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23

Appendix A

APPENDIX A - CONE NUMBERS, SAMPLE SIZES, VISCOSITY RANGES

CAP 1000 AND 2000 VISCOMETERS

Cone

Number

1

Shear Rate

(sec

-1

)

Sample Size

(micro liters)

Calibrating Fluid

Low Temp Cap at 25°C

Calibrating Fluid

High Temp Cap at 60°C

Part No.

*Viscosity

Part No.

*Viscosity

01

13.33N

67

CAP1L

89 cP

CAP1H

89 cP

02

13.33N

38

CAP2L

177 cP

CAP2H

177 cP

03

13.33N

24

CAP3L

354 cP

CAP3H

354 cP

04

3.33N

124

CAP4L

708 cP

CAP4H 

708 cP

05

3.33N

67

CAP5L

1417 cP

CAP5H

1417 cP

06

3.33N

32

CAP6L

3542 cP

CAP6H 

3542 cP

07

2N

1700

CAP7L

1328 cP

CAP7H

1328 cP

08

2N

400

CAP8L

5313 cP

CAP8H

5313 cP

09

2N

100

CAP9L

21,250 cP

CAP9H

21,250 cP

10

5N

170

CAP10L

236 cP

CAP10H

236 cP

N = RPM

*Approximate Value

Table A-1

CAP 1000 VISCOSITY RANGES (POISE)

Cone

Number

1

750 RPM

900 RPM

Cone Range

Coefficient 

Cone Angle

(degrees) 

Cone Radius

(cm) 

01

0.25 - 2.5

0.21 - 2.08

1,875

0.45

1.511

02

0.5 - 5.0

0.42 - 4.17

3,750

0.45

1.200

03

1.0 - 10.0

0.83 - 8.33

7,500

0.45

0.953

04

2.0 - 20.0

1.67 - 16.67

15,000

1.8

1.200

05

4.0 - 40.0

3.33 - 33.33

30,000

1.8

0.953

06

10.0 - 100.0

8.33 - 83.33

75,000

1.8

0.702

07

0.42 - 4.2

0.347 - 3.47

3,150

3.0

2.399

08

1.67 - 16.7

1.39 - 13.9

12,500

3.0

1.511

09

6.67 - 66.7

5.56 - 55.6

50,000

3.0

0.953

10

0.667 - 6.67

0.556 - 5.56

5,000

1.2

1.511

Table A-2

Содержание CAP 1000+

Страница 1: ...Additives Instruments A member of Measure what you see CAP 1000 Viscometer Manual...

Страница 2: ......

Страница 3: ...8 D 82538 Geretsried Germany Tel 0 800 gardner 0 800 4273637 49 8171 3493 0 Fax 49 8171 3493 140 BYK Gardner USA 9104 Guilford Road Columbia MD 21046 USA Phone 800 343 7721 301 483 6500 Fax 800 394 82...

Страница 4: ...Therefore in addition to our products we offer many VALUE ADDED services Technical Sales Force Technical Application Support Application and Technical Seminars Repair Certification Service BYK Gardner...

Страница 5: ...II 2 Cone Spindle Selection and Setting 14 II 3 Speed Setting 16 II 4 Temperature Control Setting 16 II 5 Hold Time Settings 17 II 6 Run Time 17 II 7 Printing 17 II 8 Run and Stop Keys 18 III OPERATIO...

Страница 6: ...6...

Страница 7: ...e control of sample is possible between either 5 C or 15 C below ambient whichever is higher and 75 C or 50 C and 235 C depending on viscometer model The CAP1000 can also be ordered with a single cust...

Страница 8: ...to be sure that you have received all components and that there is no damage If you are missing any parts please notify BYK Gardner or your local BYK Gardner representative immediately Any shipping da...

Страница 9: ...pindles and temperature plates are made of tungsten carbide Operating Environment CAP 1000 Viscometers must be operated within the following ambient temperatures 5 C 41 F to 40 C 149 F and humidity 20...

Страница 10: ...irements match your power source BEFORE connecting it to power The AC input voltage and frequency must be within the appropriate range as shown on the name plate of the viscometer NOTE The CAP Viscome...

Страница 11: ...the manual for specific warning or caution information to avoid personal injury or damage to the instrument SAFETY OVERVIEW If this instrument is used in a manner not specified by the manufacturer the...

