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Hach POLYMETRON 8810, User Manual

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Hach POLYMETRON 8810 User Manual Download Page 1

DOC024.52.93057

POLYMETRON Model 8810 ISE Analyzer

User Manual

05/2015, Edition 19

Summary of Contents for POLYMETRON 8810

Page 1: ...DOC024 52 93057 POLYMETRON Model 8810 ISE Analyzer User Manual 05 2015 Edition 19 ...

Page 2: ......

Page 3: ... 5 1 3 Electrode connections 16 4 5 2 Mains power supply 17 4 5 3 Input Output connections 18 4 5 3 1 Alarms 20 4 5 3 2 Analog outputs 20 4 5 3 3 Sample level detector 20 4 5 3 4 Reagent level detector 20 4 5 3 5 RS232 connection 21 4 5 4 Additional accessories 22 Section 5 User interface 23 5 1 Front panel description 23 5 2 Function keys 23 5 3 Analyzer modes 23 5 4 Displays 23 Section 6 Menu ov...

Page 4: ...n 34 7 2 Troubleshooting 34 Section 8 Additional options 37 8 1 Automatic calibration 38 8 1 1 One point calibration with a volumetric pump 38 8 1 2 Two point calibration with a micro piston pump 39 8 1 3 Two point calibration with a pulse pump 39 8 2 Chemical cleaning 39 8 3 Conditioning 40 8 4 Dilution or decantation 40 8 5 External sample 43 8 6 Heating system 44 8 7 Extra channel 44 8 8 Reagen...

Page 5: ...ried Rinse water pressure 0 5 6 bar Reagents 10 liter storage canister supplied Analog outputs Number 2 0 20 or 4 20 linear logarithmic or dual programmable Alarms 2 x Relay concentration 1 x Warning or System alarm Exchangeable sensors ISE reference electrode Pt100 Level control Sample Reagents Calibration solution Chemical cleaning Pumps Peristaltic micro piston pulse or volumetric pumps for cal...

Page 6: ...1 1 Dimensions Figure 1 Panel dimensions mm inches Specifications 4 ...

Page 7: ...Figure 2 Cabinet dimensions mm inches Specifications 5 ...

Page 8: ...Specifications 6 ...

Page 9: ...D AN GE R Indicates a potentially or imminently hazardous situation which if not avoided will result in death or serious injury WA RNING Indicates a potentially or imminently hazardous situation which if not avoided could result in death or serious injury C AUTION Indicates a potentially hazardous situation that may result in minor or moderate injury N OTICE Indicates a situation which if not avoi...

Page 10: ... to return end of life equipment producer supplied electrical accessories and all auxiliary items for proper disposal Products marked with this symbol indicates that the product contains toxic or hazardous substances or elements The number inside the symbol indicates the environmental protection use period in years Products marked with this symbol indicates that the product conforms to relevant So...

Page 11: ...mp 13 Power supply connection 2 Measurement chamber see Figure 4 on page 10 8 Input Output connections 14 Rinse valve 3 19 inch panel 9 Reagent pump cover 15 Sample valve 4 Main switch 10 Compressed air valve 16 Reagent canister 5 Peristaltic pump 11 Electronic unit rear 17 Level detector 6 Micro piston pump 12 Power supply box 18 Tube weight 9 ...

Page 12: ... to clean the measurement chamber between measurements Chemical cleaning option The cleaning can be improved with the addition of a chemical reagent to the rinse water Siphon Used to ensure a constant and reproducible volume of sample in the measurement chamber Overflow pipe To avoid any sample overflow from the measurement chamber Reagent additions Reagents and calibration solutions are added to ...

Page 13: ...hould be located in an easily accessible area to facilitate periodic checking of the sample flow rate and for regular maintenance Wherever the analyzer is to be mounted it is important to note that it must be placed in an upright position with the electronic unit No 1 in Figure 3 on page 9 at the top It is recommended to use a spirit level to ensure that the analyzer is correctly positioned and no...

Page 14: ...the analyzer for initial startup Make sure that no backflow occurs in this tube or the other two drainage tubes overflow No 8 in Figure 4 on page 10 and siphon No 5 in Figure 4 on page 10 Note With the cabinet model all three tubes drain into a receptacle with a 50 mm outlet 4 4 Compressed air connection The analyzer requires dry and filtered compressed air at a pressure of 4 to 7 bar It should be...

