent service representa tive Probable cause Suggested actio...

Page 117: ...cause Suggested actions 1 Defective sensor Please contact your Agilent service representa tive 2 Defective cable Please contact your Agilent service representa tive 3 Defective mainboard Please contac...

Page 118: ...r Please contact your Agilent service representa tive 2 Defective mainboard Please contact your Agilent service representa tive 3 Defective cable Please contact your Agilent service representa tive Pr...

Page 119: ...rmostats User Manual 119 8 Test Functions and Calibrations Tests and Calibrations in Agilent Lab Advisor 120 Thermostat Test 121 System Pressure Test 122 Sensors Offset Calibration 123 This chapter de...

Page 120: ...tions Tests and Calibrations in Agilent Lab Advisor Tests and Calibrations in Agilent Lab Advisor Use the tests and diagnostic features provided in the Agilent Lab Advisor software to check if your mo...

Page 121: ...ltier elements The instrument starts the test when the heater temperature is within 5 C of the current measured ambient temperature After the start the instrument is cooling down to 4 C below the star...

Page 122: ...valve installed in the MCT CAUTION Wrong use of System Pressure Test may damage components Do not use higher test max pressure settings as the lowest rated pressure component in the tests flow path NO...

Page 123: ...n the heat sink and heat exchanger This is to ensure that no temperature gradient inside the heat exchanger is present and both temperature sensors are exposed to the exact same temperature Because th...

Page 124: ...Maintenance 125 Cautions and Warnings 127 Overview of Maintenance 129 Cleaning the Module 130 Correcting Leaks 131 Maintain the Column Switching Valve 132 Replace Valve Heads 135 Prepare the MCT for T...

Page 125: ...ion to Maintenance The module is designed for easy maintenance The most frequent maintenance such as maintaining valve heads if optional valve drive is installed or replacing heat exchangers can be do...

Page 126: ...b LC Series Multicolumn Thermostats User Manual 126 9 Maintenance Introduction to Maintenance Figure 19 Overview of maintenance parts G7116A Valve Door NOTE There are no serviceable parts inside Do no...

Page 127: ...the material handling and safety data sheet supplied by the vendor and follow good laboratory practice The volume of substances should be reduced to the minimum required for the analysis Do not operat...

Page 128: ...to the products failure to comply with procedures in Agilent product user guides or use of the products in violation of applicable laws rules or regulations Use your Agilent products only in the manne...

Page 129: ...stall Heat Exchanger on page 48 When new application requires a change Installing the capillaries on page 61 When new application requires a change Correcting Leaks on page 131 If a leak has occurred...

Page 130: ...void using organic solvents for cleaning purposes They can cause damage to plastic parts WARNING Liquid dripping into the electronic compartment of your module can cause shock hazard and damage the mo...

Page 131: ...ue to dry the leak sensor area 3 Observe the capillary connections and the column switching valve for leaks and correct if required 4 Reinstall the door When If a leakage has occurred at the heat exch...

Page 132: ...ules use bio inert parts only For 1290 Infinity II Bio LC modules use bio bio compatible parts only Do not mix parts between 1260 Infinity II Bio Inert LC modules and 1290 Infinity II Bio LC modules W...

Page 133: ...tor seal 8 Replace the stator ring Ensure the stator ring is flush with the valve body 9 Place the new if required stator face in place on the stator head Reinstall the stator head 10 Insert the stato...

Page 134: ...seal 6 Bearing ring 7 Spanner nut available for service only NOTE Figure 20 on page 134 illustrates replacement parts for the valve heads with the 6 column selector valve as an example The valves can...

Page 135: ...can drop out of the solvent connections when removing them from your valve head When working with these substances observe appropriate safety procedures for example by wearing goggles safety gloves an...

Page 136: ...herefore bias measurement results Always install a valve head for operation and storage For protecting the actuator a dummy valve head part of Transportation Lock Kit G1316 67001 can be used instead o...

