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Installation

This chapter contains instructions for installing the HP 5973 MSD system.

Installation of any MSD system includes the following steps:

•

Inspection of shipped materials

•

GC installation and preparation

•

MSD installation

•

Data system installation

•

GC and MSD integration

•

Performance evaluation

•

Customer familiarization

Installing the CI MSD system requires additional steps:

•

Methane/isobutane gas purifier installation

•

Methane reagent gas line and gas purifier purge

•

Methane reagent gas line hookup

After system performance has been verified in EI mode, the MSD must be
switched to CI mode and evaluated:

•

CI ion source and CI interface tip seal installation

•

Bakeout and purge at least 2 hours

•

CI setup

•

PCI autotune and sensitivity verification

•

NCI autotune and sensitivity verification

The EI/CI interface on the CI MSD requires a different column installation
procedure.

The HP 59864B vacuum gauge controller is required for CI operation.

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Summary of Contents for 5973

Page 1: ...H Hardware Installation Manual HP 5973 Mass Selective Detector ...

Page 2: ...rectly performed or adhered to could result in personal injury Part Numbers In this manual Hewlett Packard part numbers are generally listed in parentheses after the name of the part or in tables in the Parts chapter Most Hewlett Packard part numbers are either four digit by four digit 1234 1234 numbers or five digit by five digit 12345 12345 numbers A few tools and supplies listed have no part nu...

Page 3: ...Installation 16 Inspecting the shipped materials 17 Installing the GC 18 Installing the MSD 22 Plumbing the methane line to the CI MSD flow module 26 Installing the MSD ChemStation 28 Integrating the GC MSD and ChemStation 29 Verifying EI system performance 30 Switching from EI to CI operating mode 31 Verifying CI performance 32 Familiarizing the customer 33 Chapter 3 Checklists Installation check...

Page 4: ...4 ...

Page 5: ...1 General Information Introduction 6 Customer responsibilities 8 Site requirements 9 Other documentation 13 ...

Page 6: ...on pump MSD or HP G1099A Turbo molecular pump version of the HP 5973 MSD Turbo pump MSD or HP G1999A PCI NCI Turbo molecular pump version of the HP 5973 MSD CI MSD Gas Chromatograph HP 6890 Plus GC with options 112 and 201 HP 7683 Automatic Liquid Sampler optional PC and MSD ChemStation software Refer to your MSD ChemStation documentation for additional information Optional software Mass spectral ...

Page 7: ...l Information 7 HP 7983 ALS tower HP 7983 ALS tray HP 6890 Plus GC HP 5973 MSD HP 7983 ALS tower HP 7983 ALS tray HP 6890 Plus GC CI flow control module HP 5973 CI MSD HP 5973 CI MSD system HP 5973 MSD system ...

Page 8: ...lvents Required high purity methane reagent gas for PCI NCI MSD Optional other reagent gas es for CI MSD Additional methane isobutane gas purifier if isobutane will we used Hose for venting pump exhaust outside or to a fume hood if toxic chemicals will be analyzed or if dangerous carrier or CI reagent gases will be used Installation and testing of additional detectors on the HP 6890 Series GC Trai...

Page 9: ...ong enough to be used at the computer will allow the MSD operator to communicate with HP support personnel In addition a second analog phone line is strongly recommended to allow remote control and diagnosis of the MSD through a modem This is required for some service contracts Environmental requirements Indoor use only Thermal outputs of the MSD system components are listed in Table 1 Temperature...

Page 10: ...0 240 V ac 5 10 47 5 63 Hz single phase nominal 900 VA maximum 400VA maximum for foreline pump only IEC Transient Overvoltage Category Overvoltage Category II IEC Pollution Degree 2 Gases GC carrier gas A regulated supply of high purity 99 999 carrier gas typically helium is required A two stage regulator should be used at the gas supply to eliminate pressure surges If other gases are required for...

Page 11: ...GC 50 58 5 50 50 2 250 8 100 Fast heating oven 2 950 10 620 HP 6890 Series ALS HP 7683 Injector above GC 44 HP 7683 Tray left of GC 30 3 Instrument Height inches Width inches Depth inches Weight pounds Power Volt Amps Heat Btu hr HP 5973 MSD Diffusion Pump MSD 16 0 11 75 21 25 80 900 3 000 Turbo Pump MSD 16 0 11 75 21 25 90 900 3 000 PCI NCI Turbo Pump MSD 16 12 21 25 97 900 3 000 HP 6890 Series G...

Page 12: ...utane The gas purifier can cannot be used with ammonia Clean stainless steel 1 8 inch tubing is supplied for use with the reagent gas Copper tubing is not recommended for carrier gas and must not be used with ammonia Methane required UHP 99 97 Regulator 3320 Stand model J05 Swagelok female connector SS 200 7 2 Isobutane optional Instrument grade 99 5 pure Regulator 3321 or 3320 Stand model J05 Swa...

