2
Biotage
®
Flash 75/150 User Manual | © Biotage 2018
Contents
Biotage
®
Flash 75/150
User Manual
CONTENTS
1
Introduction
1
Speed
1
Safety
1
Performance
2
System Components
2
Prepacked Biotage
®
Flash Cartridge
2
Radial Compression Module
3
AM-190 Manifold
4
Solvent Reservoir
4
Sample Injection Module (Biotage
®
SIM) Kit
5
Grounding Kit
5
Start-Up Kit
5
Cartridge Extraction Tool
6
Chemical Resistance
7
Safety
7
Intended Use
7
Education, Training, and Competence
7
Warranty and Liability
7
Service
7
Labels
7
Safety Requirements
9
Installation
9
Set Up the Radial Compression Module
9
Set Up the AM-190 Manifold
9
Set Up the Sample Injection Module (Biotage
®
SIM)
10
Set Up the Solvent Reservoir
10
Attach the Inert Gas Supply and Solvent Lines
12
Ground the System
14
How to Use the system
14
Fill the Solvent Reservoir
14
Insert a Flash Cartridge
15
Pressurize the Radial Compression
Module and the Solvent Reservoir
15
Equilibrate the Cartridge
16
Load Sample and Collect Fractions
18
Refill the Solvent Reservoir
18
Empty the Solvent Reservoir
18
Depressurize the Radial Compression Module
and Remove the Used Cartridge
19
Clean the Sample Injection Module (Biotage
®
SIM)
20
Troubleshooting
20
AM-190 Manifold
20
Biotage
®
Flash 75/150 Radial Compression Module
21
Operation
21
Sample Injection Module (Biotage
®
SIM)
21
Solvent Reservoir
22
Optimizing Flash Separations
22
Column Separations are Governed by ΔCV, not ΔR
f
22
Vary Solvent Strength to Maintain
R
f
Values Between 0.15 and 0.40
23
Vary Solvent Selectivity to Maintain
R
f
Values Between 0.15 and 0.40
24
The Relationship Between the Size of a Column
and the Sample Load is Dependent on ΔCV
25
Flash Chromatography Workbook
31
General Information
31
Price List and Ordering Information
31
Download User Documentation
31
Manufacturer
31
Contact Us
32
Notes
Содержание Flash 150
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