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Chapter 4



pH, pH/ISE and pH/LogR Measurement Modules



Orion Versa Star Pro Meter User Manual

Thermo Scientific

Press the





key to highlight a menu option and press the





key to highlight a

submenu option. Onscreen text prompts provide instructions for changing parameters
within a selected menu option.

Use the popup alphanumeric keypad screen for menu options including Electrode
Serial Number and Sample ID.

Press the









key to highlight a character, press the f2 (Enter) key

to input the character and repeat until the desired name is entered.

ii.

Press the f3 (Clear) key to delete any undesired characters.

iii.

Press the f1 (Done) key to save the entry.

Содержание Orion Versa Star Pro

Страница 1: ...Orion Versa Star Pro Electrochemistry Meters UserManual 68X000791 Revision B May 2018...

Страница 2: ......

Страница 3: ...ngle Dual or Multiple Channel Displays 16 Measurement Display Examples 18 Additional Measurement Display Icons 19 pH Electrode Condition Icon 20 Customizing the Display 21 Meter and Module Maintenance...

Страница 4: ...r 5 74 Conductivity Measurement Module 74 Connecting Electrodes to the Module 74 Channel 1 4 Setup Menus 75 Mode Menus for Conductivity TDS Salinity and Resistivity 75 Conductivity Calibration 80 Auto...

Страница 5: ...rodes and Solutions 126 Appendix A 128 Channel Specific Settings and Features 128 General Mode Settings 128 Sample ID 128 Stability 129 Averaging 129 Alarms 129 pH and ISE Mode Settings 130 Buffer Gro...

Страница 6: ...ith temperature including LogR technology that measures sample temperature using a glass bulb pH electrode no separate ATC probe needed in samples VSTAR CND module measures conductivity TDS salinity o...

Страница 7: ...ation fast and simple The meter interface can be set to a variety of languages Packing List Versa Star Pro meters and meter kits include the following items Meter attachable electrode stand Universal...

Страница 8: ...y for use with Versa Star Pro meters Use of other power adapters can damage the meter and void the warranty The use of a surge protector or uninterrupted power supply UPS is also recommended 1 Select...

Страница 9: ...the stand will be installed on and remove the screw between the circles on that side of the meter 4 Align the base plate of the stand with the circles on the meter 5 Replace the screw from step 3 to a...

Страница 10: ...ngs Communication Printing Printing Format in the Instrument Settings setup menu to ensure the meter output settings are correct to interface the meter with a printer or computer The following image s...

Страница 11: ...key when two or more modules are connected to the meter to change the measurement display to show each channel individually or a combination of two or more channels simultaneously measure esc Press t...

Страница 12: ...ey to scroll down through a list of items Press to enter a value of eight 8 when using the numeric keypad log view Press the log view key to access the data log and calibration log from the measuremen...

Страница 13: ...ude the option to also measure temperature Module Catalog VSTAR PH VSTAR ISE VSTAR LR VSTAR CND VSTAR RD Label pH pH ISE pH LogR Cond RDO DO Measure Modes pH pH pH Conductivity Saturation mV mV mV TDS...

Страница 14: ...the module is fully connected to the meter 3 Release the top and bottom tabs on the module 4 If the meter is powered on it will automatically recognize the module and update the channel ID display top...

Страница 15: ...es meters Make sure the module is properly inserted in the meter and the meter is connected to a power source using the included universal power adapter Module Catalog VSTAR PH VSTAR ISE VSTAR LR VSTA...

Страница 16: ...test Versa Star software and all Versa Star Pro software revisions View Format Displayed Information Customizable Measurement Dependent Single Channel Channel 1 Channel 2 Channel 3 Channel 4 Channel I...

Страница 17: ...Number Measure Mode Method Number Read Type AR TM SS Icons Stabilizing Ready Indicator Main Measurement with Units Secondary Measurement with Units Temperature with Units and Source Example Three Cha...

