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88 

8.24. FLUORIDE HIGH RANGE

SPECIFICATIONS

Range 

 

0.0 to 20.0 mg/L (as F

)

Resolution   

0.1 mg/L

Accuracy   

±0.5 mg/L ±3% of reading at 25 °C

Light Source 

LED with narrow band interference filter @ 575 nm 

Method   

Adaptation of the Standard Methods for the Examination of Water and  

  Wastewater, 

18

th

 edition, SPADNS method. 

REQUIRED REAGENT
Code 

 Description   Quantity

HI93739A‑0

 

Fluoride High Range Reagent A   

2 mL

HI93739B‑0

 

Fluoride High Range Reagent B   

8 mL

REAGENT SETS

HI93739‑01

 

Reagents for 100 tests

HI93739‑03

 

Reagents for 300 tests

For other accessories see page 200.

MEASUREMENT PROCEDURE

• Select the 

Fluoride HR 

method using the procedure 

described in the Method Selection section 

  (see page 18).

• Add 2.00 mL of 

HI93739A‑0 

Fluoride High Range 

Reagent A to the cuvette and use the pipette to fill 
up the cuvette to the 10 mL mark with 

HI93739B‑0

 

Fluoride High Range Reagent B.

• Replace the cap and invert several times to mix.

• Place the cuvette into the holder and close the lid.

FLUORIDE HIGH RANGE

2 mL

10 mL

Summary of Contents for HI83300

Page 1: ...INSTRUCTION MANUAL HI83300 Multiparameter Photometer...

Page 2: ...the instrument as well as a precise idea of its versatility If you need additional technical information do not hesitate to e mail us at tech hannainst com or view our worldwide contact list at www ha...

Page 3: ...G SAMPLE USER NAMES TO LOG DATA 5 7 DATA MANAGEMENT 5 8 CONTEXTUAL HELP 6 PHOTOMETER MODE 6 1 METHOD SELECTION 6 2 COLLECTING AND MEASURING SAMPLES AND REAGENTS 6 2 1 PROPER USE OF SYRINGE 6 2 2 PROPE...

Page 4: ...L 8 15 CHLORINE TOTAL ULTRA LOW RANGE 8 16 CHLORINE TOTAL ULTRA HIGH RANGE 8 17 CHROMIUM VI LOW RANGE 8 18 CHROMIUM VI HIGH RANGE 8 19 COLOR OF WATER 8 20 COPPER LOW RANGE 8 21 COPPER HIGH RAGE 8 22 C...

Page 5: ...YLAMINE DEHA 8 47 OXYGEN SCAVENGERS HYDROQUINONE 8 48 OXYGEN SCAVENGERS ISO ASCORBIC ACID 8 49 OZONE 8 50 pH 8 51 PHOSPHATE MARINE ULTRA LOW RANGE 8 52 PHOSPHATE LOW RANGE 8 53 PHOSPHATE HIGH RANGE 8...

Page 6: ...y damaged or defective item must be returned in its original packing material with the supplied accessories 2 SAFETY MEASURES The chemicals contained in the reagent kits may be hazardous if improperly...

Page 7: ...9 18 10 01 pH Electrode Intelligent pH temperature electrode Temperature Range 20 0 to 120 0 C 4 0 to 248 0 F Resolution 0 1 C 0 1 F Accuracy 0 5 C 0 9 F 25 C 77 F Additional Specifications Logging 1...

Page 8: ...ck cuvettes to confirm meter functionality Dual purpose micro USB flash drive Li polymer rechargeable battery Auto off Absorbance mode User and sample name entry GLP features 4 2 PRECISION AND ACCURAC...

Page 9: ...ective port covers 5 Light blocking cover panel 6 Cuvette holder 7 ON OFF power button 8 3 5 mm TRRS jack input for digital electrodes 9 Standard USB host connector for data transfer to a USB flash dr...

Page 10: ...ss second level functions Press to move right in a menu or to increment a set value Press to access the setup screen Press to log the current reading Press to review saved logs Press to exit the curre...

Page 11: ...tput Improved optical filters ensure greater wavelength accuracy and allow a brighter stronger signal to be received The end result is higher measurement stability and less wavelength error A focusing...

Page 12: ...charged meter connected to AC DC adapter battery capacity no external adapter battery near 0 no external adapter battery at 0 no external adapter To conserve battery the meter will turn off automatic...

Page 13: ...value Press the Accept key to confirm the value or ESC to return to the Setup menu without saving the new value Date Time Press the Modify key to change the date time Press the functional keys or the...

Page 14: ...language Press Select to choose one of the 7 languages installed Beeper Option Enable or Disable When enabled a short beep is heard every time a key is pressed A long beep alert sounds when the presse...

Page 15: ...5 mm port marked with EXT PROBE located at the rear of the meter If the meter is in Photometer Mode set the meter to Probe Mode by pressing the MODE key 5 4 MODE SELECTION The HI83300 has two operatio...

Page 16: ...ID and user ID can be added to the saved log Use the keys to highlight the Sample ID or User ID then press Modify Text Entry Sample ID and User ID care entered using the alphanumeric multi tapping ke...

Page 17: ...a can be exported to a USB flash drive or to a PC To access Data Export functions press Recall then Export Use the keys to select the desired export location For export to USB Flash Drive insert the U...

Page 18: ...ted as a single file containing all logged photometer and probe data The file name is HI83300 csv The CSV file Comma Separated Values may be opened with a text editor or spreadsheet application 6 PHOT...

Page 19: ...anging on the tip of the syringe Then keeping the syringe in vertical position above the cuvette push the plunger down into the syringe the desired volume has been delivered into the cuvette 6 2 2 PRO...

Page 20: ...indicated with invert to mix and the following icon b Shaking the cuvette moving the cuvette up and down The movement may be gentle or vigorous This mixing method is indicated with shake gently or sh...

