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ba75802e02

12/2008

pH 3310

Operating manual

pH meter

HOLD

AR

25.0

6.093

pH

°C

USB outp

ut

Menu

15.11

.2008

08:37

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Содержание pH 3210

Страница 1: ...ba75802e02 12 2008 pH 3310 Operating manual pH meter HOLD AR 25 0 6 093 pH C USB output Menu 15 11 2008 08 37...

Страница 2: ...tween this operating manual and your meter Also we cannot guarantee that there are absolutely no errors in this manual Therefore we are sure you will understand that we cannot accept any legal claims...

Страница 3: ...6 4 2 2 Navigation 17 4 2 3 Example 1 on navigation Setting the language 19 4 2 4 Example 2 on navigation Setting the date and time 22 4 3 Sensor independent settings 24 4 3 1 System 24 4 3 2 Data sto...

Страница 4: ...e 57 4 6 1 Options for data transmission 57 4 6 2 Connecting a PC 58 4 7 Reset 59 4 7 1 Resetting the measurement settings 59 4 7 2 Resetting the system settings 60 5 Maintenance cleaning disposal 61...

Страница 5: ...of operating comfort reliability and measuring certainty for all applications The proven calibration procedures and automatic stability control function AR support your work with the pH meter The USB...

Страница 6: ...Softkeys providing situation dependent functions e g F1 Menu Opens the menu for measurement settings F1_ Menu Opens the menu for system settings On Off Switches the meter on or off M Selects the measu...

Страница 7: ...4 Continuous measurement control CMC function 5 Sensor symbol calibration evaluation calibration interval 6 Measured temperature with unit 7 Status line 8 Softkeys and date time HOLD AR 25 0 6 093 pH...

Страница 8: ...ter that cannot return any voltages or currents that are not allowed SELV and current circuit with current limiting Almost all customary sensors fulfill these conditions Connectors 1 pH electrode 2 Re...

Страница 9: ...erience the operators will know the necessary safety precautions to take when handling chemicals Safety instructions Safety instructions in this operating manual are indicated by the warning symbol tr...

Страница 10: ...nd secure technical condition Function and operational safety The smooth functioning and operational safety of the meter can only be guaranteed if the generally applicable safety measures and the spec...

Страница 11: ...ou are in any doubt please contact the supplier of the meter Obligations of the purchaser The purchaser of this meter must ensure that the following laws and guidelines are observed when using dangero...

Страница 12: ...Safety pH 3310 12 ba75802e02 12 2008...

Страница 13: ...led operating manual 3 2 Initial commissioning Perform the following activities z Insert the supplied batteries z Switch on the meter z Set the date and time 3 2 1 Inserting the batteries 1 Unscrew th...

Страница 14: ...on the meter Note The meter has an energy saving feature to avoid unnecessary battery depletion The energy saving feature switches off the meter if no key is pressed during the adjusted interval How t...

Страница 15: ...ries see section 4 3 1 The automatic switch off switches off the meter if no key is pressed for an adjustable period The automatic switch off is not active z if the communication cable is connected z...

Страница 16: ...nd section 4 2 2 4 2 1 Operating modes The meter has the following operating modes z Measurement The measurement data of the connected sensor is shown in the measured value display z Calibration The c...

Страница 17: ...s contain further submenus The selection is made with the keys The current selection is displayed with a frame z Submenus The name of the submenu is displayed at the upper edge of the frame Submenus a...

Страница 18: ...he principles of navigation are explained in the two following sections by reference of examples z Setting the language section 4 2 3 z Setting the date and time see section 4 2 4 Calibration record B...

Страница 19: ...The instrument is in the measuring mode 2 Using F1_ Menu open the Storage config menu The instrument is in the setting mode 3 Select the System submenu with The current selection is displayed with a...

Страница 20: ...etting mode for the Language with ENTER 8 Select the required language with General Measurement Interface Clock Service information Reset System 22 09 2008 08 00 Back Language Deutsch Beep Off Illumin...

Страница 21: ...pH 3310 Operation 21 ba75802e02 12 2008 9 Confirm the setting with ENTER The meter switches to the measuring mode The selected language is active...

Страница 22: ...Therefore check the time at regular intervals Note After a fall of the supply voltage empty batteries the date and time are reset to 01 01 2008 00 00 00 hours Setting the date time and date format Th...

Страница 23: ...lighted 6 Change and confirm the setting with and ENTER The time is set 7 If necessary set the Date and Date format The setting is made similarly to that of the time 8 If necessary select and set the...

Страница 24: ...ndependent system settings to the default condition Settings To open the Storage config menu press the F1_ Menu or ENTER key in the measured value display After completing the settings switch to the m...

Страница 25: ...ace Output format ASCII CSV Output format for data transmission For details see section 4 6 System Interface Output header Output of a header for Output format CSV System Clock Time Date Date format S...

Страница 26: ...a considerable impact on the reproducibility of measured values You can activate or switch off the automatic Stability control function see section 4 3 1 The measured parameter flashes on the display...

