Koehler K71000 Скачать руководство пользователя страница 11

K71000 Automatic PMCC Flash Point Analyzer 

Operation and Instruction Manual 

 
 

K71000-Manual

    

 

-

9-

 

 

acceptance  of  this  instrument  signifies  that  the 
purchasing  company  and  their  agents,  the  end 
users,  are  responsible  for establishing  all  safety 
and 

health 

practices 

and 

assumes 

full 

responsibility  for  safely  using  the  K71000 
Automatic PMCC Flash Point Analyzer. 
 

2.3 

Contaminated Samples  

 

Samples  contaminated  with  light  ends  (highly 
volatile  petroleum  products)  may  light  and 
continue  burning  when  the  expected  flash  point 
is  set  above  the  fire  point  of  the  material.  In 
addition,  burning  material  may  be  ejected 
through  the  ignition  aperture  in  the  test  cup 
cover.  For  this  reason, the most  recent  updates 
to  ASTM  D93  require  a  first  application  of 
ignition  at  ambient  temperature  (<24°C  below 
EFP)  and  every  10°C.    This  helps  when  the 
contaminant  flashes  at  room  temperature  but 
does not address all contamination situations. 
   
Samples contaminated with water can bump and 
eject  hot  and  flammable  material  from  the  test 
cup. 
 
At all times, refrain from leaning or bending over 
the  test  cup  when  the  test  is  being  carried  out. 
An unexpected flash can cause serious injury to 
exposed body parts that are in close proximity to 
the  test  area.    Ejected  material  may  cause 
serious harm. 
 

2.4 

Safe Quick Test Method 

 

The  K71000  has  a  quick  test  option  that  begins 
testing  at  ambient  then  heats  the  sample  at  an 
accelerated  pace  while  applying  the  igniter  at 
3°C  increments.    The  detected  flash  is  an 
estimate  of  the  expected  flash  point  which  is 
then used in a subsequent run (under prescribed 
standard  test  conditions)  to  safely  arrive  at  the 
flash  point.    The  only  disadvantage  of  this 
screening  method  is  that  it  requires  additional 
time  and  material  to  complete  a  safe  analysis.  
The  Maximum  Quick  Test  Temperature  is  370 
°C.  
 

NOTE:

  The  user  must  set  this  prescribed  end 

point  prior  to  running  a  quick  test.  The  set 
maximum run temperature is solely at the user's 
discretion.  

 
We recommend this method of screening for 
ALL samples. 

2.5 

Fire  Detection  /  Suppression  and  Draft 
Shield / Dome System 

 

The  K71000  comes  standard  with  a  fire 
detection and inert gas fire suppression system. 
This system is designed to flood the sample cup 
area  with  an  inert  gas,  extinguishing  sample 
based  fires.    The  system  is  triggered  when  a 
high  temperature  event  melts  the  thermal  fuse.  
The  open  circuit  condition  triggers  the  flame 
suppression  system.    The  electronics  are 
extremely  fast  relying  solely  on  electronic  logic 
(no  software).    The  flame  suppression  system 
also shuts off the ignition gas source, closes the 
cup  cover  by  de-energizing  the  motor,  and  de-
energizes the electric igniter if in use. 

 

WARNING:

 

Never operate the instrument 

without  the  draft  shield  make  it  difficult  to 
inadvertently touch hot working surfaces. 
 

2.6 

Equipment 

Modification 

and 

Replacement Parts 

 

Any  modification  or  alteration  of  this  equipment 
from  that  of  factory  specifications  is  not 
recommended  and  voids  the  manufacturer 
warranty, 

product 

safety, 

performance 

specifications,  and/or  certifications  whether 
specified  or  implied,  and  may  result  in  personal 
injury  and/or  property  loss.  Replacement  parts 
must be O.E.M. exact replacement equipment. 
 

