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Vzor MAPK-302E, Руководство по эксплуатации

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10 

1.6 Measuring instruments, tools and accessories 

 
 
 

1.6.1 The following tools and accessories, which are not included in the de-

livery set, will be additionally required for maintenance of the analyzer: 

  2 mm cross screwdriver; 

  В-1-250 beaker; 

  КН-100-19/26 flask; 

  hydroquinone, chemically pure; 

  sodium or potassium hydroxide, chemically pure. 

Instead of hydroquinone, chemically pure and sodium or potassium  hydrox-

ide, chemically pure the following reagents may be used: 

  sodium sulphite Na

2

SO

4

, chemically pure; 

  potassium permanganate KMnO

4

, chemically pure. 

 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 

Содержание MAPK-302E

Страница 1: ...MAPK 302E DISSOLVED OXYGEN METER Operation Manual Nizhny Novgorod 2010 АЯ 74 ...

Страница 2: ...product quality improvement If you have any trouble with the instrument performance please contact us in writing or by phone Postal address 603106 Russia Nizhny Novgorod POB 253 Telephone 7 831 229 65 67 412 29 40 E mail market vzor nnov ru Website www vzornn com ...

Страница 3: ...ion 7 1 6 Measuring instruments tools and accessories 10 2 INTENDED USE 11 2 1 Operating limitations 11 2 2 Safety 11 2 3 Pre starting procedures 11 2 4 Measurement procedure 17 2 5 Functional check 20 2 6 Troubleshooting 20 3 MAINTENANCE 27 4 DELIVERY SET 27 APPENDIX A Solubility of 100 humidity air oxygen in distilled water depending on the temperature 28 ...

Страница 4: ...tomatic temperature compensation with dip sensor with automatic calibration when the sensor is placed in the oxygen envi ronment air at temperatures varying between 15 С and 35 С with automatic adjustment for atmospheric pressure during calibration 1 2 Basic parameters 1 2 1 By resistance to climatic effects the analyzer version group is B4 in accordance with GOST 12997 84 1 2 2 By resistance to m...

Страница 5: ...d power supply two AA type alkaline batteries 1 2 10 Power consumption at a rated voltage of 2 8 V mW max 10 1 2 11 The analyzer retains its characteristics within the ranges set in the analyzer specifications after replacement of the sensor s spare parts batteries and calibration 1 2 12 The overall dimensions and weights of analyzer components are summarized in Table 1 1 below Table 1 1 Name and ...

Страница 6: ...erating temperature range from 1 to 50 С mg dm3 0 001 0 002C 1 3 5 Limits of the analyzer allowable additional absolute error in DOC measurement at surplus pressure of analytical environment up to 0 2 MPa mg dm3 0 1C 1 3 6 Limits of the analyzer allowable absolute error in DOC measurement at an analyte temperature coinciding with the calibration temperature which varies be tween 15 С and 35 С at a...

Страница 7: ... the analyte temperature The DOC values measured in mg dm3 or temperature measured in Celsius degrees depending on the measuring mode are displayed on the readout device a digital LCD display the display The minimum value of the least significant digit for DOC measurement is 0 001 mg dm3 The least significant digit value for temperature measurement is 0 1 С The analyzer is calibrated by atmospheri...

Страница 8: ...l voltage applied cross the electrodes In the process the sensor generates a DC signal which is at a fixed temperature proportional to DOC in the analyte The analyzer features a temperature sensor platinum thermal resistor to measure temperature and to automatically compensate for the temperature de pendence of the oxygen sensor signal The temperature sensor signal is supplied to the ADC input The...

Страница 9: ... bushing 15 covers the sensor electrode portion and is screwed into cable bushing 16 Fig 1 1а Cable 17 connects the sensor electrode assembly to the converter unit Protective cap 6 is made of plastic it is cylindrical form with slots and should be put on protective bushing 15 1 5 4 Functions of buttons on the converter unit front panel The analyzer front panel features the following buttons as sho...

Страница 10: ...r maintenance of the analyzer 2 mm cross screwdriver В 1 250 beaker КН 100 19 26 flask hydroquinone chemically pure sodium or potassium hydroxide chemically pure Instead of hydroquinone chemically pure and sodium or potassium hydrox ide chemically pure the following reagents may be used sodium sulphite Na2SO4 chemically pure potassium permanganate KMnO4 chemically pure ...