Page 15: ...les before connecting them to the electronic unit of the analyzer Materials required Shielded cable diameter minimum 4 5 mm maximum 6 mm with 2 or 3 wires depending on function RS232 3 wires Alarm 2 wires etc Metal cable gland Grounding ferrule 2 or 3 protective plugs for the exposed wires Clamp for the grounding ferrule Crimping pliers for the protective plugs Installation 13 ...

Page 16: ...tach the protective plugs to the wires 8 Bring the metal shield up over the ferrule and lock the two together making sure the ferrule is not exposed at the cable end of the shield Bring up the nut to cover the shield 9 Pass the threaded part of the cable gland over the wires and screw into the nut on the cable The cable is now ready to be connected following the procedure described in Connecting p...

Page 17: ...t removed in step 1 to secure in place 4 Pass the rest of the cable through the gland 5 Pull the cable slightly with one hand until the inner shield comes into contact with the gland Tighten the nut onto the gland with the other hand 6 Tighten the nut with a wrench to secure in place It may be necessary to use a second wrench to hold the top nut in place 7 Connect the wires to the correct terminal...

Page 18: ...als on page 14 Once both wires measurement and shield are in place pass them both through the ferrite block Make a loop by passing them through a second time before connecting them to their respective inputs as illustrated in Figure 5 Figure 5 Selective or combined electrode connection For the reference electrode not applicable in the case of a combined electrode and the temperature sensor install...

Page 19: ...zer is factory configured to either 110 220 or 240 VAC Make sure to connect the correct power supply to the analyzer Open the power supply box No 12 in Figure 3 on page 9 Pass the power cable through the cable gland and connect the earth neutral and live wires to terminals 1 2 and 3 respectively as indicated in Figure 7 Figure 7 Power supply box 1 Mains power cable gland 2 Connection terminals 1 E...

Page 20: ... of the analyzer The electronic unit No 11 in Figure 3 on page 9 must be opened from the rear to make these connections Unscrew the four screws holding the unit rear panel and gently swing open from left to right Refer to Figure 8 for terminal locations and the following tables for the functions Note The terminal connectors diagram is also physically located on the rear of the electronic unit Figu...

Page 21: ... 1 3 4 Analog output 2 5 6 Analog output 3 7 8 Analog output 4 9 10 Analog output 5 11 12 Analog output 6 13 14 Analog output 7 15 16 Analog output 8 Table 4 Serial interface J10 Terminal Use 1 TXD RS 232 user configured with X5 2 RXD 3 GND 4 5 6 7 8 Not used Table 5 Accessories 1 J13 Terminal Use 1 11 Heating system 2 3 Mixer 4 5 Rinse valve 6 7 Flush valve 8 9 Sample valve 12 13 Alarm 2 14 15 Al...

Page 22: ... be set to normally open terminals 16 and 17 or normally closed terminals 16 and 18 4 5 3 2 Analog outputs Refer also to Figure 8 on page 18 and Table 3 on page 19 The analog outputs 0 20 mA or 4 20 mA are galvanically insulated The following table shows the allocation of the different outputs 1 channel analyzer 2 channel analyzer I out 1 Terminal 1 2 of J9 Channel 1 I out 2 Terminal 3 4 of J9 Mea...

Page 23: ...are version ANALYZER 8810 00 00 00 ISE X XX 00 00 00 In measurement mode the analyzer sends the following data Measure HH MM SS M1 XXXXEXX XX X C XXX Where MX M1 for channel 1 or M2 for channel 2 XXXXEXX concentration measurement value XX X C temperature XXX value of the potential Where appropriate the analyzer also sends the following messages with a time stamp HH MM SS ACTIONS Cleaning Chemical ...

Page 24: ...alibration error 4 5 4 Additional accessories Any accessories that have been purchased but that have not been factory installed can be installed now Instructions for the installation and wiring are given in the section entitled Additional options on page 37 Once everything has been installed check the following in the measurement chamber Nothing is in contact with the stirrer The upper part of the...