Страница 27: ...ted in electrode z Manual determination and input of the temperature The meter recognizes whether a suitable sensor is connected and automatically switches on the temperature measurement The display o...

Страница 28: ...the Stability control function is prematurely terminated the current measurement data are output to the interface without AutoRead info 1 Perform the preparatory activities according to section 4 4 1...

Страница 29: ...al The minimum duration until a measured value is assessed as stable is the monitored time interval The actual duration is mostly longer 3 Release the frozen measured value again with AR or M The AR s...

Страница 30: ...26 in the System menu Note You can prematurely terminate the Stability control function manually with ENTER at any time If the Stability control function is 1 Perform the preparatory activities accor...

Страница 31: ...s are stable within the monitored time interval The minimum duration until a measured value is assessed as stable is the monitored time interval The actual duration is mostly longer 3 Release the froz...

Страница 32: ...lay with M Menu item Possible setting Description Calibration Calibration record Displays the calibration record of the last calibration Calibration Buffer TEC NIST DIN ConCal Buffer sets to be used f...

Страница 33: ...he selected unit Resolution pH 0 001 0 01 0 1 Resolution of the pH display Resolution mV 0 1 1 Resolution of the mV display Stability control On Off Switches on or off the automatic stability control...

Страница 34: ...bination electrode z When the calibration interval has expired Buffer sets for calibration You can use the buffer sets quoted in the table for an automatic calibration The pH values are valid for the...

Страница 35: ...C 10 Mettler Toledo USA 1 679 4 003 7 002 10 013 25 C 11 Mettler Toledo EU 1 679 4 003 7 002 10 013 25 C 12 Fisher 2 007 4 002 7 004 10 002 25 C 13 Fluka BS 4 006 6 984 8 957 25 C 14 Radiometer 1 678...

Страница 36: ...in the menu pH F1 Menu Calibration Buffer see page 32 18 Hamilton Duracal 4 005 7 002 10 013 25 C 19 Precisa 3 996 7 003 8 999 25 C 20 Reagecon TEC 2 000 4 010 7 000 10 000 25 C 21 Reagecon 20 2 000 4...

Страница 37: ...epting the current value Calibration record The new calibration values are displayed when the calibration is finished Display calibration and output to interface You can have the data of the last cali...

Страница 38: ...pH 3310 Ser no 08502113 CALIBRATION pH 31 10 2008 16 13 33 AutoCal TEC Buffer 1 4 01 Buffer 2 7 00 Buffer 3 10 01 Voltage 1 184 0 mV 24 0 C Voltage 2 3 0 mV 24 0 C Voltage 3 177 0 mV 24 0 C Slope 60...

Страница 39: ...ate after the calibration interval has expired Setting the calibration interval The calibration interval is set to 7 days d7 in the factory You can change the interval 1 999 days 1 Connect the pH comb...

Страница 40: ...procedure is identical Note If single point calibration is set in the menu the calibration is automatically terminated after measurement of buffer solution 1 and the calibration record displayed 1 In...

Страница 41: ...he next buffer appears 7 If necessary terminate the calibration as a single point calibration with M The calibration record is displayed pH 181 3mV 24 8 C AutoCal 4 010 22 09 2008 08 00 AR TEC pH 2 18...

Страница 42: ...erminate the calibration as a two point calibration with M The calibration record is displayed pH 1 3mV 24 8 C AutoCal 7 000 22 09 2008 08 00 AR TEC pH 3 1 3mV 24 8 C AutoCal 22 09 2008 08 00 TEC 14 T...

Страница 43: ...last buffer of a buffer set has been measured Then the calibration record is displayed Note The calibration line is determined by linear regression 18 Use M to finish calibration or switch to calibra...

Страница 44: ...he buffer set see section 4 4 4 Note If single point calibration is set in the menu the calibration is automatically terminated and the calibration record displayed 1 In the measured value display sel...

Страница 45: ...lity control to be completed Set the nominal buffer value for the measured temperature with 8 Take over the calibration value for the asymmetry with ENTER The calibration display for the next buffer a...

Страница 46: ...e buffer manually and enter it with 13 Start the measurement with ENTER The measured value is checked for stability stability control 14 Wait for the measurement with stability control to be completed...

Страница 47: ...e found in the menu Storage config Data storage Calibration data storage To open the Storage config menu press the F1_ Menu key in the measured value display Menu item Setting function Description Dat...

Страница 48: ...printout 31 10 2008 16 55 pH 3310 CALIBRATION pH 31 10 2008 16 13 33 AutoCal TEC Buffer 1 4 01 Buffer 2 7 00 Buffer 3 10 01 Voltage 1 184 0 mV 24 0 C Voltage 2 3 0 mV 24 0 C Voltage 3 177 0 mV 24 0 C...

Страница 49: ...is available white Measured values in this range are suitable for documentation 2 Measuring range for which no valid calibration is available light gray Measured values in this range are not suitable...

Страница 50: ...value of the connected sensor z Measured temperature value of the connected sensor z AutoRead info AR appears with the measured value if the AutoRead criterion was met while storing stable measured va...