Page 21: ...hod requires a different preparation procedure reaction times sample preparations etc If a timer or timers are necessary for proper sample preparation the Timer key will be available To use a reaction...

Page 22: ...o 77 0 F Validation of the HI83300 involves absorbance measurements of certified HANNA CAL Check Standards see Accessories The CAL Check screen guides the user through the measurement of each CAL Chec...

Page 23: ...pressing the MODE key 2 Press the METHOD key 3 Highlight the appropriate Absorbance method according to the wavelength to be used then press Select Absorbance methods are located at the bottom of the...

Page 24: ...the buffer number Buffer 1 for the 1st buffer Buffer 2 for the 2nd buffer The following functions are available in pH Calibration Mode Clear Press to clear the current calibration from the probe Conf...

Page 25: ...asurement screen press the Calibrate key to begin the calibration process When the reading is stable and close to the selected buffer the Confirm key will become available Press Confirm to accept and...

Page 26: ...selection Cleaning may also improve this response Wrong Temperature The buffer temperature is too extreme for the selected buffer value 7 3 pH MEASUREMENT The HI83300 can be used to perform direct pH...

Page 27: ...rinse the electrode with a small amount of sample Discard the rinse Submerse the electrode tip approximately 3 cm 1 into the sample to be tested and stir the sample gently Make sure the electrode jun...

Page 28: ...patible Calibration The probe s current calibration is not compatible with this meter The calibration must be cleared to use this probe Exceeded Probe Range The pH and or temperature measurement excee...

Page 29: ...calibrations and measurements To view the GLP information press the GLP key from the Probe Measurement screen The pH GLP screen displays the following information about the last pH calibration Date an...

Page 30: ...trode in HI70300 or HI80300 storage solution for at least one hour For refillable electrodes If the fi lling solution electrolyte is more than 2 cm 1 below the fill hole add HI7082 or HI8082 3 5M KCl...

Page 31: ...ction electrodes Allow the electrode to stand upright for 1 hour Follow the Storage Procedure above Cleaning Procedure Use diagnostic messages to aid pH electrode troubleshooting Several cleaning solu...

Page 32: ...ent 1 mL HI93755 53 Chlorine Removal Reagent 1 drop REAGENT SETS HI775 26 Reagents for 25 tests For other accessories see page 200 MEASUREMENT PROCEDURE Select the Alkalinity method using the procedur...

Page 33: ...add one drop of HI93755 53 Chlorine Removal Reagent to the unreacted sample Add 1mL of HI775S Alkalinity Reagent to the sample using a 1 mL syringe Replace the cap and invert 5 times Reinsert the cuve...

Page 34: ...ity Reagent 1 mL REAGENT SETS HI755 26 Reagents for 25 tests For other accessories see page 200 MEASUREMENT PROCEDURE Select the Alkalinity Marine method using the procedure described in the Method Se...

Page 35: ...mes Reinsert the cuvette into the instrument and close the lid Press Read to start the reading The instrument displays the results in mg L as calcium carbonate CaCO3 Press or to access the second leve...

Page 36: ...minum Reagent B 1 packet HI93712C 0 Aluminum Reagent C 1 packet REAGENT SETS HI93712 01 Reagents for 100 tests HI93712 03 Reagents for 300 tests For other accessories see page 200 MEASUREMENT PROCEDUR...

Page 37: ...s is the blank Place the first cuvette 1 into the holder and close the lid Press Timer and the display will show the countdown prior to zeroing the blank Alternatively wait for 15 minutes and then pre...

Page 38: ...or to access the second level functions Press the Chem Frm key to convert the result to mg L of aluminum oxide Al2 O3 Press or to return to the measurement screen INTERFERENCES Interference may be cau...

Page 39: ...Low Range Reagent A 4 drops HI93700B 0 Ammonia Low Range Reagent B 4 drops REAGENT SETS HI93700 01 Reagents for 100 tests HI93700 03 Reagents for 300 tests For other accessories see page 200 MEASUREME...

Page 40: ...nd mix the solution Reinsert the cuvette into the instrument and close the lid Press Timer and the display will show the countdown prior to the measurement or alternatively wait for 3 minutes and 30 s...

Page 41: ...rm key to convert the result to mg L of ammonia NH3 and ammonium NH4 Press or to return to the measurement screen INTERFERENCE Interference may be caused by Acetone Alcohols Aldehydes Glycine Hardness...

Page 42: ...m Range Reagent A 4 drops HI93715B 0 Ammonia Medium Range Reagent B 4 drops REAGENT SETS HI93715 01 Reagents for 100 tests HI93715 03 Reagents for 300 tests For other accessories see page 200 MEASUREM...

Page 43: ...the cap and mix the solution Reinsert the cuvette into the instrument and close the lid Press Timer and the display will show the countdown prior to the measurement or alternatively wait for 3 minutes...

Page 44: ...result in mg L of ammonia NH3 and ammonium NH4 Press or to return to the measurement screen INTERFERENCES Interference may be caused by Acetone Alcohols Aldehydes Glycine Hardness above 1 g L Iron Org...

Page 45: ...High Range Reagent A 4 drops HI93733B 0 Ammonia High Range Reagent B 9 mL REAGENT SETS HI93733 01 Reagents for 100 tests HI93733 03 Reagents for 300 tests For other accessories see page 200 MEASUREMEN...

Page 46: ...solution Reinsert the cuvette into the instrument and close the lid Press Timer and the display will show the countdown prior to the measurement or alternatively wait for 3 minutes and 30 seconds and...

Page 47: ...esult to mg L of ammonia NH3 and ammonium NH4 Press or to return to the measurement screen INTERFERENCES Interference may be caused by Acetone Alcohols Aldehydes Glycine Hardness above 1 g L Iron Orga...

Page 48: ...Quantity HI93716 0 Bromine Reagent 1 packet REAGENT SETS HI93716 01 Reagents for 100 tests HI93716 03 Reagents for 300 tests For other accessories see page 200 MEASUREMENT PROCEDURE Select the Bromin...