2.7 

Chemical Reagents Information 

 

Chemicals  and  reagents  used  in  performing  the 
test  may  exhibit  potential  hazards.  Any  user 
must  be  familiarized  with  the  possible  dangers 
before  use. We  also  recommend  consulting  the 
Material Data and Safety Sheet (MSDS) on each 
chemical  reagent  for  additional  information. 
MSDS  information  can  be  easily  located  on  the 
internet at http://siri.uvm.edu or 

http://www.sigma-aldrich.com

 

2.8 

Additional Important Safety Information 

 

WARNING:

  As  an  important  safety 

precaution, 

NEVER 

use  unregulated  gas  with 

the  K71000  Pensky-Martens  Closed  Cup  Flash 
Point Analyzer!   
 
Use  in  an  area  that  is  adequately  ventilated, 
preferably with an exhaust tube / pipe to remove 

Содержание K71000

Страница 1: ...enue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 http www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing Analysis...

Страница 2: ......

Страница 3: ...e statement is given cataloging the items that require separation from the equipment along with basic information on subsequent processing or recycling prior to disposal of the equipment http www dpa...

Страница 4: ...As a minimum the following substances preparations and components have to be removed from any separately collected WEEE Mercury containing components such as switches or backlighting lamps compact fl...

Страница 5: ...Safety Considerations 8 2 2 Unit Design 8 2 3 Contaminated Samples 9 2 4 Safe Quick Test Method 9 2 5 Fire Detection Suppression and Draft Shield Dome System 9 2 6 Equipment Modification and Replacem...

Страница 6: ...ility for losses arising from the negligent or improper use of our equipment nor for losses arising from the improper use or use other than intended Only deliberate action or gross negligence are grou...

Страница 7: ...ng needs Our products are backed by our staff of technically knowledgeable trained specialists who are experienced in both petroleum products testing and instrument service to better understand your r...

Страница 8: ...The scope of the method covers the analysis of products in the temperature range of 40 to 360 C but this automated apparatus extends the range from dew point 10 C to 400 C Internet Link to Summary AST...

Страница 9: ...ange Ambient to 405 C 761 F Flash Detection System Differential Thermocouple Ionization Detection Stirring Speed 0 to 300 RPM Heating Rate In accordance to ASTM D93 procedure A B C Quick Test 12 C min...

Страница 10: ...fety problems associated with the use of this equipment It is the responsibility of any user of this equipment to investigate research and establish appropriate safety and health practices and determi...

Страница 11: ...prescribed end point prior to running a quick test The set maximum run temperature is solely at the user s discretion We recommend this method of screening for ALL samples 2 5 Fire Detection Suppress...

Страница 12: ...emoved WARNING Electrical hazards exist inside the instrument case Lethal voltages and current are present Only factory authorized or otherwise qualified personnel may repair or service this instrumen...

Страница 13: ...r claim if requested When submitting a claim for shipping damage request that the carrier inspect the shipping container and equipment Do not return goods to Koehler without written authorization 3 3...

Страница 14: ...results outside the above mentioned criteria Ventilation A fume hood or exhaust system is required after performing a test Flammable vapors and or steam are generated during operation and must not be...

Страница 15: ...K71000 Automatic PMCC Flash Point Analyzer Operation and Instruction Manual K71000 Manual 13 4 Descriptions 4 1 Front of Instrument Figure 1 Instrument Descriptions_Front...

Страница 16: ...load factory software updates 4 Touch Screen Control Panel Main control point of instrument Please refer to section _ _ for full operational details 5 Leveling Feet To make adjustments to instrument l...

Страница 17: ...K71000 Automatic PMCC Flash Point Analyzer Operation and Instruction Manual K71000 Manual 15 4 2 Back of Instrument Figure 2 Instrument Descriptions_Back...

Страница 18: ...reen control panel 15 USB Port For connection to Keyboard or Mouse 16 RS232 Port For connection to external PC 17 Ethernet Port For connection to LIMS system 18 CPU Port For programming of internal CP...

Страница 19: ...etection thermocouple will automatically detect this and initiate re lighting of the flame 27 Pilot Flame The pilot flame ensures the test flame is lit prior to each test dip 28 Electric Ignitor Alter...

Страница 20: ...orities Key The fourth or factory level is designed for administrative purposes only and specifically allows for access to the factory settings menu From this screen the user can also Change User Pass...