Page 137: ...it to its outer position 3 Remove all capillary connections from the valve head 4 Unscrew the nut and remove the valve head 5 Put the new valve head onto the valve drive such that the lobe fits to the...

Page 138: ...s Multicolumn Thermostats User Manual 138 9 Maintenance Replace Valve Heads 7 Install all required capillary connections to the valve 8 Push the valve head until it snaps in and stays in the rear posi...

Page 139: ...nsportation valve head Bring the transportation valve head to the outer position 3 Fix the Transportation Lock to the MCT When If an MCT including the Valve Drive Option shall be transported NOTE The...

Page 140: ...osted module and always needs to be connected to a host with matching firmware of same revision When The installation of newer firmware might be necessary if a newer version solves problems of older v...

Page 141: ...ts 144 Valve Options Overview for G7116B 146 Valve Options Overview for G7116A 148 Column ID Parts 150 Accessories and Consumables 151 Accessories and Consumables for G7116B 151 Accessories and Consum...

Page 142: ...Kit Infinity II MCT includes parts 2 7 2 G7116 40100 Base Cover Infinity II MCT 3 G7116 40103 Side Cover Left Insert Infinity II MCT 4 Side Cover Left Infinity II MCT available only as a part of the...

Page 143: ...ies Multicolumn Thermostats User Manual 143 10 Parts and Materials for Maintenance Leak Parts Leak Parts Figure 22 Plastic parts 1 2 Item p n Description 1 G7116 40043 Leak Adapter Top MCT 2 G7116 400...

Page 144: ...ons and Parts Valve Options and Parts MCT External Valve Drive p n Description G1353D Valve drive upgrade kit for MCT p n Description G1170A External Valve Drive 5067 6138 Valve Holder Kit Right IF II...

Page 145: ...alves can vary in their appearance and do not necessarily include all of the illustrated parts Neither every spare part is available for each flavor of the valve Use the tables Valve Options Overview...

Page 146: ...Ring 5067 4233 8 Position 18 Port Valve 1300 bar 5068 0200 PEEK 5068 0199 5068 0089 n a 5067 4241 2 Position 6 Port Valve 1300 bar 5068 0207 PEEK 5068 0006 1535 4857 5068 0120 5067 4240 2 Position 10...

Page 147: ...bsolete valve heads for G7116B Valve Head Rotor Seal Stator Head Stator Screws Stator Ring 5067 4121 8 Position 9 Port Valve 1200 bar 5068 0002 Vespel 5068 0001 1535 4857 5068 0127 5067 4117 2 Positio...

Page 148: ...ring 1535 4045 5067 4282 2 Position 6 Port Valve 800 bar 0101 1409 PEEK 0101 1417 1535 4857 5068 0120 n a Bearing ring 1535 4045 5067 4148 2 Position 6 Port Bio Inert Valve 600 bar 0101 1409 PEEK 5068...

Page 149: ...no longer orderable Table 23 Replacement parts obsolete valve heads for G7116A Valve Head Rotor Seal Stator Head Stator Screws Stator Ring 5067 4287 4 Position 10 Port Valve 600 bar 5068 0264 PEEK 50...

Page 150: ...cription G4750B Column ID upgrade kit for G7116B p n Description G4750A Column ID upgrade kit for G7116A p n Description G7116 81001 Column ID flex board connection right G7116 81002 Column ID flex bo...

Page 151: ...intenance p n Description 5181 1516 CAN cable Agilent module to module 0 5 m 5063 6527 Tubing Silicon Rubber 1 2 m ID OD 6 9 mm 5500 1191 InfinityLab Quick Turn Capillary ST 0 12 mm x 280 mm long sock...

Page 152: ...ing tool G7116 60006 Divider Assembly MCT 5023 2625 Union MP35N Double Drain Connector 5500 1578 Quick Connect Capillary MP35N 0 12 mm x 105 mm 5067 5965 InfinityLab Quick Connect LC fitting 5500 1598...