Page 49: ...imer ends the meter will perform the reading The instrument displays the results in mg L of bromine Br2 INTERFERENCES Interference may be caused by Chlorine Iodine Ozone Oxidized forms of Chromium and...

Page 50: ...A Ca Calcium Reagent A 7 mL HI93752B Ca Calcium Reagent B 1 mL REAGENT SETS HI937521 01 Reagents for 50 tests HI937521 03 Reagents for 150 tests For other accessories see page 200 MEASUREMENT PROCEDUR...

Page 51: ...e meter is zeroed and ready for measurement Remove the cuvette Add 1 mL of HI93752B Ca Calcium Reagent B to the sample using the 1 mL syringe Invert the cuvette 10 times to mix about 15 seconds Reinse...

Page 52: ...the cuvette into the instrument and close the lid Press Read to start the reading The instrument displays the results in mg L of calcium Ca2 INTERFERENCES Interferences may be caused by Acidity as Ca...

Page 53: ...Calcium Reagent B 1 packet REAGENT SETS HI758 26 Reagents for 25 tests For other accessories see page 200 MEASUREMENT PROCEDURE Select the Calcium Marine method using the procedure described in the Me...

Page 54: ...e Add one packet of HI7582 Calcium Reagent B Replace the cap and shake vigorously for 15 seconds or until the powder is completely dissolved Allow air bubbles to dissipate for 15 seconds before taking...

Page 55: ...0 tests HI93753 03 Reagents for 300 tests For other accessories see page 200 MEASUREMENT PROCEDURE Select the Chloride method using the procedure described in the Method Selection section see page 18...

Page 56: ...te by inverting for approximately 30 seconds Add 0 5 mL of HI93753B 0 Chloride Reagent B to each cuvette using the second 1 mL syringe Replace the caps and mix each cuvette by inverting for approximat...

Page 57: ...nutes and press Zero The display will show 0 0 when the meter is zeroed and ready for measurement Remove the cuvette Insert the other cuvette 2 with the reacted sample into the instrument and close th...

Page 58: ...e adding reagents The pH of the sample after addition of reagents should be about 2 Intensely colored samples will cause interference therefore they should be adequately treated before performing the...

Page 59: ...cket HI93738C 0 Chlorine Dioxide Reagent C 1 mL HI93738D 0 Chlorine Dioxide Reagent D 1 mL REAGENT SETS HI93738 01 Reagents for 100 tests HI93738 03 Reagents for 300 tests For other accessories see pa...

Page 60: ...rine Dioxide Reagent C to each cylinder 1 2 using a 1 mL syringe cap and invert several times to mix Add 0 5 mL of HI93738D 0 Chlorine Dioxide Reagent to each cylinder 1 2 using a 1 mL syringe cap and...

Page 61: ...the lid Press Read to start the reading The instrument displays the results in mg L of chlorine dioxide ClO2 SAMPLING PROCEDURE It is recommended to analyze chlorine dioxide samples immediately after...

Page 62: ...n Quantity HI93701A F Free Chlorine Reagent A 3 drops HI93701B F Free Chlorine Reagent B 3 drops REAGENT SETS HI93701 F Reagents for 300 tests liquid HI93701 01 Reagents for 100 tests powder HI93701 0...

Page 63: ...20 seconds Reinsert the cuvette into the instrument and close the lid Press Timer and the display will show the countdown prior to the measurement or alternatively wait for 1 minute and press Read Wh...

Page 64: ...ine Ozone Oxidized forms of Chromium and Manganese In case of water with hardness greater than 500 mg L CaCO3 shake the sample for approximately 2 minutes after adding the powder reagent If the water...

Page 65: ...gent 1 packet REAGENTS SETS HI95762 01 Reagents for 100 tests HI95762 03 Reagents for 300 tests For other accessories see page 200 MEASUREMENT PROCEDURE Select the Chlorine Free ULR method using the p...

Page 66: ...mg L CaCO3 if present as bicarbonate HCO3 sample pH 8 3 above 25 mg L CaCO3 if present as carbonate CO3 2 sample pH 9 0 In both cases it will not reliably develop the full amount of color or it may ra...

Page 67: ...Chlorine Reagent A 3 drops HI93701B T Total Chlorine Reagent B 3 drops HI93701C T Total Chlorine Reagent C 1 drop REAGENT SETS HI93701 T Reagents for 300 tests liquid HI93711 01 Reagents for 100 total...

Page 68: ...ent and close the lid Press Timer and the display will show the countdown prior to the measurement or alternatively wait for 2 minutes and 30 seconds and press Read When the timer ends the meter will...

Page 69: ...elated procedure if both values are desired INTERFERENCES Interference may be caused by Bromine Iodine Ozone Oxidized forms of Chromium and Manganese In case of water with hardness greater than 500 mg...

Page 70: ...eagent 1 packet REAGENT SETS HI95761 01 Reagents for 100 tests HI95761 03 Reagents for 300 tests For other accessories see page 200 MEASUREMENT PROCEDURE Select the Chlorine Total ULR method using the...

Page 71: ...d by Alkalinity above 1 000 mg L CaCO3 if present as bicarbonate HCO3 sample pH 8 3 above 25 mg L CaCO3 if present as carbonate CO3 2 sample pH 9 0 In both cases it will not reliably develop the full...

Page 72: ...acket HI95771B 0 Total Chlorine Ultra High Range Reagent B 1 packet REAGENTS SETS HI95771 01 Reagents for 100 tests HI95771 03 Reagents for 300 tests For other accessories see page 200 MEASUREMENT PRO...

Page 73: ...ment and close the lid Press Timer and the display will show the countdown prior to the measurement or alternatively wait for 1 minute and press Read When the timer ends the meter will perform the rea...