Page 25: ...limited number of parameters can also be displayed using the scroll keys In Command mode the analyzer can be programmed parameters displayed and analyzer functions tested By default the analyzer is in Command mode when first switched on To enter Operating mode from Command mode select START from the MAIN MENU To enter Command mode from Operating mode press Select to display the STOP command then i...

Page 26: ...its measurement type and any activated alarms The bottom line indicates the analyzer status e g calibration titration etc Command mode The top line indicates the main menu The bottom line indicates submenus and data settings User interface 24 ...

Page 27: ...ory has been installed 6 1 System configuration PM XXXX option Refer also to any Installation Procedure documents delivered with the analyzer for application specific information 1 Select PM XXXX with the scrolling keys and press Enter Using the Select key to move from one digit to the next enter the special code and press Enter Option Description ELECTRODE Define the electrode parameters Name Slo...

Page 28: ...measurements are taken alternatively on each channel but calibrations are always made on channel 1 DATE and TIME Set the analyzer date and time parameters 6 2 Calibration CALIBRATION option 6 2 1 Calibration in READING mode The CALIBRATION option is available for viewing the calibration parameters Scroll through the list of parameters as they are displayed 6 2 2 Calibration in PROGRAMMING mode 1 F...

Page 29: ...AUTOMAT CAL1 PT option has been selected Option Description INJ TIME Enter the injection time of the calibration solution in seconds and confirm with Enter CONC Enter the concentration of the calibration solution and press Enter IMMEDIATE Select YES or NO followed by Enter If YES is selected an automatic calibration will start immediately No more input is required 4 If the AUTOMAT CAL 2PTS option ...

Page 30: ...for all future measurements If the new calibration parameters are in Zone 2 it is necessary to CONFIRM the new parameters If YES is selected the new parameters are used for all future measurements If NO is selected the new parameters are rejected and the previous values are used for all future measurements If the new calibration parameters are in Zone 3 the message ERROR CALIBRAT is displayed Pres...

Page 31: ...is available in the PMXXXX Adjust Iout menu option 3 Define the output Option Description OUT Conc Output corresponds to the last measured values OUT Full Output is set to 20 mA OUT Zero Output is set to 0 or 4 mA Note You can only exit this menu when the option Conc is displayed 6 4 Set the alarms and thresholds ALARM option The analyzer has three alarms which are allocated according to the defin...

Page 32: ... is required 2 If FIX TIME is selected Option Description Inj Time PX YYs Adjust the pump action time X pump number 1 to 4 YY time in seconds Adjustable between 0 and 99 seconds 6 6 Test analyzer and accessories SERVICE option Check various physical options e g pumps are working correctly The option to view the version number of the latest installed software is also available from the list 1 Selec...

Page 33: ... in the sample before measurement 6 9 View calibration details CAL PARAMETER option This option lets you view the details of the primary and last calibrations made by the analyzer 1 Select CAL PARAMETER with the scrolling keys and press Enter 2 Use the scroll keys to select LAST CAL or PRIMARY CAL then scroll through the details by pressing Enter 6 10 Measurement cycle parameters TIMING option Def...

Page 34: ...Menu overview 32 ...

Page 35: ...oothly Calibrate if necessary 7 1 3 Software upgrade D AN GE R Electrocution hazard Always make sure the analyzer is turned off and power is disconnected before upgrading the software If a new software version is made available it should be installed as follows 1 Open the electronic unit from the rear and disconnect the data cable from terminal J1 on the measurement board 2 Unscrew the three screw...

Page 36: ...no condition must the electrodes be left in an empty measurement chamber as this will cause them to dry out and become damaged Finally turn the power off 7 2 Troubleshooting Malfunction Possible cause Corrective action High fluctuation of results Irregular sample volume in the measurement cell Siphon working intermittently because of erratic sample flow rinse water when diluting Check sample flow ...

Page 37: ...ditioning solution tubes Check the cleaning parameters Check valves are not leaking Check all tubing for any constriction Sample conditioning Check the quality of the sample conditioning solution Check the sample conditioning parameters Measurement cell clean Conditioning reagents Check the quality of the sample conditioning solution Automatic calibration Increase the frequency of calibrations Sta...

Page 38: ...Maintenance and Troubleshooting 36 ...

Page 39: ...Chemical cleaning 2 Reagent pump or automatic calibration 2 point version 5 Control valve for the dilution system 3 Reagent pump or automatic calibration 2 point version 6 Extra channel Installation instructions for these additional options are described in the following sections NOTIC E A cable gland is provided for each option that must be connected inside the analyzer The cable glands are desig...

Page 40: ...nd power is disconnected before installing this option Figure 11 Automatic calibration option 1 Pump 3 Polyethylene tubing 5 Input block already installed on the analyzer 2 Elbow fitting 4 Connection to attach to top of input block 6 Electric cable Install the pump as follows the numbers in brackets refer to Figure 11 1 Mount the pump 1 in position 4 on the rear of the panel see Figure 10 on page ...

Page 41: ... cleaning D AN GE R Electrocution hazard Always make sure the analyzer is turned off and power is disconnected before installing this option This option allows the addition of a chemical cleaning solution during rinsing The kit includes a pump and a 10 liter canister equipped with a level detector and strainer Figure 12 Chemical cleaning option 1 Tygon tubing 3 Plastic nipple 5 Electric cable 2 Me...

Page 42: ...pare the sample before measurement The kit includes one or two reagent pumps peristaltic or micro piston and one or two 10 liter canisters equipped with level detector and strainer To install the pump s refer to Reagent pumps on page 45 To install the 10 liter canister s refer to Canister kit on page 48 Reconnect power to the analyzer and proceed as follows 1 From the PROGRAMMING menu select SERVI...

Page 43: ...ir inlet from 19 7 PE tubing 3 5 14 PE tubing 3 2 6 4 21 Rinse valve already installed on the analyzer Install the rinsing assembly as follows the numbers in brackets refer to Figure 13 1 Remove the rinse valve 21 2 Unscrew the sample valve 2 from the panel 3 Install the sample valve 2 on the flow block 3 using the supplied fitting 4 4 Screw the new assembly 2 and 3 back on the panel using the two...

Page 44: ...stment screw 17 The system should close as slowly as possible 8 Connect the sample to the input 10 with 12 mm internal diameter tubing pressure 0 5 6 bar 9 Connect the rinse water to the input 11 with 6 mm internal diameter tubing pressure 2 5 6 bar 10 Connect input P on the T connection 18 to the compressed air supply pressure 4 7 bar Dilution reservoir Figure 14 Dilution reservoir 1 Elbow fittin...

Page 45: ...tween the pump 2 and the input block 5 installed on the measurement cell cover using the fitting 4 3 Connect the cable 6 to terminals 1 and 11 of J14 in the electronic unit and make sure that jumper X4 is installed between terminals 2 and 3 and a strap placed between terminals 8 and 10 of J14 refer also to Figure 8 on page 18 and Table 6 on page 20 4 Install the beaker holder mounted externally 5 ...

Page 46: ...Figure 3 on page 9 and screw in finger tight For optimal operation of the heater system the sample in the measurement chamber should cover at least 3 cm of the heating cartridge 2 Connect the cable to terminals 1 and 11 of J13 in the electronic unit refer also to Figure 8 on page 18 and Table 5 on page 19 Reconnect power to the analyzer and proceed as follows 1 From the PROGRAMMING menu select PM ...

Page 47: ...eumatic link between the two valves using the 4 x 6 PE tubing 7 5 Install the assembly on the rear of the panel using the 4 screws 6 Connect the 10 x 12 PE tubing to the output connection of the two valves 3 7 Connect the new cable 8 to terminals 2 and 3 of J14 in the electronic unit refer also to Figure 8 on page 18 and Table 6 on page 20 Reconnect power to the analyzer and proceed as follows 1 F...

Page 48: ...th 2 lateral ridges to prevent any excessive crushing of the pump tubes The cassette is not resistant to acids or high concentration reagents In the event of leakage remove and rinse thoroughly with water Figure 17 Peristaltic pump cassette Tubing The Tygon tubing has been specially designed for use with this cassette The smaller diameter tubes have fittings on the ends for easy connection to larg...

Page 49: ... the pump by pressing laterally on the catch see also Figure 17 3 Remove the pump tubing 4 Install new tubing into the cassette 5 Attach the color coded label to the new tubing 6 Install the cassette on the pump and press until the catch engages 7 Submerge the free end of the tubing into the reagent canister 8 Reconnect power to the analyzer 8 8 2 Micro piston pump D AN GE R Electrocution hazard A...