Page 153: ...le Agilent module to module 0 5 m 5063 6527 Tubing Silicon Rubber 1 2 m ID OD 6 9 mm 0100 1516 Finger tight fitting PEEK 2 pk 5500 1193 InfinityLab Quick Turn Capillary ST 0 17 mm x 105 mm long socket...

Page 154: ...xchanger Bio inert 5043 0915 Fitting mounting tool 5063 6527 Tubing Silicon Rubber 1 2 m ID OD 6 9 mm 5067 5403 UHP fitting 5067 4741 ZDV union Bio inert p n Description G7116 68003 Column Holder Lame...

Page 155: ...Flow rate 0 075 mm i d capillary 0 12 mm i d capillary 0 17 mm i d capillary 2 mL min Ultra low Dispersion G7116 60021 Internal volume 1 0 L Standard Flow G7116 60015 Internal volume 1 6 L Large ID G...

Page 156: ...twist lock clips of the Quick Connect Heat Exchanger are used to secure the Quick Connect Heat Exchanger in the heater block of the MCT New design Quick Connect Heat Exchanger col umn holders lamella...

Page 157: ...05 mm 5067 6163 InfinityLab Quick Connect Assy ST 0 075 mm x 150 mm 5067 6164 InfinityLab Quick Connect Assy ST 0 075 mm x 220 mm 5067 6165 InfinityLab Quick Connect Assy ST 0 075 mm x 280 mm 5067 595...

Page 158: ...5500 1173 InfinityLab Capillary ST 0 12 mm x 105 mm 5500 1172 InfinityLab Capillary ST 0 12 mm x 150 mm 5500 1171 InfinityLab Capillary ST 0 12 mm x 220 mm 5500 1170 InfinityLab Capillary ST 0 12 mm x...

Page 159: ...anual 159 10 Parts and Materials for Maintenance Accessories and Consumables InfinityLab Quick Turn Fitting Figure 25 InfinityLab Quick Turn Fitting p n Description 5067 5966 InfinityLab Quick Turn Fi...

Page 160: ...nityLab Quick Turn Capillary ST 0 12 mm x 280 mm long socket 5500 1192 Capillary ST 0 12 mm x 500 mm long socket 5500 1193 InfinityLab Quick Turn Capillary ST 0 17 mm x 105 mm long socket 5500 1194 Ca...

Page 161: ...0 1576 Quick Connect Capillary MP35N 0 075 mm x 220 mm 5500 1577 Quick Connect Capillary MP35N 0 075 mm x 280 mm 5500 1578 Quick Connect Capillary MP35N 0 12 mm x 105 mm 5500 1579 Quick Connect Capill...

Page 162: ...mm x 250 mm 5500 1592 Quick Turn Capillary MP35N 0 075 mm x 500 mm 5500 1593 Quick Turn Capillary MP35N 0 12 mm x 105 mm 5500 1594 Quick Turn Capillary MP35N 0 12 mm x 150 mm 5500 1595 Quick Turn Cap...

Page 163: ...tats User Manual 163 11 Identifying Cables Cable Overview 164 Analog Cables 166 Remote Cables 168 CAN LAN Cables 172 RS 232 Cables 173 USB 174 This chapter provides information on cables used with the...

Page 164: ...Description 35900 60750 Agilent 35900A A D converter 01046 60105 Analog cable BNC to general purpose spade lugs p n Description 5188 8029 ERI to general purpose 5188 8044 Remote Cable ERI ERI 5188 80...

Page 165: ...e shielded 7 m for point to point connec tion p n Description RS232 61601 RS 232 cable 2 5 m Instrument to PC 9 to 9 pin female This cable has special pin out and is not compatible with connecting pri...

Page 166: ...log Cables One end of these cables provides a BNC connector to be connected to Agilent modules The other end depends on the instrument to which connection is being made Agilent Module to 35900 A D con...

