Koehler K71000 Скачать руководство пользователя страница 12

K71000 Automatic PMCC Flash Point Analyzer 

Operation and Instruction Manual 

 
 

K71000-Manual

    

 

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any  fumes  that  may  be  emitted  during  the  test. 
Conduct  tests  behind  a  safety  shield,  especially 
if  you  are  not  sure  of  the  flash  point  or  the 
ignition  temperature. Wear  appropriate  personal 
protective equipment (PPE) during testing.  
 

NOTE:

  ASTM  D93  specifically  notes  that 

a hood should not be operated during testing as 
excessive drafts can cause erroneous results! 
 
Exercise  caution  in  removing  and  replacing  the 
cup in the furnace. Hot surfaces and substances 
may cause injury if they come in contact with the 
operator. 
 
All  connections  should  be  properly  made  and 
tested for leaks prior to carrying out the tests. 
 
The ignition gas source should be equipped with 
a proper safety regulator capable of delivering a 
maximum  of  5  psi  of  pressure  to  the  test  flame 
assembly.  Some  propane  regulators  give 
pressure  in  inches  of  water  (inH

2

0)  at  60°F.  A 

standard  11  inches  of  water  (inH

2

0)  regulator 

should  give  sufficient  gas  for  normal  use.  
Minimum  pressure  required  is  about  7  kPa  or 
1.0 psi. 
 
The flame suppression (inert gas) source should 
be  regulated  to  between  20  and  30  psi  for  safe 
use. 
 

2.9 

Other Important Hazards 

 

Working  surfaces  on  the  instrument  may 
become  hot  enough  to  produce  severe  burns 
even with momentary contact.   
 
Open  flames  and  electrically  heated  resistance 
elements  are  present.    Direct  momentary 
contact can cause severe burns. 
 
The  draft  shield  around  the  sample  area  also 
functions  as  a  mechanical  guard.    The 
instrument should never be used if this guard is 
removed.  
 

WARNING:

 

Electrical hazards exist inside 

the  instrument  case.    Lethal  voltages  and 
current  are  present.    Only  factory  authorized  or 
otherwise  qualified  personnel  may  repair  or 
service this  instrument.  Only original parts may 
be  used  for  repair.    No  substitution  parts  or 

alterations  to  this  equipment  are  allowed;  doing 
so may void the warranty. 

 

PC Motherboard

 

WARNINGS

 

-  Due  to  high  voltages  inside  the  instrument, 

under no circumstances should the instrument 
be  opened  or  access  covers  removed  while 
energized. 

-  Lethal  voltages  are  present  inside  power 

supplies.    Under  no  circumstances  should 
Power  Supply  covers  be  removed.  Power 
Supply  warranties  are  voided  once  the  cover 
is removed. 

-  For  indoor  use  only.    Please  operate  the 

power supply in a safe and dry environment. 

-  Do  not  insert  any  objects  into  the  open 

ventilation or fan grill area of the power supply. 

 

3  Getting Started 

 

The  instructions  for  preparing  the  equipment 

assume that the user is aware of the contents of 
this  document,  which  lists  the  warranty 
conditions and important precautions.

 

 

3.1 

Packing List 

 

 

K71000 Automatic PMCC Flash Point 
Analyzer, 115/230V 50/60Hz 

 

Brass Test Cup with Handle 

 

Combination Gas/Electric Igniter 

 

Stirrer Shaft and Blade Assembly 

 

PT-100 Temperature Probe / Thermal 
Detector 

 

Ionization Detector 

 

Cover Assembly 

 

Draft Shield 

 

Stylus 

 

Temperature Calibration Cable 

 

Power Cords, 115V & 230V 

 

K71000-Manual K71000 Automatic PMCC 
Flash Point Analyzer Operation and 
Instruction Manual 
 

Installed in the K71000 

 

 

Panel PC and Microprocessor Controllers 

 

Operating  Software,  Instruction  Manual 
PDF, Recovery Software on Hard Disk Drive 

 

Thermocouple and Ionization Detection 

 

Fire Sensing  and Suppression System 

 

Collision / Interference Detection 

 

Mechanical Lift System 

 

Dual Fan Cooling System 

Содержание K71000

Страница 1: ...enue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 http www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing Analysis...