Page 74: ...Reagents for 100 tests HI93749 03 Reagents for 300 tests For other accessories see page 200 MEASUREMENT PROCEDURE Select the Chromium VI LR method using the procedure described in the Method Selectio...

Page 75: ...g The instrument displays concentration in g L of chromium Cr6 Press or to access the second level functions Press the Chem Frm key to convert the result to g L of chromate CrO4 2 and dichromate Cr2 O...

Page 76: ...Reagents for 100 tests HI93723 03 Reagents for 300 tests For other accessories see page 200 MEASUREMENT PROCEDURE Select the Chromium VI HR method using the procedure described in the Method Selectio...

Page 77: ...g The instrument displays concentration in g L of chromium Cr6 Press or to access the second level functions Press the Chem Frm key to convert the result to g L of chromate CrO4 2 and dichromate Cr2 O...

Page 78: ...Cobalt method REQUIRED ACCESSORIES 0 45 m membrane for true color measurement For other accessories see page 200 MEASUREMENT PROCEDURE Select the Color of Water method using the procedure described in...

Page 79: ...the cap This is the true color Insert the apparent color cuvette 2 into the instrument and close the lid Press Read to start the reading The meter displays the value of apparent color in Platinum Cob...

Page 80: ...ent 1 packet REAGENT SETS HI95747 01 Reagents for 100 tests HI95747 03 Reagents for 300 tests For other accessories see page 200 MEASUREMENT PROCEDURE Select the Copper LR method using the procedure d...

Page 81: ...Press Timer and the display will show the countdown prior to the measurement or alternatively wait for 45 seconds and press Read When the timer ends the meter will perform the reading The instrument d...

Page 82: ...nt 1 packet REAGENT SETS HI93702 01 Reagents for 100 tests HI93702 03 Reagents for 300 tests For other accessories see page 200 MEASUREMENT PROCEDURE Select the Copper HR method using the procedure de...

Page 83: ...Press Timer and the display will show the countdown prior to the measurement or alternatively wait for 45 seconds and press Read When the timer ends the meter will perform the reading The instrument...

Page 84: ...et REAGENT SETS HI93722 01 Reagents for 100 tests HI93722 03 Reagents for 300 tests For other accessories see page 200 MEASUREMENT PROCEDURE Select the Cyanuric Acid method using the procedure describ...

Page 85: ...cap Reinsert the cuvette into the instrument and close the lid Press Timer and the display will show the countdown prior to the measurement or alternatively wait for 45 seconds and press Read When th...

Page 86: ...ts HI93729 03 Reagents for 300 tests For other accessories see page 200 MEASUREMENT PROCEDURE Select the Fluoride LR method using the procedure described in the Method Selection section see page 18 Ad...

Page 87: ...in mg L of fluoride F Note For wastewater or seawater samples before performing measurements distillation is required For most accurate results use two graduated pipettes to deliver exactly 8 mL of d...

Page 88: ...93739B 0 Fluoride High Range Reagent B 8 mL REAGENT SETS HI93739 01 Reagents for 100 tests HI93739 03 Reagents for 300 tests For other accessories see page 200 MEASUREMENT PROCEDURE Select the Fluorid...

Page 89: ...Remove the cuvette Add 1 mL of sample to the cuvette using the second 1 mL syringe Replace the cap and invert several times to mix Insert the cuvette into the instrument and close the lid Press Timer...

Page 90: ...ces may be caused by Alkalinity as CaCO3 above 5000 mg L Aluminum above 0 1 mg L Iron ferric above 10 mg L Chloride above 700 mg L ortho Phosphate above 16 mg L Sodium hexametaphosphate above 1 0 mg L...

Page 91: ...HI93720C 0 Calcium Hardness Reagent C 1 drop REAGENT SETS HI93720 01 Reagents for 100 tests HI93720 03 Reagents for 300 tests For other accessories see page 200 MEASUREMENT PROCEDURE Select the Hardn...

Page 92: ...to the holder and close the lid Press the Zero key The display will show 0 0 when the meter is zeroed and ready for measurement Remove the blank 1 and insert the second cuvette 2 into the instrument P...

Page 93: ...on systems When testing some other sources of water it is not uncommon to come across levels of hardness that are greater than the range of this meter This problem can be overcome through dilution Dil...

Page 94: ...HI93719C 0 Magnesium Hardness Reagent C 1 drop HI93719D 0 Magnesium Hardness Reagent D 1 drop REAGENT SETS HI93719 01 Reagents for 100 tests HI93719 03 Reagents for 300 tests For other accessories see...

Page 95: ...nk Add 1 drop of HI93719D 0 Magnesium Hardness Reagent D to the second cuvette 2 replace the cap and invert the cuvette several times to mix This is the sample Place the blank 1 into the holder and cl...

Page 96: ...to the measurement screen Note This test will detect any magnesium contamination in the beakers measuring syringes or sample cells To test cleanliness repeat the test multiple times until you obtain...

Page 97: ...eagent 1 packet REAGENT SETS HI93735 00 Reagents for 100 tests LR 0 to 250 mg L HI93735 0 Reagents for 300 tests LR 100 tests MR 100 tests HR 100 tests For other accessories see page 200 MEASUREMENT P...

Page 98: ...e the cuvette and add the contents of one packet of HI93735C 0 Fixing Reagent Replace the cap and shake gently to mix 20 seconds Place the cuvette into the holder and close the lid Press Read to start...

Page 99: ...Press the Chem Frm key to convert the result to French degrees f English degrees E and German degrees dH Press or to return to the measurement screen INTERFERENCE Interferences may be caused by excess...

Page 100: ...ent 1 packet REAGENT SETS HI93735 01 Reagents for 100 tests MR 200 to 500 mg L HI93735 0 Reagents for 300 tests LR 100 tests MR 100 tests HR 100 tests For other accessories see page 200 MEASUREMENT PR...