Страница 51: ...process and switch to the measured value display confirm No Then you can e g transmit the stored data to a PC see section 4 5 3 and subsequently erase the storage see section 4 5 4 1 Press the STO key...

Страница 52: ...the STO_ key The menu for automatic storage appears Adjusted entire storage duration Max available storage duration Graphical display of the storage usage ID number 1 Interval 30 s Duration 180 min C...

Страница 53: ...the automatic storing function is active the meter provides an energy saving mode Eco mode to avoid unnecessary energy consumption The energy saving mode switches off functions of the meter that are...

Страница 54: ...the automatic storage function before the adjusted storage duration has expired 1 Press the STO_ key The following window appears 2 Using select Yes and confirm with ENTER The meter switches to the me...

Страница 55: ...in the measured value display Note The settings are explained here using the manual storage as an example The same settings and functions are available for the automatic storage Settings Menu item Se...

Страница 56: ...ack 4 5 4 Erasing the measurement data storage How to erase the measurement data storage is described in section 4 5 3 EDITING THE MEASURED VALUE STORAGE Manual data storage 200 Data record 3 of 64 30...

Страница 57: ...ds Data Control Operation description Current measured values of all connected sensors Manual z With F2 USB output z Simultaneously with every manual storage process see section 4 5 1 Automatic at int...

Страница 58: ...iver on the PC System requirements of the PC for installation of the USB driver z PC with Pentium processor or higher with at least one free USB connection and CD ROM drive z Windows 2000 XP Vista 1 I...

Страница 59: ...set pH The following settings for pH measurements are reset to the default settings with the Reset function The sensor settings are reset under the Reset menu item in the measuring menu To open the se...

Страница 60: ...delivery status The system settings are reset in the menu Storage config System Reset To open the Storage config menu press the F1_ Menu key in the measured value display Setting Default settings Lang...

Страница 61: ...y you can also use Ni MH rechargeable batteries type Mignon AA In order to charge the batteries an external charging device is required Caution Make sure that the poles of the batteries are positioned...

Страница 62: ...that contain solvents Remove any splashes immediately 5 3 Packing This meter is sent out in a protective transport packing We recommend Keep the packing material The original packing protects the mete...

Страница 63: ...able broken Replace combination electrode Gel electrolyte dried out Replace combination electrode Cause Remedy pH combination electrode The values determined for zero point and slope of the combinatio...

Страница 64: ...ure with air excluded if necessary Temperature not stable Adjust temperature if necessary Combination electrode test sample Conductivity too low Use suitable combination electrode Temperature too high...

Страница 65: ...ode Temperature difference between buffer and test sample too high Adjust temperature of buffer or sample solutions Measurement procedure not suitable Follow special procedure Cause Remedy Operating c...

Страница 66: ...What to do if pH 3310 66 ba75802e02 12 2008...

Страница 67: ...e batteries 4 x 1 2 V NiMH rechargeable batteries type AA no charging function Operational life up to 1000 h without 150 h with illumination Sensor input Input resistance 5 1012 ohm Input current 1 10...

Страница 68: ...2 0 20 0 0 1 2 00 20 00 0 01 2 000 19 999 0 001 U mV 1200 0 1200 0 0 1 2500 2500 1 T C 5 0 105 0 0 1 T F 23 0 221 0 0 1 Manual temperature input Variable Range Increment Tmanual C 25 130 1 Tmanual F...

Страница 69: ...ted in a commercial environment This equipment generates uses and can radiate radio frequency energy and if not installed and used in accordance with the instruction manual may cause harmful interfere...

Страница 70: ...Technical data pH 3310 70 ba75802e02 12 2008...

Страница 71: ...used when the measuring system is adjusted at the same time see adjusting Electromotive force of a combination electrode The electromotive force U of the combination electrode is the measurable elect...

Страница 72: ...The electrical current remains constant Reset Restoring the original condition of all settings of a measuring system Resolution Smallest difference between two measured values that can be displayed by...

Страница 73: ...mmissioning 13 14 Initialize 59 Interval calibration 39 K Keys 6 M Measured value display 17 Measurement accuracy 39 Measurement data memory Edit 55 Erase 55 Storage locations 50 Measurement dataset 5...

Страница 74: ...Lists pH 3310 74 ba75802e02 12 2008 pH 42 Transmitting data 57 Transmitting measured values 57 Two point calibration pH 41 44 46 Z Zero point of pH combination electrode 34...

Страница 75: ...new software version see page 65 1 Install the downloaded firmware update on a PC An update folder is created in the Windows start menu If an update folder already exists for the meter or meter type t...

Страница 76: ...Appendix Firmware update pH 3310 76 ba75802e02 12 2008...

Страница 77: ......

Страница 78: ...Wissenschaftlich Technische Werkst tten GmbH Dr Karl Slevogt Stra e 1 D 82362 Weilheim Germany Tel 49 0 881 183 0 49 0 881 183 100 Fax 49 0 881 183 420 E Mail Info WTW com Internet http www WTW com...

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