Page 13: ...ine help HP 5973 MSD Reference Collection CD ROM set HP 6890 Series GC manuals and online help HP GC accessories autosampler etc manuals and online help PC installation manuals PC peripheral manuals printer backup drives etc Application note Optimizing splitless injections on your GC for high performance MS analysis 5091 4587E Hydrogen Carrier Gas Safety Guide 5955 5398 Windows NT 4 0 manual and o...

Page 14: ...14 ...

Page 15: ...ing the MSD 22 Plumbing the methane line to the CI MSD flow module 26 Installing the MSD ChemStation 28 Integrating the GC MSD and ChemStation 29 Verifying EI system performance 30 Switching from EI to CI operating mode 31 Verifying CI performance 32 Familiarizing the customer 33 ...

Page 16: ...onal steps Methane isobutane gas purifier installation Methane reagent gas line and gas purifier purge Methane reagent gas line hookup After system performance has been verified in EI mode the MSD must be switched to CI mode and evaluated CI ion source and CI interface tip seal installation Bakeout and purge at least 2 hours CI setup PCI autotune and sensitivity verification NCI autotune and sensi...

Page 17: ...ing items will not be honored unless an HP representative verifies the contents of each shipping container as it is unpacked 1 KHFN HDFK LWHP RII RQ WKH SDFNLQJ OLVW DQG YHULI VHULDO QXPEHUV 2 5HFRUG WKH VHULDO QXPEHUV LQ WKH LQVWDOODWLRQ GRFXPHQWDWLRQ 3 5HWDLQ VKLSSLQJ FRQWDLQHUV DQG PDWHULDO XQWLO FRQWHQWV DUH FKHFNHG IRU FRPSOHWHQHVV DQG LQVWUXPHQW SHUIRUPDQFH LV YHULILHG 4 I WKHUH DUH DQ GLVFU...

Page 18: ...EOH IRU WKH DQG WKDW WKH OLQH YROWDJH LV FRUUHFW 2 8QSDFN WKH DQG SODFH LW RQ WKH EHQFK This job requires assistance from another person Do not take the Swagelok fittings off the EPC ports until the carrier gas supply is ready to be connected to the GC The system was sealed containing helium gas to prevent contamination by air 3 RQQHFW WKH IRRW FRSSHU WXELQJ RU D FXVWRP OHQJWK WR WKH FDUULHU JDV V...

Page 19: ... 3 FDEOHV WR WKH 3 FRQQHFWRU RQ WKH EDFN RI WKH 11 RQQHFW WKH SRZHU FRUG WR WKH DSSURSULDWH HOHFWULFDO RXWOHW 12 7XUQ RQ WKH DQG YHULI WKDW WKH SDVVHV VHOI WHVW Keep the GC oven turned off 13 6HW WKH 3 DGGUHVV LQ WKH WR On the GC keypad select Options Communication HP IB address 15 and then press Enter 14 RQILJXUH WKH FROXPQ SDUDPHWHUV IRU WKH 06 FROXPQ WKDW LV LQVWDOOHG LQ WKH On the GC keypad se...

Page 20: ...While the oven is heating proceed with the next steps Work quickly to remove the oven wall knockout before the oven gets too hot 21 5HPRYH WKH OHIW VLGH SDQHO RI WKH 22 5HPRYH WKH XSSHU IURQW NQRFNRXW IURP WKH H WHULRU RYHQ ZDOO XVLQJ D IODW EODGH VFUHZGULYHU 23 R QRW UHPRYH WKH LQVXODWLRQ EHWZHHQ WKH H WHULRU DQG LQWHULRU RYHQ ZDOOV EXW PRYH LW DVLGH 8VH WKH VFUHZGULYHU QRW RXU ILQJHUV 24 3RS RXW...

Page 21: ... Installation QVWDOOLQJ WKH 21 Plastic knockouts Metal knockout GC MSD interface heater cable GC end ...

Page 22: ...e install the blue pump exhaust oil trap on the outlet of the foreline pump Otherwise install a hose to take the exhaust to a fume hood or outside Obey all local safety and environmental regulations 5 I WKH 06 LV HTXLSSHG ZLWK D FDS RQ WKH GLIIXVLRQ SXPS RSWLRQ UHPRYH WKH FDS QRZ C A U T I O N Remove the red plug from the outlet of the pump before switching on the power Operation with the plug in ...