Page 101: ...oed and ready for measurement Remove the cuvette and add one packet of HI93735C 0 Fixing Reagent Replace the cap and shake gently to mix 20 seconds Place the cuvette into the holder and close the lid...

Page 102: ...E Press the Chem Frm key to convert the result to French degrees f English degrees E and German degrees dH Press or to return to the measurement screen INTERFERENCES Interferences may be caused by exc...

Page 103: ...Reagent 1 packet REAGENT SETS HI93735 02 Reagents for 100 tests HR 400 to 750 mg L HI93735 0 Reagents for 300 tests LR 100 tests MR 100 tests HR 100 tests For other accessories see page 200 MEASUREMEN...

Page 104: ...nt Remove the cuvette and add one packet of HI93735C 0 Fixing Reagent Replace the cap and shake gently to mix 20 seconds Place the cuvette into the holder and close the lid Press Read to start the rea...

Page 105: ...Press the Chem Frm key to convert the result to French degrees f English degrees E and German degrees dH Press or to return to the measurement screen INTERFERENCES Interferences may be caused by exce...

Page 106: ...I93704 0 Hydrazine Reagent 24 drops REAGENT SETS HI93704 01 Reagents for 100 tests HI93704 03 Reagents for 300 tests For other accessories see page 200 MEASUREMENT PROCEDURE Select the Hydrazine metho...

Page 107: ...d press Zero The display will show 0 0 when the meter is zeroed and ready for measurement Remove the blank Insert the cuvette with the reacted sample 2 into the instrument and close the lid Press Read...

Page 108: ...Quantity HI93718 0 Iodine Reagent 1 packet REAGENT SETS HI93718 01 Reagents for 100 tests HI93718 03 Reagents for 300 tests For other accessories see page 200 MEASUREMENT PROCEDURE Select the Iodine...

Page 109: ...ends the meter will perform the reading The instrument displays the concentration in mg L of iodine I2 INTERFERENCES Interference may be caused by Bromine Chlorine Ozone Oxidized forms of Chromium an...

Page 110: ...50 tests HI93746 03 Reagents for 150 tests For other accessories see page 200 MEASUREMENT PROCEDURE Select the Iron LR method using the procedure described in the Method Selection section see page 18...

Page 111: ...raduated mixing cylinder up to the 25 mL mark with the sample Add one packet of HI93746 0 Iron Low Range Reagent close the cylinder and shake vigorously for 30 seconds This is the reacted sample Fill...

Page 112: ...ation in mg L of iron Fe INTERFERENCES Interference may be caused by Cadmium above 4 0 mg L Chromium3 above 0 25 mg L Chromium6 above 1 2 mg L Cobalt above 0 05 mg L Copper above 0 6 mg L Cyanide abov...

Page 113: ...3721 0 Iron High Range Reagent 1 packet REAGENT SETS HI93721 01 Reagents for 100 tests HI93721 03 Reagents for 300 tests For other accessories see page 200 MEASUREMENT PROCEDURE Select the Iron HR met...

Page 114: ...Timer and the display will show the countdown prior to the measurement or alternatively wait for 3 minutes and press Read When the timer ends the meter will perform the reading The instrument display...

Page 115: ...L REAGENT SETS HI937520 01 Reagents for 50 tests HI937520 03 Reagents for 150 tests For other accessories see page 200 MEASUREMENT PROCEDURE Select the Magnesium method using the procedure described i...

Page 116: ...he lid Press Timer and the display will show the countdown prior to the measurement or alternatively wait for 15 seconds and press Read When the timer ends the meter will perform the reading The instr...

Page 117: ...ge Reagent C 2 mL HI93703 51 Dispersing Agent 6 drops REAGENT SETS HI93748 01 Reagents for 50 tests HI93748 03 Reagents for 150 tests For other accessories see page 200 MEASUREMENT PROCEDURE Select th...

Page 118: ...ly Add 3 drops of HI93703 51 Dispersing Agent to each cuvette replace the caps and invert gently to mix for about 30 seconds Place the first cuvette 1 with the reacted deionized water into the holder...

Page 119: ...ns Press the Chem Frm key to convert the result to g L of potassium permanganate KMnO4 and permanganate MnO4 Press or to return to the measurement screen INTERFERENCES Interference may be caused by Al...

Page 120: ...eagent B 1 packet REAGENT SETS HI93709 01 Reagents for 100 tests HI93709 03 Reagents for 300 tests For other accessories see page 200 MEASUREMENT PROCEDURE Select the Manganese HR method using the pro...

Page 121: ...ay will show the countdown prior to the measurement or alternatively wait for 1 minute and 30 seconds and press Read When the timer ends the meter will perform the reading The instrument displays the...

Page 122: ...122 MANGANESE HIGH RANGE INTERFERENCES Interference may be caused by Calcium above 700 mg L Chloride above 70000 mg L Iron above 5 mg L Magnesium above 100000 mg L...

Page 123: ...agent B 1 packet HI93730C 0 Molybdenum Reagent C 1 packet REAGENT SETS HI93730 01 Reagents for 100 tests HI93730 03 Reagents for 300 tests For other accessories see page 200 MEASUREMENT PROCEDURE Sele...

Page 124: ...solved Add one packet of HI93730B 0 Molybdenum Reagent B to the cylinder close and invert several times until completely dissolved Add one packet of HI93730C 0 Molybdenum Reagent C to the cylinder clo...

Page 125: ...to access the second level functions Press the Chem Frm key to convert the result to mg L of molybdate MoO4 2 and sodium molybdate Na2 MoO4 Press or to return to the measurement screen INTERFERENCES...

Page 126: ...1 Reagents for 50 tests HI93740 03 Reagents for 150 tests For other accessories see page 200 MEASUREMENT PROCEDURE Select the Nickel LR method using the procedure described in the Method Selection sec...