Page 167: ...ing Cables Analog Cables Agilent Module to BNC Connector Agilent Module to General Purpose p n 8120 1840 Pin BNC Pin Agilent module Signal Name Shield Shield Analog Center Center Analog p n 01046 6010...

Page 168: ...tension Cable 1 2 m D Sub15 pin male female p n 5188 8029 pin Color code Enhanced Remote Classic Remote Active TTL 1 white IO1 START REQUEST Low 2 brown IO2 STOP Low 3 green IO3 READY High 4 yellow IO...

Page 169: ...s 5188 8045 ERI to APG Connector D_Subminiature 15 pin ERI Connector D_Subminiature 9 pin APG p n 5188 8045 Pin ERI Signal Pin APG Active TTL 10 GND 1 1 Start Request 9 Low 2 Stop 8 Low 3 Ready 7 High...

Page 170: ...provides a Agilent Technologies APG Analytical Products Group remote connector to be connected to Agilent modules The other end depends on the instrument to be connected to Table 26 5188 8057 ERI to A...

Page 171: ...d 2 Brown 2 Brown Prepare run Low 3 Gray 3 Gray Start Low 4 Blue 4 Blue Shut down Low 5 Pink 5 Pink Not connected 6 Yellow 6 Yellow Power on High 7 Red 7 Red Ready High 8 Green 8 Green Stop Low 9 Blac...

Page 172: ...to be connected to Agilent modules CAN or LAN connectors CAN Cables LAN Cables p n Description 5181 1516 CAN cable Agilent module to module 0 5 m 5181 1519 CAN cable Agilent module to module 1 m p n D...

Page 173: ...escription RS232 61601 RS 232 cable 2 5 m Instrument to PC 9 to 9 pin female This cable has special pin out and is not compatible with connecting printers and plotters It is also called Null Modem Cab...

Page 174: ...ostats User Manual 174 11 Identifying Cables USB USB To connect a USB Flash Drive use a USB OTG cable with Mini B plug and A socket p n Description 5188 8050 USB A M USB Mini B 3 m PC Module 5188 8049...

Page 175: ...179 Rear View of the Module 180 Information on Instrument Serial Number 181 Interfaces 182 Overview Interfaces 184 ERI Enhanced Remote Interface 186 USB Universal Serial Bus 188 2 bit Configuration Sw...

Page 176: ...s properties are the complete communication capabilities CAN LAN USB and RS 232 memory management ability to update the firmware of the main system Main System Its properties are the complete communic...

Page 177: ...t number for example 1315B for the G1315B DAD R the firmware revision for example A for G1315B or B for the G1315C DAD VVV is the revision number for example 650 is revision 6 50 XXX is the build numb...

Page 178: ...their initial firmware revision For example a G1315C DAD SL cannot be downgraded below firmware revision B 01 02 or to a A xx xx Some modules can be re branded e g G1314C to G1314B to allow operation...

Page 179: ...the module from a computer through a LAN connection This connector is activated and can be configured with the configuration switch With the appropriate software the USB connector may be used to contr...

Page 180: ...Agilent InfinityLab LC Series Multicolumn Thermostats User Manual 180 12 Hardware Information Electrical Connections Rear View of the Module Figure 27 Rear view of the Multicolumn Thermostat G7116A B...

Page 181: ...al number information on the instrument labels provide the following information CCYWWSSSSS Format CC country of manufacturing DE Germany JP Japan CN China YWW year and week of last major manufacturin...

Page 182: ...232 Analog APG A ERI E Special Pumps G7104A C 2 No Yes Yes 1 A G7110B 2 Yes Yes No No E G7111A B G5654A 2 Yes Yes No No E G7112B 2 Yes Yes No No E G7120A G7132A 2 No Yes Yes 1 A G7161A B 2 Yes Yes No...

Page 183: ...equires a host module with on board LAN with minimum FW B 06 40 or C 06 40 or with addi tional G1369C LAN Card G1364E F G5664B 2 Yes Yes No No E THERMOSTAT for G1330B Others G7116A B 2 No No No No No...

