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Operation

46

Waltron User Manual 101-046-B.3
9096 Degassed Cation Conductivity Analyzer

saving any changes
that were made.

The entire procedure
above can be repeated
for the Cation
Conductivity sensor.

Note: the DC sensor
relies on the CC sensor
calibration and does not
need to be calibrated
individually.

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Summary of Contents for 9096

Page 1: ...101 046 B 3 EXPERTS IN WATER CHEMISTRY SINCE 1903 9096 Degassed Cation Conductivity Analyzer User Manual...

Page 2: ...908 534 5546 www waltron net Please be ready to provide the following information Date analyzer was purchased Analyzer model and serial number Recent maintenance history Calibration slope values and d...

Page 3: ...enclosures containers packages and chemicals Only qualified personnel should be involved in the installation operation and servicing of the analyzer Follow safety precautions when operating analyzer...

Page 4: ...ron Technical Service Department Customer name address and department Name and telephone number of the individual responsible for returning items for repair Brief problem description Ship to Waltron s...

Page 5: ...uture moving and shipping needs Check all items received against those on the packing list Chemicals are usually shipped in a separate package and will be itemized accordingly Verify that the number o...

Page 6: ...mple 10 1 2 4 Analyzer General Hazards 10 2 Introduction 11 2 1 Preliminary Remarks 11 2 2 Working Principle 11 2 3 Flow Component Diagram 13 2 4 Wet Section 14 2 5 Electronics 14 3 Installation 15 3...

Page 7: ...vigation 29 5 4 Alarm Log 31 5 4 1 Analog Outputs 32 5 4 2 Calibration Menu 38 5 5 Configuration 41 5 5 1 Temperature Compensation 41 6 Operation 43 6 1 Calibration 43 7 Maintenance 47 7 1 Scheduled M...

Page 8: ...mple Stainless steel PVC Power Supply AC 110 to 240 V 10 15 48 to 63 Hz or AC DC 20 to 30 V 48 to 63 Hz Required Maintenance Replace Cation Resin Bottle monthly Replace Decarbonization Column monthly...

Page 9: ...ll the national and local regulations and laws regarding workers health and safety Use maintenance and service of this analyzer is allowed only by qualified personnel who are fully trained on the anal...

Page 10: ...sconnect input power to analyzer before servicing Hazard of chemical burns This symbol is used to present a hazard of severe burns and serious injury for dangerous chemicals manipulation All handling...

Page 11: ...1 2 4 1 Electrical Hazards and Precautions General information In all electrical devices that are 110 220 Vac powered there is a hazard of electrical shock or electrocution Only qualified service per...

Page 12: ...et production goals The conductivity measurements in power plants provide indispensable information about the state of the water steam circuit Specific conductivity can be used to infer the pH and Amm...

Page 13: ...on dioxide from the sample In this way the CO2 contribution is removed from the cation conductivity The removal of carbon dioxide is carried out in an exchange column using a counterflow principle The...

Page 14: ...Introduction 13 Waltron User Manual 101 046 B 3 9096 Degassed Cation Conductivity Analyzer 2 3 FLOW COMPONENT DIAGRAM Figure 2 1 Flow Component Diagram...

Page 15: ...ssembly are located in the electronic section It provides control for the entire analyzing system It handles the analyzer operations it collects all the information and data coming from the different...

Page 16: ...manually empty all of the liquid containing components 3 3 LOCATION AND MOUNTING It is recommended to install the analyzer in a suitable position The location is to be clean covered and properly enclo...

Page 17: ...Installation 16 Waltron User Manual 101 046 B 3 9096 Degassed Cation Conductivity Analyzer 3 4 MOUNTING SCHEMATICS Figure 3 1 The dimensions for mounting the analyzer...

Page 18: ...allation 17 Waltron User Manual 101 046 B 3 9096 Degassed Cation Conductivity Analyzer 3 5 SAMPLE CONNECTIONS Figure 3 2 Sample Connections Sample Inlet 6mm Swagelok Sample Outlet To Atmospheric Press...

Page 19: ...To turn off power from an electrical device it is necessary to interrupt the power line using a circuit breaker or an isolating switch to be sure that there is no power in the area to be serviced Prot...

Page 20: ...in that level of protection all communications and power cables passing through the transmitter enclosure must use the appropriate cable glands To gain access to the terminal block connections for pow...

Page 21: ...g guidelines should be followed when making connections to avoid damaging the connectors and to ensure good electrical contact is made Maximum wire guage thickness for power input wire to Supply Unit...

Page 22: ...block connector by pulling it out 2 Loosen the screw 3 Insert wire into the connector and tighten screw 4 Push connector back into place and gently tug on wire to confirm the wire is in place To remo...

Page 23: ...nary Maintenance switch Base unit IN 2 Binary Flow measurement Base unit IN 4 Analog Temp Ion exchanger Base unit IN 5 Analog Temp DC sensor Option board IN 7 Analog SC Sensor Option board IN 8 Analog...

Page 24: ...procedures for a proper installation have been followed Please verify that all the suggestions and recommendations have been followed 4 1 PREPARING THE ANALYZER FOR START UP 4 1 1 INSTALLING CATION RE...

Page 25: ...older assembly Make sure that the gasket and bottle holder assembly mating surfaces are free of resin beads 5 Install the bottle by threading the top of the bottle into the bottle holder assembly Tigh...