Страница 11: ...er should only be operated by personnel who are familiar with this manual and chemical handling safety rules in accordance with GOST 12 1 007 76 and GOST 12 4 021 75 2 2 2 The analyzer meets the requirements of Safety Class III to GOST R 52319 2005 The rated supply voltage varies between 2 2 and 3 4 V No protective earthing is required 2 2 3 By electromagnetic compatibility the analyzer meets the ...

Страница 12: ...rt blinking on the display use the MODE and ENTER buttons to set the hour value press the CAL button to complete time setting the analyzer goes into the time indication mode Switch on the analyzer and check if the display shows DOC or temperature readings in mg dm3 or sat or С respectively WARNING ALWAYS OBSERVE polarity when installing batteries Fail ure to meet this condition may damage the anal...

Страница 13: ...e outside air calibration mode Press the ENTER button The analyzer display will show DOC readings cor responding to the table of 100 humidity air oxygen solubility for analyzer measured temperatures with allowance for the atmospheric pressure at the time of calibration for example c8 38 mg dm3 Wait at least 8 s before pressing the ENTER button once again The donЕ caption will appear shortly on the...

Страница 14: ...eed as follows to carry out the cycling operation switch on the analyzer prepare a null solution as per para 2 3 3 2 submerge the sensor with its membrane down in the solution and move it to slightly agitate the solution in order to prevent air bubbles from amassing on the membrane hold the sensor in the null solution for 5 min then take it out shake off the solution drops from the membrane and ho...

Страница 15: ...e flask with a water layer 3 to 5 mm as shown in Fig 2 1 Position the flask at an angle of 30 to 45 to the horizontal for the remaining water to flow off the membrane Fig 2 1 Position of the sensor inside the flask for analyzer calibration Wait for 10 min before performing the outside air calibration steps which fol low 1 Press the CAL button twice The c1 character will appear on the display showi...

Страница 16: ...n and move it to slightly agitate the solution in order to prevent air bubbles from amassing on the membrane hold the sensor in the null solution for at least 40 min Perform the following steps to set the analyzer zero 1 Press CAL The analyzer display will show the с0 caption 2 Press ENTER The analyzer display will show DOC Z0 readings in the null solution without allowance for zero adjustment e g...

Страница 17: ...on which the membrane is fitted equalizes hydrostatic pressure of membrane assembly s intracavity and ambient medium In addition the measurements stay constant if oxygen concentration is constant independent of hydrostatic pressure WARNING Before measuring deeply check that membrane assembly is fully filled with electrolyte 2 4 3 Measuring in standard BOD flask While measuring in standard oxygen B...

Страница 18: ...submerge in the flask glass or plastic balls and stir arm circling the flask till the readout set about 2 min If values of dissolved oxygen decrease slowly and do not set in admitted time then there may be air bubbles on the membrane If so it is important while measuring in reservoir stir the probe harshly leaving it submerged in the water while measuring in BOD flask invert the flask with the pro...

Страница 19: ...6 45 0 0 0041 5 0 0 0060 16 0 0 0055 26 0 0 0049 36 0 0 0045 46 0 0 0040 6 0 0 0060 17 0 0 0054 27 0 0 0049 37 0 0 0045 47 0 0 0040 7 0 0 0060 18 0 0 0054 28 0 0 0049 38 0 0 0044 48 0 0 0039 8 0 0 0058 19 0 0 0053 29 0 0 0048 39 0 0 0044 49 0 0 0039 9 0 0 0058 20 0 0 0053 30 0 0 0048 40 0 0 0043 50 0 0 0038 10 0 0 0058 Exemplary calculation of correction factor Let Сsalt 10 g dm3 t 20 C thus ε 0 0...

Страница 20: ...humidity air oxygen in distilled water at temperature t С and normal atmospheric pressure of 101 325 кPa as per Ta ble A 1 mg dm3 Рatm atmospheric pressure as of the time of calibration kPa 2 6 Troubleshooting 2 6 1 The typical faults of the analyzer and remedial methods are summa rized in Table 2 2 In case of troubles set out in Table 2 2 proceed as recommended in the Remedy column in accordance ...