Page 184: ...B interface replaces the RS 232 Serial interface in new FUSION generation modules For details on USB refer to USB Universal Serial Bus on page 188 Analog Signal Output The analog signal output can be...

Page 185: ...V power supply A TTL signal is defined as low or L when between 0 V and 0 8 V and high or H when between 2 0 V and 5 0 V with respect to the ground terminal Table 28 ERI signal distribution Pin Signa...

Page 186: ...es products using the FUSION core electronics use ERI This interface is already used in the Agilent Universal Interface Box 2 UIB2 ERI Description The ERI interface contains eight individual programma...

Page 187: ...trolled 1 Wire Data Future Use This serial line can be used to read out an EPROM or write into an EPROM of a connected ERI device The firmware can detect the connected type of device automatically and...

Page 188: ...se Available by firmware command defined turn on off For devices that need higher power Class 0 0 5 A maximum 12 W Class 1 1 0 A maximum 24 W Class 2 2 0 A maximum 48 W Class depends on hosting module...

Page 189: ...are Information 2 bit Configuration Switch 2 bit Configuration Switch Figure 29 Location of Configuration Switch 2 bit configuration switch Table 29 Dip switches settings for G7116A B Mode Select 1 2...

Page 190: ...This pack is then housed in a metal inner cabinet which is enclosed by a plastic external cabinet The advantages of this packaging technology are virtual elimination of fixing screws bolts or ties red...

Page 191: ...the user interface when the limit is exceeded Some counters can be reset to zero after the required maintenance procedure Using the EMF Counters The user settable EMF limits for the EMF Counters enab...

Page 192: ...4 Do Not Operate in an Explosive Atmosphere 195 Do Not Remove the Instrument Cover 195 Do Not Modify the Instrument 195 In Case of Damage 195 Solvents 196 Safety Symbols 197 Waste Electrical and Elect...

Page 193: ...ies assumes no liability for the customer s failure to comply with these requirements Safety Standards This is a Safety Class I instrument provided with terminal for protective earthing and has been m...

Page 194: ...d compliance with safety or EMC regulations Make all connections to the unit before applying power NOTE Note the instrument s external markings described under Safety Symbols on page 197 WARNING Missi...

Page 195: ...RNING Presence of flammable gases or fumes Explosion hazard Do not operate the instrument in the presence of flammable gases or fumes WARNING Instrument covers removed Electrical shock Do Not Remove t...

Page 196: ...compartment For the solvents methanol and ethanol keep the solvent temperature at least 25 C 45 F below the boiling point Do not operate the instrument in an explosive atmosphere Do not use solvents o...

Page 197: ...l warming potential GWP see instrument label Flammable Material For Sample Thermostat which uses flammable refrigerant consult Agilent Information Center User Manual before attempting to install or se...

Page 198: ...ay from devices and objects that could be damaged by strong magnetic fields Indicates a pinching or crushing hazard Indicates a piercing or cutting hazard Table 30 Symbols WARNING A WARNING alerts you...

Page 199: ...pment WEEE Directive This product complies with the European WEEE Directive marking requirements The affixed label indicates that you must not discard this electrical electronic product in domestic ho...

Page 200: ...d to provide optimized protection against radio interference All cables are in compliance with safety or EMC regulations Test and Measurement If test and measurement equipment is operated with unscree...

Page 201: ...01 13 Appendix Sound Emission Certification for Federal Republic of Germany Sound Emission Certification for Federal Republic of Germany Sound pressure Sound pressure Lp 70 db A accroding to DIN EN 27...

Page 202: ...icolumn Thermostats User Manual 202 13 Appendix Agilent Technologies on Internet Agilent Technologies on Internet For the latest information on products and services visit our worldwide web site on th...

Page 203: ...tains technical reference information about the Agilent 1290 Infinity II Multicolumn Thermostat G7116B and Agilent 1260 Infinity II Multicolumn Thermostat G7116A The manual describes the following Int...

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