Страница 12: ...Stops cone spindle rotation at any time Exits data entry field DELETE Overwrites entered data PRINT Sends data to the parallel port RUN Starts spindle rotation and measurement RUN TIME Selects time en...

Страница 13: ...ge condition If the viscometer settles out with a final reading below zero negative values will be displayed Temperature is displayed in C degrees centigrade I 8 Cleaning Instrument Keypad Painted Sur...

Страница 14: ...pressing the STOP key during instrument power up The CAP 1000 can be configured to operate at 750 RPM or 900 RPM This selection is set by choosing 1 SPEED in the special functions screen then selecti...

Страница 15: ...viscometer calculations The screen will display the following message Spindle 04 CALIBRATE YES NO Figure II 3 Normally there is no requirement to perform a cone calibration Cones supplied at the time...

Страница 16: ...The default temperature on start up is 25 0 C on low temperature models and 50 C on high temperature models The temperature ranges are Low temperature 5 C or 15 C below ambient whichever is higher to...

Страница 17: ...time of zero sets the viscometer to infinite run mode In this mode the spindle will rotate at the set speed for as long as the RUN button is pressed When the RUN key is released the spindle will stop...

Страница 18: ...imer setting 3 Used in executing a cone calibration The STOP key has three functions 1 Stops the cone rotation at any time 2 Pressing and holding the STOP ESCAPE key during power up selects the viscos...

Страница 19: ...er for accuracy information for CAP spindles 07 10 Table III 1 Accuracy of Viscosity Measurement CAP 1000 L VISCOMETERS Cone FULLSCALE VISCOSITY RANGE ACCURACY 750 RPM 900RPM Over 900 RPM to 1000 RPM...

Страница 20: ...viscosity measurement With the viscometer on a clean level surface connect it to the proper power supply Section I 4 1 Turn the power switch ON Section II 1 The procedure assumes that the following li...

Страница 21: ...e about 1 0 mm see table A 1 for sample size 3 Release the solvent trap placing it onto the plate over the cone so it does not touch the cone shaft The user should ensure that the substances placed un...

Страница 22: ...n the test conditions and viscosity results from the viscometer display 10 Relocate the solvent trap onto the cone adapter and raise the handle 11 It is recommended to remove the cone for cleaning How...

Страница 23: ...700 CAP7L 1328 cP CAP7H 1328 cP 08 2N 400 CAP8L 5313 cP CAP8H 5313 cP 09 2N 100 CAP9L 21 250 cP CAP9H 21 250 cP 10 5N 170 CAP10L 236 cP CAP10H 236 cP N RPM Approximate Value Table A 1 CAP 1000 VISCOSI...

Страница 24: ...viscosity range FSR for any cone speed divide the Cone Range Coefficient refer to Table A2 by the rotational speed RPM Full Scale Viscosity Range Poise Cone Range Coefficient Equation A1 RPM CAP 1000...

Страница 25: ...l scale viscosity range at 750 RPM Full Scale Viscosity Range poise 3 750 5 00 poise 750 Using Equation A5 determine the viscosity at 73 8 of full scale range Viscosity poise 5 00 poise x 73 8 3 69 po...

Страница 26: ...on INTERPRETATION OF CALIBRATION TEST RESULTS When verifying the calibration of the CAP 1000 the instrument and viscosity standard fluid error must be combined to calculate the total allowable error T...

Страница 27: ...solvent trap NOTE The solvent trap must be utilized when calibrating to ensure proper temperature control 7 Select the spindle to be calibrated by using the SPINDLE key 8 Select YES for CALIBRATE and...

Страница 28: ...cosity The SMC and SRC must be entered after entering the spindle number 11 20 and selecting YES 1 for calibration Follow the screen prompts Once SMC and SRC are entered follow the procedure described...

Страница 29: ...Rate range they are measured Non Newtonian These fluids have different viscosities at different shear rates different RPMs They fall into two groups 1 Time Independent non Newtonian 2 Time Dependent...

Страница 30: ...000 rpm the two viscosity values produced may be different because the readings were made at different shear rates The faster the spindle speed the higher the shear rate The shear rate of a given mea...

Страница 31: ...ipping damage The Viscometer should be shipped in its carrying case together with all spindles originally provided with the instrument For repair or service return to one of the locations listed below...

Страница 32: ...199 024 584 E 1610...

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