Страница 21: ...mbrane in water for 2 3 days without dismantling the sensor Defective membrane Para 2 6 4 Replace the membrane assembly Analyzer sensor off the outside air Position the sensor in air 5 Electrolyte leaking out fast Ruptured membrane Para 2 6 4 Replace the membrane assembly 6 1 Sharp change in and increased instability of ana lyzer readings 6 2 During analyzer calibra tion by outside air Е4 ex cess ...

Страница 22: ...g dm3 Operator s errors in an alyzer calibrations Para 2 6 6 Perform op erations to set initial ana lyzer parameters Broken analyzer Factory repair 10 During measurements Е8 is displayed on the screen Faulty temperature measuring channel heat probe breakage Factory repair 11 Е9 is displayed on the screen Writing error in ЕЕРRОМ memory Factory repair 2 6 2 Membrane cleaning The sensor membrane may ...

Страница 23: ...bly and holding it with the mem brane down inject electrolyte to fill two thirds of the volume taking care to avoid damaging the membrane While continuing to keep vertical the membrane assem bly filled with electrolyte set it on the bushing against the stop Screw in the protec tive bushing Cable bushing Protective bushing Bushing Remove Syringe filled with electrolyte Membrane assembly Case Capron...

Страница 24: ... in the null solution and longer time of response during DOC measurement Unscrew and remove the protective bushing from the sensor as per Fig 2 3 Remove the membrane assembly form the inner case and drain the electrolyte Check the teflon film for damage The film should be firmly pressed against the cathode in a wrinkle free man ner Damaged film should be replaced Once the teflon film is removed ch...

Страница 25: ...acid 80 to 100 Pour the solutions into vessels making sure that the liquid level is up to 3 mm Then proceed as follows remove the teflon film wash the sensor with distilled water place the sensor into a vessel with Solution 1 and hold it there for 1 h wash the sensor with distilled water place the sensor into a vessel with Solution 2 and hold it there also for 1 h WARNING NEVER PLACE the silver an...

Страница 26: ...s in mg dm3 with zero shift 2 6 6 2 Average slope setting 1 Switch off the analyzer 2 Press the CAL button and keeping it pressed switch on the analyzer Af ter a sound signal release the CAL button The screen will display с2 Press the CAL button again The screen will display с3 3 Press the ENTER button The donЕ capture will briefly appear on the screen and the analyzer will go into the measurement...

Страница 27: ...han 24 hours This operation ensures the highest response rate of the instrument in DOC measurements When the conditions described in para 2 5 are fulfilled the analyzer meets the specifications listed in para 1 3 4 DELIVERY SET 4 1 The delivery set is shown in Table 4 1 Table 4 1 Description Quantity 1 MAPK 302E dissolved oxygen analyzer with probe cable length 5 m 1 2 Protective cap 1 3 Spare par...

Страница 28: ...10 08 10 06 10 04 10 02 10 00 9 98 9 96 9 94 9 92 9 90 16 9 87 9 85 9 83 9 81 9 79 9 77 9 75 9 73 9 71 9 69 17 9 66 9 64 9 62 9 60 9 58 9 56 9 54 9 52 9 50 9 49 18 9 47 9 45 9 43 9 41 9 39 9 37 9 36 9 34 9 32 9 30 19 9 28 9 26 9 24 9 22 9 21 9 19 9 17 9 15 9 13 9 11 20 9 09 9 08 9 06 9 04 9 02 8 01 8 99 8 97 8 95 8 93 21 8 91 8 89 8 87 8 86 8 85 8 83 8 81 8 80 8 78 8 76 22 8 74 8 73 8 71 8 69 8 68...

Страница 29: ... 13 43 6 12 6 11 6 10 6 09 6 08 6 07 6 06 6 05 6 04 6 04 44 6 03 6 02 6 01 6 00 5 99 5 98 5 97 5 96 5 95 5 94 45 5 93 5 92 5 92 5 91 5 90 5 89 5 88 5 87 5 86 5 85 46 5 84 5 83 5 82 5 82 5 81 5 80 5 79 5 78 5 77 5 76 47 5 75 5 74 5 74 5 73 5 72 5 71 5 70 5 69 5 68 5 67 48 5 66 5 66 5 65 5 64 5 63 5 62 5 61 5 60 5 59 5 59 49 5 58 5 57 5 56 5 55 5 54 5 53 5 52 5 52 5 51 5 50 50 5 49 5 48 5 47 5 47 5 ...

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