Страница 18: ...ment ISE condition icon and slope value of most recent active calibration Date and time Method Temperature measurement and source Main measurement units mV corresponding to main measurement pH electro...

Страница 19: ...play as High Limit Alarm Low Limit Alarm Cal Due Alarm or Set Point Alarm Alarm must be enabled in the channel specific setup menu Channel ID for measurement modules connected to meter Channel number...

Страница 20: ...active account when the System Access feature is enabled Electrode ID Icon Shown with the electrode serial number or name entered using a channel specific setup menu Sample ID Icon Shown with the samp...

Страница 21: ...o highlight an item and press the f3 Select key to check display or uncheck hide the item Some items will only be shown in the single channel display when checked 5 Press the f1 Done key and then pres...

Страница 22: ...on and data history and perform a meter self test or view meter and module serial number and software revisions Since the Versa Star Pro meter offers four channels that can be configured in any combin...

Страница 23: ...e channel icon shows the current measure mode i e pH ISE Cond RDO for the module Use the Channel 3 setup menu to customize the measurement parameter settings for the module connected to the meter inpu...

Страница 24: ...or the selected channel and module Refer to the individual module chapters for detailed information on the available settings for each measure mode Use the Temperature menu to set the temperature unit...

Страница 25: ...TC MAN Temperature Cal MAN Ch ATC Ch LogR All ATC Module and setting dependent Incremental Techniques Module dependent Single Known Addition The Incremental Techniques menu is displayed only when the...

Страница 26: ...the same VSTAR CND conductivity module Edit Create 1 In the measurement mode press the setup key 2 Press the or key to highlight Channel 1 Channel 2 Channel 3 or Channel 4 and press the f3 Select key...

Страница 27: ...t channel Copy Use the copy function to duplicate an existing custom method measure mode settings and setup parameters to a new or different method If two or more channels have the same measurement ca...

Страница 28: ...ress the f3 Select key d For the conductivity module press the or key to highlight the conductivity TDS Salinity or Resistivity measure mode and press the f3 Select key e The RDO DO module will procee...

Страница 29: ...Temperature Unit and press the or key to highlight C or F as the displayed temperature units 5 Press the measure esc key to return to the measurement mode Temperature Input The temperature source for...

Страница 30: ...calibration is applied to all future temperature measurements recalibrate the temperature if a different ATC probe is used ATC Probe Temperature Calibration Prepare and connect all ATC probes to be c...

Страница 31: ...l temperature value when MAN is selected in the Temperature Input menu 1 In the measurement mode press the setup key 2 Press the or key to highlight Channel 1 Channel 2 Channel 3 or Channel 4 and pres...

Страница 32: ...arm is triggered Stirrer Connect one or two Orion Star stirrer probes Cat No 096019 to the meter assign a stirrer probe to each measurement channel and set the stirring speed of each stirrer probe fro...

Страница 33: ...hannel 2 4 Channel 3 4 Channel 1 2 3 Channel 1 2 4 Channel 1 3 4 Channel 2 3 4 Channel 1 2 3 4 Communication USB RS232 1200 2400 4800 9600 19200 38400 57600 115200 USB PRINTER Buzzer Key Press Off On...

Страница 34: ...o highlight Log View and press the f3 Select key 3 Press the or key to highlight Data Log 4 To view the log press the or key to highlight View and press the f3 Select key A list of the saved data log...

Страница 35: ...30 calibrations have been saved for a parameter the meter will not overwrite an existing calibration log with a new calibration until the calibration log is manually deleted This function is helpful...

Страница 36: ...te drift and noise of the electrode Self Test Tests the keypad meter accuracy and stirrer inputs A self test is also performed automatically by the meter at each power up About Meter Displays the mete...

Страница 37: ...to the meter functions listed the in following table Meter Access Options Admin Full Advanced Basic Custom Create Edit Accounts Instrument Settings Data Log Delete Calibration Log Delete Diagnostics...

Страница 38: ...Select key 3 Press the f3 Admin key to proceed with setting up the administrator account 4 Press the or key to highlight Admin Name and press the f3 Edit key Use the alphanumeric keypad to enter one t...

Страница 39: ...ist of accounts will be shown with the Admin account and ten available user accounts 9 Press the or key to highlight a new user account and press the f3 Edit key 10 Press the or key to highlight Accou...

Страница 40: ...or Basic is selected press the f2 Save key and the meter will use the preset access level settings and return to the list of accounts b If Custom is selected press the f3 Select key and a new screen...

Страница 41: ...n in the single measurement display c The active account will only be able to access the meter functions defined by their account s access level setting Full Advanced Basic or Custom d The active acco...

Страница 42: ...ll open From this screen the system administrator can edit their name and password create a new user account edit an existing user account load an existing account or turn off the System Access featur...

Страница 43: ...he measurement mode and the loaded activated account name will be shown in the single measurement display Logging Out of Existing User Account 1 In the measurement mode press the setup key 2 Press the...

Страница 44: ...pter 2 Meter Basics for instructions For information on customizing meter settings refer to Chapter 3 Setup Menu It is recommended that electrodes be placed in the meter attached electrode stand for e...

Страница 45: ...lectrode with BNC connector is used 5 Prepare the electrodes for use as instructed in the electrode user manuals VSTAR ISE Versa Star pH ISE Module 1 Remove the shorting cap protecting the BNC connect...

Страница 46: ...to the 8 pin MiniDIN connector on the module 4 Connect a reference half cell electrode to the pin tip connector on the module for use when a half cell sensing electrode with BNC connector is used 5 Pr...

Страница 47: ...available This section provides detailed information on the Mode menus for each measurement parameter available when using a pH pH ISE or pH LogR module 1 In the measurement mode press the setup key...

Страница 48: ...pts provide instructions for changing parameters within a selected menu option a Use the popup alphanumeric keypad screen for menu options including Electrode Serial Number and Sample ID i Press the o...

Страница 49: ...aging Off Automatic Smart Set averaging for faster measurement stability Read Type Auto Read Timed Single Shot Continuous For Timed and Single Shot set the time in hours minutes seconds HH MM SS using...

Страница 50: ...y Smart Fast Medium Slow Set when a measurement is recognized as stable Averaging Off Automatic Smart Set averaging for faster measurement stability Read Type Auto Read Timed Single Shot Continuous Fo...

Страница 51: ...it 3 Digit 4 Digit Set how many significant digits will be shown for the resolution of the measurement value Stability Smart Fast Medium Slow Set when a measurement is recognized as stable Averaging O...

Страница 52: ...stirrer probe the stirrer probe will start stirring when the f3 Start key is pressed and stop stirring when the reading stabilizes 4 Wait for the pH value on the meter to stabilize and perform one of...

Страница 53: ...mpts and function keys update with the appropriate instructions and options Example 4 While each pH buffer is being read the display shows the previous calibration points with corresponding mV and tem...

Страница 54: ...the or key to highlight the desired channel and press the f3 Select key 2 Rinse the electrode and any other electrodes in use with distilled water blot dry with a lint free tissue and place into the s...

Страница 55: ...inputs on the selected channel In the measurement mode press the channel key until the channel with the pH pH ISE or pH LogR module with ORP electrode connected is shown If needed press the mode key...

Страница 56: ...ctrodes in use with distilled water or rinse solution required for that electrode Blot the electrode dry with a lint free tissue or shake the electrode and then place into the standard Do not wipe or...

Страница 57: ...tup key 2 Press the or key to highlight Channel 1 Channel 2 Channel 3 or Channel 4 and press the f3 Select key a Select the appropriate channel number that the ATC probe of interest is connected 3 Pre...

Страница 58: ...nnel 2 Channel 3 or Channel 4 and press the f3 Select key a Select the appropriate channel number that the manual temperature will be applied 3 Press the or key to highlight Temperature and press the...