Страница 21: ...t the which operations they want a particular user level to have access to The user can choose to turn on or off access to the Diagnostics Calibration and Custom Test Menus Click Save when complete Fi...

Страница 22: ...eset all global parameter settings back to the factory default Figure 7 Last Global Parameter Pop Up 5 Main Home Screen After clicking Yes or No to the Last Global Parameter pop up the user will be br...

Страница 23: ...d to a Laboratory LIMS system by clicking this button Print This function is only accessible when the user is in the results database screen Data can be sent to a printer by clicking this button Save...

Страница 24: ...dard Test Parameters Change Save minimum temperature in which the instrument lift can open safely and the temperature in which the cooling fan can be turned off Inst ID Setup Change Save Instrument ID...

Страница 25: ...Graph Tools The Graph screen features the following functions a Zoom In b Zoom Out c Pan XY Provides cursor that can be moved along graph and display data d Restore Resets X and Y Axis to default posi...

Страница 26: ...Dip Home Brings flame dip mechanism to home position b Find Lift Home Brings mechanical lift to Home Position also considered test position c Clean Position Brings mechanical lift to Clean Position h...

Страница 27: ...med Two Point Calibration RTD Correction Table User CRM Calibration Two Point Calibration as shown in Figure 14 below is performed using an external PT100 Simulator Box Available as an Additional Acce...

Страница 28: ...in which the user can input offset values for any of temperature values shown This table is particularly convenient for those with Certified Digital Contact Thermometers or Certified Liquid in Glass...

Страница 29: ...Material CRM samples using a Gas Ignition source 1 Input the certified flash point value from the CRM bottle label or test certificate into the first column titled CRM Flash Value 2 Perform a series...

Страница 30: ...erial CRM samples using the Electrical Ignition Source 1 Input the certified flash point value from the CRM bottle label or test certificate into the first column titled CRM Flash Value 2 Perform a se...

Страница 31: ...ric Pressure Correction Feature As pictured in Figure 18 below the user can Enter Atmospheric Pressure in Kilopascals kPa into the empty field The Measured Barometric Pressure is determined by the ana...

Страница 32: ...C value as pictured in Figure 19 below This method of calibration is useful when a material of known flash point is tested and the analyzer is displaying a value greater than the known value e g know...

Страница 33: ...RPM Heating Rate C min End Test Temperature EFP X C Fan Off Temperature C Pre Heat Limit Temperature C Pre Heat Ramp Rate C min Open Lift Temperature C Soak Temperature C Typically used only for Aspha...

Страница 34: ...parameter data will automatically be sent to the database Each test is listed in a single row with the information separated by column The user also has the option to delete or update the database lis...

Страница 35: ...and clicking on the Print button will cause a temporary Print Result Screen to appear followed by a Printer Options Menu See Figures 22 and 23 below Once the appropriate printer is selected click the...

Страница 36: ...n the user first enters this menu the display screen will be blank Clicking on the Monitor Traffic box will begin displaying the data communication At this time a screenshot can be taken of the curren...

Страница 37: ...for a Test Dip The Dip On Off Switch will activate or deactivate the dipping mechanism b Adjust Lift Mechanism Pressing the Up and Down Arrows will adjust the level at which the Lift Mechanism will b...

Страница 38: ...d See Figure 26 below The corrected flash point value is prominently displayed at the center of the screen Additionally the Type of Ignition used to perform the test is displayed as well as the Sensor...

Страница 39: ...authorize the return of the product to the factory The sole responsibility of Koehler Instrument Company and the purchaser s exclusive remedy for any claim arising out of the purchase of any product i...

Страница 40: ...K71000 Automatic PMCC Flash Point Analyzer Operation and Instruction Manual K71000 Manual 38 Notes...

Страница 41: ...K71000 Automatic PMCC Flash Point Analyzer Operation and Instruction Manual K71000 Manual 39 Notes...

Страница 42: ...K71000 Automatic PMCC Flash Point Analyzer Operation and Instruction Manual K71000 Manual 40 Notes...

Отзывы: