Pine Research MSR 636A, Руководство пользователя

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DRU10002 (REV 004 / JAN 2017)
4.7.4 External Motor Stop Control 59
4.8 Circuit Protection 60
5 Electrodes 61
5.1 Electrode Handling Precautions 61
5.2 Shafts 65
5.3 RDE Tips 68
5.4 Single-Piece RDE Designs 74
5.5 RRDE Tips 76
5.6 15 mm OD RCE Tips 80
5.7 12 mm OD RCE Tips 81
6 Maintenance 82
6.1 Routine Cleaning 82
6.2 Brush Replacement 82
6.2.1 Internal Brush Replacement 82
6.2.2 Complete Brush Assembly Replacement 85
6.3 Lower Bearing Replacement 86
6.4 Removing the Motor-Coupling Assembly 87
6.5 Installing a New Motor-Coupling Assembly 91
Motor Control Cable Wiring 94
6.6 Rotation Rate Calibration 96
6.7 Changing the Input Rotation Rate Ratio 106
6.8 Changing the Motor Stop Signal Logic 108
7 Parts and Accessories 112
7.1 Mechanical Parts and Hardware 112
7.2 Power Cords 115
7.3 Power Supplies 118
8 Troubleshooting 121
9 Storage and Shipment 125
10 Theory 126
10.1 Forced Convection 126
10.2 Half Reactions 127
10.3 Voltammetry 128
10.3.1 Voltammogram Plotting Conventions 131
10.3.2 Measuring Limiting Currents 133
10.4 Rotating Disk Electrode (RDE) Theory 135
10.4.1 Levich Study 136
10.4.2 Koutecky-Levich Analysis 138
10.5 Rotating Ring-Disk Electrode (RRDE) Theory 140
10.5.1 Theoretical Computation of the Collection Efficiency 140
10.5.2 Empirical Measurement of the Collection Efficiency 142
10.5.3 Generator/Collector Experiments 143
10.5.4 Comparing Two Competing Pathways 144
10.6 Rotating Cylinder Electrode (RCE) Theory 145
10.7 References 146
11 Glossary 150