Страница 59: ...LogR temperature calibration can be performed It is recommended that at least two calibration points be used to meet optimum system accuracy Choose a temperature calibration range that is 5 C to 20 C...

Страница 60: ...that will be used for the LogR mode i e Ch2 LogR This enables the LogR mode for the selected channel and allows a LogR temperature calibration to be performed 5 Press the or key to highlight Temperatu...

Страница 61: ...ion in the beaker Electrode interferences should be at a minimum since the effect of the interference might change as the concentration of the ion of interest changes This situation may also result in...

Страница 62: ...he measurement mode press the channel key until the channel with the pH ISE module with ISE connected is shown If needed press the mode key until ISE Measurement is shown as the measure mode and use t...

Страница 63: ...e measurement mode press the setup key 2 Press the or key to highlight Channel 1 Channel 2 Channel 3 or Channel 4 and press the f3 Select key 3 Press the or key to highlight Method and press the f3 Se...

Страница 64: ...key a Select the appropriate channel number that the ISE is connected 5 Press the or key to highlight Incremental Techniques and press the f3 Select key 6 Press the or key to highlight Double Known A...

Страница 65: ...ey 3 Press the or key to highlight Method and press the f3 Select key 4 Press the or key to highlight Edit Create and press the f3 Select key 5 Press the or key to highlight a new method and press the...

Страница 66: ...the instructions in the electrode user manual Prepare all required solutions ionic strength adjusters standards etc and review any special requirements outlined in the electrode user manual Connect th...

Страница 67: ...to perform another analysis Saving the Incremental Technique as a Method For frequently used incremental techniques Versa Star Pro meters now allow individual incremental techniques to be stored as m...

Страница 68: ...ress the channel key until the channel with the pH ISE module with ISE connected is shown If needed press the mode key until ISE Measurement is shown as the measure mode and use the ISE Mode Menu to s...

Страница 69: ...ow individual incremental techniques to be stored as methods 1 In the measurement mode press the setup key 2 Press the or key to highlight Channel 1 Channel 2 Channel 3 or Channel 4 and press the f3 S...

Страница 70: ...the measurement mode press the channel key until the channel with the pH ISE module with ISE connected is shown If needed press the mode key until ISE Measurement is shown as the measure mode and use...

Страница 71: ...n the measurement mode press the setup key 2 Press the or key to highlight Channel 1 Channel 2 Channel 3 or Channel 4 and press the f3 Select key 3 Press the or key to highlight Method and press the f...

Страница 72: ...red solutions ionic strength adjusters standards etc and review any special requirements outlined in the electrode user manual Connect the ISE and any other electrodes to be used to the module inputs...

Страница 73: ...Technique as a Method For frequently used incremental techniques Versa Star Pro meters now allow individual incremental techniques to be stored as methods 1 In the measurement mode press the setup key...

Страница 74: ...ngs refer to Chapter 3 Setup Menu It is recommended that electrodes be placed in the meter attached electrode stand for easy movement in and out of beakers during calibration sample measurement and st...

Страница 75: ...easurement parameter available when using a conductivity module 1 In the measurement mode press the setup key 2 Press the or key to highlight Channel 1 Channel 2 Channel 3 or Channel 4 and press the f...

Страница 76: ...meric keypad screen for menu options including Electrode Serial Number and Sample ID i Press the or key to highlight a character press the f2 Enter key to input the character and repeat until the desi...

Страница 77: ...ure Temperature Coeff 2 10 Enter the temperature coefficient value for linear temperature compensation Stability Smart Fast Medium Slow Set when a measurement is recognized as stable Averaging Off Aut...

Страница 78: ...displayed TDS measurements will be reported to using the selected temperature compensation Temp Compensation Linear nLFn nLFu EP Off Set the temperature compensation type used to calculate and report...

Страница 79: ...e Menu Main Menu Settings Details Read Type Auto Read Timed Single Shot Continuous For Timed and Single Shot set the time in hours minutes seconds using the arrow keys Cell K 0 475 Enter the nominal c...