Page 127: ...mix until completely dissolved Fill one cuvette 1 with 10 mL of the blank up to the mark Place the cuvette into the holder and close the lid Press the Zero key The display will show 0 0 when the mete...

Page 128: ...dity is removed before zeroing the meter and reading the sample INTERFERENCES Interference may be caused by Co2 must not be present Fe2 must not be present Al3 above 32 mg L Ca2 above 1000 mg L as CaC...

Page 129: ...gent 1 packet REAGENT SETS HI93726 01 Reagents for 100 tests HI93726 03 Reagents for 300 tests For other accessories see page 200 MEASUREMENT PROCEDURE Select the Nickel HR method using the procedure...

Page 130: ...vette into the instrument and close the lid Press Timer and the display will show the countdown prior to the measurement or alternatively wait for 1 minute and press Read When the timer ends the meter...

Page 131: ...8 0 Nitrate Reagent 1 packet REAGENT SETS HI93728 01 Reagents for 100 tests HI93728 03 Reagents for 300 tests For other accessories see page 200 MEASUREMENT PROCEDURE Select the Nitrate method using t...

Page 132: ...itively affect the measurement Note The method is technique sensitive See procedure on page 20 Cuvette Preparation for proper mixing technique Reinsert the cuvette into the instrument and close the li...

Page 133: ...e NO3 Press or to return to the measurement screen INTERFERENCES Interference may be caused by Ammonia and amines as urea and primary aliphatic amines Chloride above 100 ppm Chlorine above 2 ppm Coppe...

Page 134: ...or 25 tests For other accessories see page 200 MEASUREMENT PROCEDURE Select the Nitrite Marine ULR method using the procedure described in the Method Selection section see page 18 Fill the cuvette wit...

Page 135: ...nd level functions Press the Chem Frm key to convert the result to g L of nitrite NO2 and sodium nitrite NaNO2 Press or to return to the measurement screen INTERFERENCES Interference may be caused by...

Page 136: ...REAGENT SETS HI93707 01 Reagents for 100 tests HI93707 03 Reagents for 300 tests For other accessories see page 200 MEASUREMENT PROCEDURE Select the Nitrite LR method using the procedure described in...

Page 137: ...lay will show the countdown prior to the measurement or alternatively wait for 15 minutes and press Read When the timer ends the meter will perform the reading The instrument displays concentration in...

Page 138: ...ercurous silver antimonious bismuth auric lead metavanadate and chloroplatinate Strongly reducing and oxidizing reagents High levels of nitrate above 100 mg L could yield falsely high readings due to...

Page 139: ...eagent 1 packet REAGENT SETS HI93708 01 Reagents for 100 tests HI93708 03 Reagents for 300 tests For other accessories see page 200 MEASUREMENT PROCEDURE Select the Nitrite HR method using the procedu...

Page 140: ...isplay will show the countdown prior to the measurement or alternatively wait for 10 minutes and press Read When the timer ends the meter will perform the reading The instrument displays concentration...

Page 141: ...nts for 100 tests HI93732 03 Reagents for 300 tests For other accessories see page 200 MEASUREMENT PROCEDURE Select the Oxygen dissolved method using the procedure described in the Method Selection se...

Page 142: ...ating agent dissolves completely The sample is ready for measurement when it is yellow and completely clear Fill the first cuvette 1 with 10 mL of the unreacted sample up to the mark and replace the c...

Page 143: ...sert the cuvette into the holder and close the lid Press Read to start the reading The instrument will display the results in mg L of oxygen O2 INTERFERENCES Interferences may be caused by reducing an...

Page 144: ...Oxygen Scavengers Reagent B 1 mL REAGENT SET HI96773 01 Reagents for 50 tests HI96773 03 Reagents for 150 tests For other accessories see page 200 MEASUREMENT PROCEDURE Select the Oxy Scavengers Carb...

Page 145: ...ce first cuvette 1 into the holder and close the lid Press Timer and the display will show countdown prior to the measurement or alternatively wait for 10 minutes and press Zero The display will show...

Page 146: ...e the lid Press Read to start reading The instrument displays the results in mg L of carbohydrazide INTERFERENCES Interference may be caused by Borate as Na2 B4 O7 Cobalt Copper Iron Ferrous Hardness...

Page 147: ...ts HI96773B 0 Oxygen Scavengers Reagent B 1 mL REAGENT SET HI96773 01 Reagents for 50 tests HI96773 03 Reagents for 150 tests For other accessories see page 200 MEASUREMENT PROCEDURE Select the Oxy Sc...

Page 148: ...rst cuvette 1 into the holder and close the lid Press Timer and the display will show countdown prior to the measurement or alternatively wait for 10 minutes and press Zero The display will show 0 0 w...

Page 149: ...the lid Press Read to start reading The instrument displays the results in g L of DEHA INTERFERENCES Interference may be caused by Borate as Na2 B4 O7 Cobalt Copper Iron Ferrous Hardness as CaCO3 Ligh...

Page 150: ...Oxygen Scavengers Reagent B 1 mL REAGENT SET HI96773 01 Reagents for 50 tests HI96773 03 Reagents for 150 tests For other accessories see page 200 MEASUREMENT PROCEDURE Select the Oxy Scavengers Hydr...

Page 151: ...ce first cuvette 1 into the holder and close the lid Press Timer and the display will show countdown prior to the measurement or alternatively wait for 2 minutes and press Zero The display will show 0...

Page 152: ...the lid Press Read to start reading The instrument displays the results in mg L of hydroquinone INTERFERENCES Interference may be caused by Borate as Na2 B4 O7 Cobalt Copper Iron Ferrous Hardness as C...

Page 153: ...B 0 Oxygen Scavengers Reagent B 1 mL REAGENT SET HI96773 01 Reagents for 50 tests HI96773 03 Reagents for 150 tests For other accessories see page 200 MEASUREMENT PROCEDURE Select the Oxy Scavengers I...