Страница 2: ......

Страница 3: ...e statement is given cataloging the items that require separation from the equipment along with basic information on subsequent processing or recycling prior to disposal of the equipment http www dpa...

Страница 4: ...As a minimum the following substances preparations and components have to be removed from any separately collected WEEE Mercury containing components such as switches or backlighting lamps compact fl...

Страница 5: ...Safety Considerations 8 2 2 Unit Design 8 2 3 Contaminated Samples 9 2 4 Safe Quick Test Method 9 2 5 Fire Detection Suppression and Draft Shield Dome System 9 2 6 Equipment Modification and Replacem...

Страница 6: ...ility for losses arising from the negligent or improper use of our equipment nor for losses arising from the improper use or use other than intended Only deliberate action or gross negligence are grou...

Страница 7: ...ng needs Our products are backed by our staff of technically knowledgeable trained specialists who are experienced in both petroleum products testing and instrument service to better understand your r...

Страница 8: ...The scope of the method covers the analysis of products in the temperature range of 40 to 360 C but this automated apparatus extends the range from dew point 10 C to 400 C Internet Link to Summary AST...

Страница 9: ...ange Ambient to 405 C 761 F Flash Detection System Differential Thermocouple Ionization Detection Stirring Speed 0 to 300 RPM Heating Rate In accordance to ASTM D93 procedure A B C Quick Test 12 C min...

Страница 10: ...fety problems associated with the use of this equipment It is the responsibility of any user of this equipment to investigate research and establish appropriate safety and health practices and determi...

Страница 11: ...prescribed end point prior to running a quick test The set maximum run temperature is solely at the user s discretion We recommend this method of screening for ALL samples 2 5 Fire Detection Suppress...

Страница 12: ...emoved WARNING Electrical hazards exist inside the instrument case Lethal voltages and current are present Only factory authorized or otherwise qualified personnel may repair or service this instrumen...

Страница 13: ...r claim if requested When submitting a claim for shipping damage request that the carrier inspect the shipping container and equipment Do not return goods to Koehler without written authorization 3 3...

Страница 14: ...results outside the above mentioned criteria Ventilation A fume hood or exhaust system is required after performing a test Flammable vapors and or steam are generated during operation and must not be...

Страница 15: ...K71000 Automatic PMCC Flash Point Analyzer Operation and Instruction Manual K71000 Manual 13 4 Descriptions 4 1 Front of Instrument Figure 1 Instrument Descriptions_Front...

Страница 16: ...load factory software updates 4 Touch Screen Control Panel Main control point of instrument Please refer to section _ _ for full operational details 5 Leveling Feet To make adjustments to instrument l...

Страница 17: ...K71000 Automatic PMCC Flash Point Analyzer Operation and Instruction Manual K71000 Manual 15 4 2 Back of Instrument Figure 2 Instrument Descriptions_Back...

Страница 18: ...reen control panel 15 USB Port For connection to Keyboard or Mouse 16 RS232 Port For connection to external PC 17 Ethernet Port For connection to LIMS system 18 CPU Port For programming of internal CP...

Страница 19: ...etection thermocouple will automatically detect this and initiate re lighting of the flame 27 Pilot Flame The pilot flame ensures the test flame is lit prior to each test dip 28 Electric Ignitor Alter...

Страница 20: ...orities Key The fourth or factory level is designed for administrative purposes only and specifically allows for access to the factory settings menu From this screen the user can also Change User Pass...

Страница 21: ...t the which operations they want a particular user level to have access to The user can choose to turn on or off access to the Diagnostics Calibration and Custom Test Menus Click Save when complete Fi...