Страница 80: ...ion 100 S cm 1413 S cm and or 12 9 mS cm conductivity standards 1 Press the f1 Cal key to start the calibration a If more than one channel is displayed in the measurement mode press the or key to high...

Страница 81: ...lues from 15 C to 30 C Refer to the Appendix section of this user manual for additional values from 0 to 50 C Temperature C Orion 111 9mS cm Standard Cat No 011005 01100510 mS cm Orion 12 9mS cm Stand...

Страница 82: ...for the cell constant value on the meter to stabilize 3 Press the f2 Accept key to accept the displayed value or press the f3 Edit key press the f3 Clear key use the numeric keypad to enter the cell c...

Страница 83: ...ghlight the desired channel and press the f3 Select key 3 Press the f2 Cell K key wait for the cell constant value on the meter to stabilize and press the f3 Clear key Use the numeric keypad to enter...

Страница 84: ...s recommended that electrodes be placed in the meter attached electrode stand for easy movement in and out of beakers during calibration sample measurement and storage VSTAR RD Versa Star RDO Dissolve...

Страница 85: ...Channel 1 Channel 2 Channel 3 or Channel 4 and press the f3 Select key a Select the appropriate channel number that the module of interest is connected 5 Press the or key to highlight Mode and press t...

Страница 86: ...e the built in barometer or Manual to enter a value Select the Auto option to calibrate the barometer pressure reading Salinity Correction Auto Manual Set the salinity correction source as Auto to use...

Страница 87: ...ically used to calibrate the DO probe to the value achieved by a Winkler titration Due to possible titration errors this method is inherently less accurate Set Zero This method uses an oxygen free sol...

Страница 88: ...tirring when the f3 Start key is pressed and stop stirring when the reading stabilizes 5 Wait for the dissolved oxygen value on the meter to stabilize and press the f2 Accept key a 100 0 will be displ...

Страница 89: ...ount of cobalt salt can be added to the sodium sulfite solution to act as an indicator and change color when the sodium sulfite solution no longer has zero oxygen content 1 Press the f1 Cal key to sta...

Страница 90: ...hen two or more modules are connected to the meter pressing the channel key will change the number and combination of channels displayed in the measurement mode Each channel can be displayed individua...

Страница 91: ...Example Measurement Mode and Channel Displays pH Mode Display mV Mode Display RmV Mode Display ORP Mode Display ISE Mode Display pH LogR Mode Display Conductivity Mode Display Dissolved Oxygen Mode Di...

Страница 92: ...e using the or key to scroll to the hours HH minutes MM or seconds SS field and the or key to increase or decrease the value Press the f1 Done key to confirm the value 6 Press the measure esc key to r...

Страница 93: ...meter and displayed in the measurement mode the Versa Star Pro meter will use a priority structure to determine when the displayed measurements are sent to the data log and external devices if they ar...

Страница 94: ...stirrer probe the stirrer probe will start stirring when the measure esc key is pressed and stop stirring when the predefined wait time has elapsed d Continuous Measurements will start immediately whe...

Страница 95: ...sample measurement and storage The included electrode stand can be attached to either side of the meter The recommended electrode positions for the electrode holder portion of the stand are shown belo...

Страница 96: ...rements will be saved to the data log and then transferred to a computer or printer make sure the data log is enabled in the setup menu the meter communication settings match the computer or printer s...

Страница 97: ...0000 M 101 02 Aug 12 3 40 PM USER 01 5 1 pH 2 mV 290 5 25 0 C MAN Auto Manual 2 pH 4 01 mV 174 3 25 0 C MAN Auto Manual 3 pH 6 997 mV 0 0 25 0 C MAN Auto Manual 4 pH 10 013 mV 173 7 25 0 C MAN Auto Ma...

Страница 98: ...in the search option Click the Browse button and set the computer desktop as the location Click the Next button 7 Wait while the driver is loaded and accept any warning messages Once the installation...