Page 23: ...Q WKH 06 KDUGZDUH PDQXDO 7 RRVHQ WKH UHDU VLGHSODWH WKXPEVFUHZ FRPSOHWHO 8 9HULI WKH 3 DGGUHVV RQ WKH 3 06 FRQWURO FDUG LV VHW WR Rear sideplate thumbscrew loosen completely 1 O ON OFF N 2 3 4 5 6 7 8 Remote start cable MSD power cord receptacle HP IB cable HP IB address switch Foreline pump power cord ...

Page 24: ...not protrude as far into the GC oven as that on an EI MSD 12 RQQHFW WKH UHPRWH VWDUW FDEOH IURP WKH WR WKH 06 Special procedure for CI MSD 13 3OXPE WKH PHWKDQH WR WKH JDV IORZ FRQWURO PRGXOH 6HH SDJH 14 QVWDOO WKH RSWLRQDO 3 DXJH RQWUROOHU UHTXLUHG IRU 06 See see the Operating the MSD chapter in the MSD hardware manual HP 6890 Series GC HP 5973 MSD GC MSD interface cable GC end GC MSD interface ca...

Page 25: ... QXW DQG EODQN IHUUXOH IURP WKH HQG RI WKH 06 LQWHUIDFH Special procedure for CI MSD Refer to the HP 5973 MSD CI Hardware Manual G1999 90001 20 QVWDOO WKH FROXPQ LQ WKH 06 LQWHUIDFH See the Installing GC Columns in the MSD hardware manual or CI Setup the CI MSD hardware manual The column installation tool is located in a clear plastic tube in the MSD tool kit 21 3XPS GRZQ WKH 06 See the revised pr...

Page 26: ...QQHFW RQH SLHFH RI WKH LQFK WXELQJ WR WKH PHWKDQH VXSSO UHJXODWRU 4 7XUQ RQ WKH JDV IORZ VOLJKWO 5 RQQHFW WKH RWKHU HQG RI WKH WXELQJ WR WKH LQOHW RI WKH JDV SXULILHU 6 RQQHFW WKH VHFRQG SLHFH RI WXELQJ WR WKH RXWOHW RI WKH JDV SXULILHU 7 HW WKH OLQHV SXUJH LQWR D IXPH KRRG ZKLOH RX LQVWDOO WKH FROXPQ LQWR WKH LQWHUIDFH C A U T I O N Only remove the caps in the gas stream or the gas purifier will ...

Page 27: ...H IORZ PRGXOH 9 I DQRWKHU UHDJHQW JDV LV WR EH XVHG FRQQHFW LW WR WKH DV ILWWLQJ If you are going to connect isobutane you will need another gas purifier for the Gas B line C A U T I O N Do not connect isobutane without a gas purifier Do not use the gas purifier with ammonia Gas B alternate reagent gas line Gas A methane line ...

Page 28: ...tion documentation 4 RQQHFW WKH 3 FDEOH IURP WKH WR WKH 3 5 QVWDOO WKH SULQWHU See the printer installation documentation 6 QVWDOO WKH PRGHP See the modem installation manual Not all ChemStations have modems supplied 7 7XUQ RQ WKH PRGHP SULQWHU PRQLWRU DQG 3 LQ WKDW RUGHU ALS tower cable ALS tray cable Remote start cable HP IB cable HP IB cable Parallel cable for printer Serial cable for modem ...

Page 29: ... View menu Select Pumpdown from the Vacuum menu When the pumpdown is complete follow the instructions to set the GC MSD interface temperature to 280 C 5 QWHU SDUDPHWHUV LQ ATUNE U WR PDWFK WKRVH LQ WKH WXQH UHSRUW IURP WKH IDFWRU In the Diagnostics Vacuum Control view select Edit MS Params from the Diagnostics menu Edit parameters as necessary Select Temperatures from the MoreParams menu Verify th...

Page 30: ...aluate the last autotune and print a System Verification Tune report 5 DPLQH WKH UHSRUW OO SDUDPHWHUV VKRXOG EH OK Verifying the sensitivity performance 1 Prepare a vial with the 1 pg µl 0 001 ppm OFN sample 8500 5441 2 6HW XS WR LQMHFW O HLWKHU ZLWK WKH 6 RU PDQXDOO 3 Q WKH QVWUXPHQW RQWURO YLHZ VHOHFW Sensitivity Check IURP WKH 4XDOLI PHQX The software will load and resolve the method C HPCHEM 1...

Page 31: ...WKH 06 KDUGZDUH PDQXDO 6 3XPS GRZQ WKH 06 6HH SDJH RI WKH 06 KDUGZDUH PDQXDO 7 DNH RXW WKH 06 IRU DW OHDVW WZR KRXUV 8 6HW XS WKH VRIWZDUH IRU RSHUDWLRQ 6HH SDJH RI WKH 06 KDUGZDUH PDQXDO 9 6HW XS WKH PHWKDQH UHDJHQW JDV IORZ 6HH SDJH RI WKH 06 KDUGZDUH PDQXDO 10 9HULI WKDW WKHUH LV QR YLVLEOH SHDN DW P DQG WKDW WKH SHDN DW P LV VPDOOHU WKDQ WKDW DW P 8 7 2 1 Electrostatic discharges to analyzer c...