Page 154: ...lace first cuvette 1 into the holder and close the lid Press Timer and the display will show countdown prior to the measurement or alternatively wait for 10 minutes and press Zero The display will sho...

Page 155: ...e the lid Press Read to start reading The instrument displays the results in mg L of Iso ascorbic acid INTERFERENCES Interference may be caused by Borate as Na2 B4 O7 Cobalt Copper Iron Ferrous Hardne...

Page 156: ...00 Note If the sample is suspected to contain chlorine residue free or total chlorine follow the alternative measurement procedure described below chlorine is a strong interferent Perform the Standard...

Page 157: ...display will show the countdown prior to the measurement or alternatively wait for 2 minutes and press Read When the timer ends the meter will perform the reading The instrument displays the result i...

Page 158: ...cap and shake gently for 20 seconds Replace the cuvette into the instrument and close the lid Press Timer and the display will show the countdown prior to the measurement or alternatively wait for 2...

Page 159: ...re INTERFERENCES Interference may be caused by Bromine Chlorine Dioxide Iodine Alkalinity above 250 mg L CaCO3 will not reliably develop the full amount of color or it may rapidly fade To resolve this...

Page 160: ...SETS HI 93710 01 Reagents for 100 pH tests HI 93710 03 Reagents for 300 pH tests For other accessories see page 200 MEASUREMENT PROCEDURE Select the pH method using the procedure described in the Met...

Page 161: ...and add 5 drops of HI93710 0 pH Reagent Indicator Replace the cap and mix the solution Reinsert the cuvette into the instrument and close the lid Press the Read key to start the reading The instrument...

Page 162: ...For other accessories see page 200 MEASUREMENT PROCEDURE Select the Phosphate Marine ULR method using the procedure described in the Method Selection section see page 18 Rinse cap and shake the cuvet...

Page 163: ...eading The instrument displays concentration in g L of phosphorus P Press or to access the second level functions Press the Chem Frm key to convert the result to g L of phosphate PO4 3 and phosphorus...

Page 164: ...e page 200 MEASUREMENT PROCEDURE Select the Phosphate LR method using the procedure described in the Method Selection section see page 18 Rinse cap and shake the cuvette several times with unreacted s...

Page 165: ...The instrument displays concentration in mg L of phosphate PO4 3 Press or to access the second level functions Press the Chem Frm key to convert the result to mg L of phosphorus P and phosphorus pento...

Page 166: ...drops HI93717B 0 Phosphate High Range Reagent B 1 packet REAGENT SETS HI93717 01 Reagents for 100 tests HI93717 03 Reagents for 300 tests For other accessories see page 200 MEASUREMENT PROCEDURE Sele...

Page 167: ...nd the display will show the countdown prior to the measurement or alternatively wait for 5 minutes and press Read When the timer ends the meter will perform the reading The instrument displays the re...

Page 168: ...168 PHOSPHATE HIGH RANGE INTERFERENCES Sulfide Chloride above 150000 mg L Calcium above 10000 mg L as CaCO3 Magnesium above 40000 mg L as CaCO3 Ferrous iron above 100 mg L...

Page 169: ...A 0 Potassium Reagent A 6 drops HI93750B 0 Potassium Reagent B 1 packet REAGENT SETS HI93750 01 Reagents for 100 tests HI93750 03 Reagents for 300 tests For other accessories see page 200 MEASUREMENT...

Page 170: ...nd shake gently for 1 minute Reinsert the cuvette into the instrument and close the lid Press Timer and the display will show the countdown prior to the measurement or alternatively wait for 2 minutes...

Page 171: ...to mg L of potassium oxide K2 O Press or to return to the measurement screen INTERFERENCES Interferences may be caused by Ammonium above 10 ppm Calcium above 10000 ppm as CaCO3 Chloride above 12000 p...

Page 172: ...Reagents for 100 tests HI93705 03 Reagents for 300 tests For other accessories see page 200 MEASUREMENT PROCEDURE Select the Silica LR method using the procedure described in the Method Selection sect...

Page 173: ...5C 0 Silica Low Range Reagent C and shake until it is completely dissolved Reinsert the cuvette into the instrument and close the lid Press Timer and the display will show the countdown prior to the m...

Page 174: ...measurement screen INTERFERENCES Interference may be caused by Phosphate above 60 mg L causes a 2 reduction in reading Phosphate above 75 mg L causes an 11 reduction in reading Sulfide and high conce...

Page 175: ...gent A 1 packet HI96770B 0 Silica High Range Reagent B 1 packet HI96770C 0 Silica High Range Reagent C 1 packet REAGENT SETS HI96770 01 Reagents for 100 tests HI96770 03 Reagents for 300 tests For oth...

Page 176: ...w the countdown prior adding HI96770C 0 Silica High Range Reagent C or alternatively wait 10 minutes Add one packet of HI96770C 0 Silica High Range Reagent C and shake vigorously until completely diss...

Page 177: ...ress or to return to the measurement screen INTERFERENCES Interference may be caused by Phosphate above 60 mg L causes a 2 reduction in reading Phosphate above 75 mg L causes an 11 reduction in readin...

Page 178: ...I93737C 0 Silver Reagent C 2 mL HI93737D 0 Silver Reagent D 2 mL HI93703 51 Dispersing Agent 6 drops REAGENT SETS HI93737 01 Reagents for 50 tests HI93737 03 Reagents for 150 tests For other accessori...

Page 179: ...n prior to adding HI93737C 0 Silver Reagent C or alternatively wait for 2 minutes Add 1 mL of HI93737C 0 Silver Reagent C to each beaker and swirl Press Continue and the display will show the countdow...

Page 180: ...or 10 seconds Place the cuvette into the holder and close the lid Press the Zero key The display will show 0 0 when the meter is zeroed and ready for measurement Fill a second cuvette 2 up with 10 mL...