Страница 22: ...eset all global parameter settings back to the factory default Figure 7 Last Global Parameter Pop Up 5 Main Home Screen After clicking Yes or No to the Last Global Parameter pop up the user will be br...

Страница 23: ...d to a Laboratory LIMS system by clicking this button Print This function is only accessible when the user is in the results database screen Data can be sent to a printer by clicking this button Save...

Страница 24: ...dard Test Parameters Change Save minimum temperature in which the instrument lift can open safely and the temperature in which the cooling fan can be turned off Inst ID Setup Change Save Instrument ID...

Страница 25: ...Graph Tools The Graph screen features the following functions a Zoom In b Zoom Out c Pan XY Provides cursor that can be moved along graph and display data d Restore Resets X and Y Axis to default posi...

Страница 26: ...Dip Home Brings flame dip mechanism to home position b Find Lift Home Brings mechanical lift to Home Position also considered test position c Clean Position Brings mechanical lift to Clean Position h...

Страница 27: ...med Two Point Calibration RTD Correction Table User CRM Calibration Two Point Calibration as shown in Figure 14 below is performed using an external PT100 Simulator Box Available as an Additional Acce...

Страница 28: ...in which the user can input offset values for any of temperature values shown This table is particularly convenient for those with Certified Digital Contact Thermometers or Certified Liquid in Glass...

Страница 29: ...Material CRM samples using a Gas Ignition source 1 Input the certified flash point value from the CRM bottle label or test certificate into the first column titled CRM Flash Value 2 Perform a series...

Страница 30: ...erial CRM samples using the Electrical Ignition Source 1 Input the certified flash point value from the CRM bottle label or test certificate into the first column titled CRM Flash Value 2 Perform a se...

Страница 31: ...ric Pressure Correction Feature As pictured in Figure 18 below the user can Enter Atmospheric Pressure in Kilopascals kPa into the empty field The Measured Barometric Pressure is determined by the ana...

Страница 32: ...C value as pictured in Figure 19 below This method of calibration is useful when a material of known flash point is tested and the analyzer is displaying a value greater than the known value e g know...

Страница 33: ...RPM Heating Rate C min End Test Temperature EFP X C Fan Off Temperature C Pre Heat Limit Temperature C Pre Heat Ramp Rate C min Open Lift Temperature C Soak Temperature C Typically used only for Aspha...

Страница 34: ...parameter data will automatically be sent to the database Each test is listed in a single row with the information separated by column The user also has the option to delete or update the database lis...

Страница 35: ...and clicking on the Print button will cause a temporary Print Result Screen to appear followed by a Printer Options Menu See Figures 22 and 23 below Once the appropriate printer is selected click the...

Страница 36: ...n the user first enters this menu the display screen will be blank Clicking on the Monitor Traffic box will begin displaying the data communication At this time a screenshot can be taken of the curren...

Страница 37: ...for a Test Dip The Dip On Off Switch will activate or deactivate the dipping mechanism b Adjust Lift Mechanism Pressing the Up and Down Arrows will adjust the level at which the Lift Mechanism will b...

Страница 38: ...d See Figure 26 below The corrected flash point value is prominently displayed at the center of the screen Additionally the Type of Ignition used to perform the test is displayed as well as the Sensor...

Страница 39: ...authorize the return of the product to the factory The sole responsibility of Koehler Instrument Company and the purchaser s exclusive remedy for any claim arising out of the purchase of any product i...

Страница 40: ...K71000 Automatic PMCC Flash Point Analyzer Operation and Instruction Manual K71000 Manual 38 Notes...

Страница 41: ...K71000 Automatic PMCC Flash Point Analyzer Operation and Instruction Manual K71000 Manual 39 Notes...

Страница 42: ...K71000 Automatic PMCC Flash Point Analyzer Operation and Instruction Manual K71000 Manual 40 Notes...

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