Page 32: ... PDQXDO 2 Verify positive CI performance 6HH SDJH RI WKH 06 KDUGZDUH PDQXDO Verify that rms signal to noise ratio is at least 75 1 3 Perform a negative CI autotune 6HH SDJH RI WKH 06 KDUGZDUH PDQXDO 4 Verify negative CI performance 6HH SDJH RI WKH 06 KDUGZDUH PDQXDO Verify that rms signal to noise ratio is at least 500 1 1 2 7 There are no criteria for a passing CI autotune If the CI autotune comp...

Page 33: ...ons formed To set up for NCI mode tune in PCI mode then load NCI tune file to switch parameters set gas flow to 40 adjust if necessary for specific analyte NCI operation Gas flow source temperature and emission current are the three most important parameters for optimizing NCI No PFDTD calibrant ions are formed in PCI with isobutane or ammonia Tune with methane and copy parameters to new file e g ...

Page 34: ...34 ...

Page 35: ...3 Checklists Installation checklist 36 Customer familiarization checklist 40 ...

Page 36: ... on the packing list and verify serial numbers o Record the serial numbers in the installation documentation o Retain shipping containers and material until contents are checked for completeness and instrument performance is verified o Notify the distribution center of any missing or damaged items o Shipment damaged or incomplete Distribution center notified date Person contacted DM notified date ...

Page 37: ...gured o Carrier gas line pressure set to approximately 50 psi 345 KPa o Carrier gas flow rate set to 7 ml per minute o Septum plugging end of column removed and end of column trimmed o Helium flow through column verified o Merlin Microseal installed optional o Injection port temperature set to 250 C o Oven temperature ramped from 40 C to 280 C at 15 C per minute and held for 10 minutes o Upper fro...

Page 38: ...and ac supply power cords connected to the MSD o MSD power cord connected to the appropriate ac outlet o GC turned on o GC carrier gas flow set to 1 0 ml per minute with constant flow enabled o Column installed in the GC MSD interface o MSD power on o Foreline pump and the front fan operation verified o Foreline pump stops gurgling within 60 seconds verified o MSD ChemStation installation o PC mon...

Page 39: ...alled o MSD pumped down and baked out for 2 hours o Software set up for CI operation o Methane reagent gas flow set up o Acceptable air and water background verified o CI performance verification o PCI autotune performed o PCI sensitivity verified o NCI autotune performed o NCI sensitivity verified o Instrument log book entries completed o Signal to noise results faxed or mailed to the factory HP ...

Page 40: ... of the operation and maintenance of new instruments systems and applications software It is not a substitute for a full operator training course o Topics not included in familiarization Training on PC Windows NT 4 0 or other Windows applications Advanced mass spectral processing Analysis of unknown samples Analysis of customer standards or samples Network setup of the MSD ChemStation with other P...

Page 41: ... o Starting MSD ChemStation software o Switching between EI and CI operation CI MSD only o MSD ChemStation software overview o Software configuration of the instruments MS Config demonstrated o Different quantitation modes and how to switch between them demonstrated o Views and menu structure demonstrated o MSD ChemStation software familiarization o Autotune described o Autotune demonstrated and e...

Page 42: ...explained including the TIC and spectrum windows command line and title bar o TIC spectra and extracted ion chromatogram demonstrated o Integration explained o Library search demonstrated o Difference between standalone and online data analysis explained o Quantitative report ESTD or ISTD demonstrated using provided demonstration files o Sequence o Sequence loading demonstrated o Sample log table ...

Page 43: ...tenance of the vacuum system o Troubleshooting diagnostics o Carbon Copy demonstrated o Tune charts under Qualify menu demonstrated o Online help for troubleshooting demonstrated o Additional support information o Use the manuals online help and HP MSD Reference Collection CD explained o HP support services and how to obtain help explained Hardware Software Assist Packages Additional Training Cons...

Page 44: ...44 ...

Page 45: ...ir outlets before removing any covers unless you are specifi cally instructed to do other wise by this manual WARNING Excessive fluctuations in the line voltage can create a shock hazard and can damage the instrument Make sure the sup ply voltage does not fluctuate more than 5 or 10 from the rated voltage This equip ment must be installed in a Category II environment as defined in IEC664 Thermal S...

Page 46: ...H Manual Part Number G1099 90006 Copyright 1998 Hewlett Packard Printed in USA 1 98 ...

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