Page 26: ...een made the analyzer is ready for online measurement Turn on sample flow to the analyzer and adjust to 8 10L hr 130 170ml min The analyzer will begin to display measurement readings for the specific...

Page 27: ...ter enclosure All the output input data information alarms and fault conditions are shown on the display while all the commands and settings may be transferred to the analyzer by simply pressing the t...

Page 28: ...f the main screen will bring up the Operating Level Menu Selecting the first option 9096 Degassed Acid Conductivity will return to show the main display screen with all measured values displayed Selec...

Page 29: ...how a data chart that shows recent trends for each of the measured values Selecting the fourth option from the Operating Menu Group 2 will show a data chart that shows recent trends for each of the te...

Page 30: ...essary to logon using a password to access some configurable parameters Press the box in the lower left hand corner of the display to open the Device Menu and select logon logoff To logon press the lo...

Page 31: ...3 9096 Degassed Cation Conductivity Analyzer Select the appropriate logon ID Type in the correct password and press the Enter button Appropriate access based on logon id used will now be granted and t...

Page 32: ...the bell icon along the bottom of the main display screen Choosing alarm list will bring up the alarm log The alarm log lists all alarms by date and time along with a brief description Selecting an a...

Page 33: ...The anaylzer is equipped with multiple analog outputs which can be configured for output type and scaling In order to change these settings the user will need to logon Open the main device menu by pre...

Page 34: ...available output signal types 4 20mA 0 20mA 0 5V etc Pressing the Scale Start 1 box will allow the user to input a value that will match the low range of the output 4mA Pressing the Scale End 1 box wi...

Page 35: ...vailable output signal types 4 20mA 0 20mA 0 5V etc Pressing the Scale Start 1 box will allow the user to input a value that will match the low range of the output 4mA Pressing the Scale End 1 box wil...

Page 36: ...of available output signal types 4 20mA 0 20mA 0 5V etc Pressing the Scale Start 1 box will allow the user to input a value that will match the low range of the output 4mA Pressing the Scale End 1 box...

Page 37: ...lable output signal types 4 20mA 0 20mA 0 5V etc Pressing the Scale Start 1 box will allow the user to input a value that will match the low range of the output 4mA Pressing the Scale End 1 box will a...

Page 38: ...ailable output signal types 4 20mA 0 20mA 0 5V etc Pressing the Scale Start 1 box will allow the user to input a value that will match the low range of the output 4mA Pressing the Scale End 1 box will...

Page 39: ...by pressing the bottom left hand corner of the main display screen The Calibration folder contains folders for the Specific Conductivity SC Cation Conductivity CC and Degassed Cation Conductivity DC...

Page 40: ...r Manual 101 046 B 3 9096 Degassed Cation Conductivity Analyzer Selecting one of the calibrations and pressing the Details button will provide additional information about the date time and type of ca...

Page 41: ...altron User Manual 101 046 B 3 9096 Degassed Cation Conductivity Analyzer Select Calibration Values to view the cell constant for the conductivity sensor The current cell constants for that conductivi...

Page 42: ...re below Action Display Configuration of the temperature compensation requires log in access of at least the Service Level Access the Configuration Menu by pressing the bottom left hand corner of the...

Page 43: ...t the type of temperature compensation from the list The options are as follows TC linear TC curve natural water natural water with expanded temperature range ASTM neutral ASTM acid ASTM alkaline NaOH...

Page 44: ...new cell constant is as follows where knew is the new cell constant that will be calculated kold is the existing cell constant programmed into the analyzer new is the known conductivity reading from...

Page 45: ...the main screen This will be the value for old in the equation Calculate the new cell constant using the calibration formula Once the new cell constant is calculated the value must be input into the a...

Page 46: ...for Rel Cell const 1 will bring up a number pad which can be used to input the new cell constant value that was calculated Press the green enter button to confirm the input The new cell constant valu...

Page 47: ...egassed Cation Conductivity Analyzer saving any changes that were made The entire procedure above can be repeated for the Cation Conductivity sensor Note the DC sensor relies on the CC sensor calibrat...

Page 48: ...tive measures and scheduled maintenance is strongly recommended During the performance of the basic maintenance work as described in this chapter the analyzer can not be operational Prior to the maint...

Page 49: ...the date and time you are exchanging the resin 2 Press and hold the maintenance switch on the bottom of the transmitter for 2 seconds to hold the 4 20mA outputs and reset the remaining resin counter...

Page 50: ...mating surfaces are free of resin beads 6 Install the new bottle of resin by screwing the bottle into place Tighten about turn after the top of the bottle contacts the gasket Note If it leaks slightl...

Page 51: ...IZATION CATRIDGE Step Illustration Description 1 Note the date and time that you are exchanging the soda lime 2 Unscrew the exisiting cartridge from the housing block 3 Remove plugs covering the inlet...

Page 52: ...Parts Listing Description Part Number Soda Lime Replacement Cartridge with soda lime W1234 606A Pre Rinsed Resin Bottle with resin W1234 609 Table 8 2 Spare Parts Listing Description Part Number Air P...

Page 53: ...ieved are stored on the flash drive together with their configuration data The measurement data are stored in DAT files and the configuration data in SET files These files can be opened and evaluated...

Page 54: ...T together with an additional file with the extension SET A new recording session begins as soon as the new configuration goes into effect One DAT file and one SET file are created for each recording...

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