Page 50: ...ble 3 to the electronic unit according to the pump function refer to Table 6 on page 20 and Table 7 on page 20 3 Replace the cover on the back of the panel using the 4 screws 4 Connect the outlet OUT 1 to the tube 4 using Tygon 1 6 x 3 2 tubing and insert into one of the five slots in the measurement chamber cover 5 Connect the inlet IN 2 to the reagent canister using Tygon 1 6 x 3 2 tubing 8 9 Ca...

Page 51: ...0 Complete power supply board for 8810 Version 2 analyzer and 8811 sequencer 220V Z_359110 40001 Complete power supply board for 8810 Version 2 analyzer and 8811 sequencer 240V Z_359110 40002 Measurement board 08810 A 4000 Version 1 user connection box in plastic Z_08810 A 4500 Version 2 user connection box in metal Z_08810 A 4600 Kit of 30 metallic caps and counter nuts Z_427 010 070 Measurement ...

Page 52: ...ription Item no 2 2 way solenoid valve 610 NW 12 G 3 8 PP sample 359110 02000 3 2 way solenoid valve M 311 NW 2 G 1 8 sample air valve 359110 02100 2 2 way solenoid valve 24 VDC INOX sprinkler water 689 112 031 2 2 way solenoid valve 333 PVDF drain 359110 02200 4 2 way solenoid valve dilution air 599990 04300 Tubing Description Item no Tygon tubing 1 6 x 3 2 151399 90002 Polyethylene tubing 10 12 ...

Page 53: ... ORP electrode 368430 00000 Silver ORP electrode 125 010 003 Copper electrode 125 000 004 Calcium electrode 125 000 002 Low concentration cyanide electrode 368474 00000 Fluoride electrode 368470 00000 Sulphide electrode 368490 00000 Nitrate electrode 125 000 001 Ammonia electrode 125 000 003 Tubing and connection kit 368810 95000 Description Quantity Item no Teflon tubing complete 2 359110 04200 T...

Page 54: ...gon pump tubing 12 grey 4 359090 70015 Tygon tubing 1 6 x 3 1 lg 2000 3 meters 151399 90002 Teflon tubing complete 3 159399 04200 FEP tubing 1 65 x 3 17 lg 350 3 meters 359110 04110 Options Description Item no Wall mounted cabinet complete 368810 40000 Storage canister holder 368810 00100 Free standing cabinet complete 368810 45000 Automatic dilution 08810 A 5060 Automatic dilution without valve o...

Page 55: ... addition NO CLEANING YES NO Chemical cleaning NO SAMPLE COND YES NO Chemical conditioning NO MANUAL YES NO External sample measurement NO SAMPLE TIME Sample injection time 10 seconds HEATING YES NO Regulation in temperature NO Tc Temperature value 25 C DILUTION YES NO Dilution NO 2CHANNELS YES NO Measurement of 2 different samples NO ADJUST Iout OUT 4 20 0 20 mA Output current 0 20 mA Minimum val...

Page 56: ...YCLE TIME Cycle time 15 minutes DELAY TIME Stabilization time before measurement 001 seconds MEASURE t Measurement time 001 seconds SEQUENCE FIX TIME LOOP Measurement sequence LOOP ALARM SYS ALARM ON OFF System alarm OFF WARNING R1 YES NO Warning alarm on alarm relay 1 NO ALARM 1 ON OFF Alarm 1 activation OFF ALARM 1 HIGH LOW High or low alarm HIGH ALARM 1 XXX Threshold value 0 ALARM 2 ON OFF Alar...

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Page 58: ...932 orders hach com www hach com HACH LANGE GMBH Willstätterstraße 11 D 40549 Düsseldorf Germany Tel 49 0 2 11 52 88 320 Fax 49 0 2 11 52 88 210 info de hach com www de hach com HACH LANGE Sàrl 6 route de Compois 1222 Vésenaz SWITZERLAND Tel 41 22 594 6400 Fax 41 22 594 6499 Hach 2013 2015 All rights reserved Printed in Europe ...

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