Page 181: ...bove 1 5 mg L Ca2 above 1000 mg L as CaCO3 Fe3 above 10 mg L Cd2 above 20 mg L K above 500 mg L Cl above 8000 mg L Mn2 above 25 mg L Co2 above 1 5 mg L Mg2 above 1000 mg L as CaCO3 Cr3 above 20 mg L N...

Page 182: ...fate Reagent 1 packet REAGENT SETS HI93751 01 Reagents for 100 tests HI93751 03 Reagents for 300 tests For other accessories see page 200 MEASUREMENT PROCEDURE Select the Sulfate method using the proc...

Page 183: ...ss Read When the timer ends the meter will perform the reading The instrument displays the concentration in mg L of sulfate SO4 2 INTERFERENCES Interferences may be caused by Calcium as CaCO3 above 20...

Page 184: ...Surfactants Reagent B 2 drops Chloroform Reagent 10 mL DEIONIZED120 Deionizate Water 15 mL REAGENT SETS HI95769 01 Reagents for 40 tests For other accessories see page 200 MEASUREMENT PROCEDURE Selec...

Page 185: ...s During this period the chloroform layer separates from the aqueous layer the color of the aqueous layer will fade slightly while the chloroform layer will turn blue Remove the cap Remove the upper a...

Page 186: ...y warming the cuvette holding the vial in your hand If the chloroform layer contains some aqueous drops hanging on the cuvette wall gently swirl or invert the cuvette It is important to transfer at le...

Page 187: ...s the result in mg L as SDBS INTERFERENCES Cationic surfactants negative interference Absorption particulate matter negative interference Sulfide negative interference Organic sulfates sulfonates posi...

Page 188: ...1 packet HI93731B 0 Zinc Reagent B 0 5 mL REAGENT SETS HI93731 01 Reagents for 100 tests HI93731 03 Reagents for 300 tests For other accessories see page 200 MEASUREMENT PROCEDURE Select the Zinc meth...

Page 189: ...cuvette with the supplied HDPE plastic stopper to prevent contamination Replace the cap and mix for 15 seconds Insert the sample into the instrument and close the lid Press Timer and the display will...

Page 190: ...190 ZINC INTERFERENCES Interference may be caused by Aluminum above 6 mg L Iron above 7 mg L Cadmium above 0 5 mg L Manganese above 5 mg L Copper above 5 mg L Nickel above 5 mg L...

Page 191: ...ease check that the sample does not contain any debris Light High There is too much light to perform a measurement Please check the preparation of the zero cuvette 9 ERROR DESCRIPTIONS Ambient tempera...

Page 192: ...rine Free LR 0 00 to 5 00 mg L DPD Chlorine Free ULR 0 000 to 0 500 mg L DPD Chlorine Total LR 0 00 to 5 00 mg L DPD Chlorine Total ULR 0 000 to 0 500 mg L DPD Chlorine Total UHR 0 to 500 mg L Standar...

Page 193: ...to 1 000 mg L PAN Nickel HR 0 00 to 7 00 g L Colorimetric Nitrate 0 0 to 30 0 mg L Cadmium reduction Nitrite Marine ULR 0 to 200 g L Diazotization Nitrite LR 0 to 600 g L Diazotization Nitrite HR 0 t...

Page 194: ...0 0 to 20 0 mg L Tetraphenylborate Silica LR 0 00 to 2 00 mg L Heteropoly Blue Silica HR 0 to 200 mg L EPA Silver 0 000 to 1 000 mg L PAN Sulfate 0 to 150 mg L Barium Chloride Surfactants Anionic 0 0...

Page 195: ...100 copper HR tests HI93702 03 300 copper HR tests HI93703 52 100 ozone tests HI93704 01 100 hydrazine tests HI93704 03 300 hydrazine tests HI93705 01 100 silica LR tests HI93705 03 300 silica LR tes...

Page 196: ...100 chromium VI HR tests HI93723 03 300 chromium VI HR tests HI93726 01 100 nickel HR tests HI93726 03 300 nickel HR tests HI93728 01 100 nitrate tests HI93728 03 300 nitrate tests HI93729 01 100 flu...

Page 197: ...01 100 potassium tests HI93750 03 300 potassium tests HI93751 01 100 sulfate tests HI93751 03 300 sulfate tests HI937520 01 50 magnesium tests HI937520 03 150 magnesium tests HI937521 01 50 calcium f...

Page 198: ...H temperature electrode with enhanced diagnostics HI12300 Plastic body double junction gel filled non refillable pH temperature electrode HI12301 Plastic body double junction gel filled non refillable...

Page 199: ...DA approved bottle 500 mL HI8010L pH 10 01 Buffer Solution in FDA approved bottle 500 mL ELECTRODE STORAGE SOLUTIONS HI70300L Storage Solution 500 mL HI80300L Storage Solution in FDA approved bottle 5...

Page 200: ...astic beaker HI740224 170 mL plastic beaker 12 pcs HI740225 60 mL graduated syringe HI740226 5 mL graduated syringe HI740227 filter assembly HI740228 filter discs 25 pcs HI 740229 100 mL graduated cyl...

Page 201: ...icrograms per liter ppb mg L milligrams per liter ppm g L grams per liter ppt mL milliliter GLP good laboratory practice UHR ultra high range ULR ultra low range HR high range MR medium range LR low r...

Page 202: ...nterferences to other electronic equipment Take all necessary steps to correct such interferences Any variation introduced by the user to the supplied equipment may degrade the instruments EMC perform...

Page 203: ...of purchase serial number and the nature of the problem If the repair is not covered by the warranty you will be notified of the charges incurred If the instrument is to be returnedtoHannaInstruments...

Page 204: ...a Instruments Inc Highland Industrial Park 584 Park East Drive Woonsocket RI 02895 USA www hannainst com Local Office Hanna Instruments USA 270 George Washington Highway Smithfield RI 02917 Phone 800...

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