Страница 99: ...power adapter from the meter 4 Connect the USB cable included with meter to the MINI B USB input on the back of the meter and USB input on the computer 5 Press and hold down the f1 key on the meter ke...

Страница 100: ...older and wait for the file to transfer completely about one minute 10 Disconnect the power adapter and USB cable from the meter 11 Reconnect the power adapter to the meter and ensure uninterrupted po...

Страница 101: ...ate Laptop computers must also be plugged into a power supply when running the software update performing the software update while the computer is on battery power is not recommended Printer Requirem...

Страница 102: ...so the data string ends with a new line instead of overwriting the last line of data with new data string 7 Set the meter communication settings using the Instrument Settings setup menu Communication...

Страница 103: ...LLOG X CR Prints all the logged calibration data If no calibration is available will return to receive next command X Select calibration data for specific mode as a number PH 1 COND 6 RMV 3 DO 10 ORP...

Страница 104: ...ls enter channel numbers without commas c Example SETCHANNEL 1 CR 2 SETREADTYPE X 1 CR a X Channel number b Y Read Type 1 Auto Read c Z leave blank d Example SETREADTYPE 1 1 CR 3 GETMEAS CR a Prints t...

Страница 105: ...SETRTC SETRTC YY MM DD HH MM SS CR Set the date and time in 24 hour format for the meter Example SETRTC 18 03 29 15 00 00 GETCHCONFIG GETCHCONFIG CR Prints the meter channel configuration with mode d...

Страница 106: ...Sample ID User ID Module Serial Number Mode Electrode Type ISE Value ISE Unit mV Value mV Unit Temperature Value Temperature Unit Average Slope Value Average Slope Unit Method Number Example Versa St...

Страница 107: ...lue Current Unit Solution Temperature Value Solution Temperature Unit Membrane Temperature Value Membrane Temperature Unit Barometric Pressure Value Barometric Pressure Unit Salinity Correction Value...

Страница 108: ...Value RDO Saturation Unit Partial Pressure in Torr Solution Temperature Value Solution Temperature Unit Barometric Pressure Value Barometric Pressure Unit Salinity Correction Value in ppt Slope Value...

Страница 109: ...r Example VERSA STAR V00000 2 73 Ch 1 SENSOR 01 VA12345 M 101 15 03 14 1 30 30 PM USER 01 199 8 RmV 199 7 mV 25 0 C MAN 0 1 mV 101 CR ORP Meter Type Meter Serial Number Meter Software Revision Channel...

Страница 110: ...le Volume Unit Total Volume Value Total Volume Unit Standard Concentration Value Standard Concentration Unit Reaction Ratio known subtraction only Measured Sample Value Measured Sample Unit First Stan...

Страница 111: ...Unit Slope Value Slope Unit Calibration Log Number Example VERSA STAR V00000 2 73 Ch 4 SENSOR 04 VA12345 M 401 15 03 14 1 30 30 PM USER 01 102 3 1334 9 nA 0 0 nA 23 8 C ATC 24 0 C ATC Auto 760 0 mmHg...

Страница 112: ...contact your local Technical Sales Representative Product Specialist or Technical Support Team Americas Technical Support Team Phone 1 978 232 6000 US Toll free Phone 1 800 225 1480 US toll free Emai...

Страница 113: ...ue freezes and will not change The read type is set to Auto Read mode AR icon shown on the display Press the measure esc key to take a new measurement or use the setup menu to change the read type to...

Страница 114: ...NC inputs and press the f3 Start key to begin the test b The test results for all channels with a module that has a BNC input will be displayed and Pass should be indicated for all channels Press the...

Страница 115: ...r more recycling disposal companies in each EU Member State and this product should be disposed of or recycled through them Further information on compliance with these directives the recyclers in you...

Страница 116: ...rations per measure mode with time and date stamp Computer Software Orion Navigator Pro computer software Cat No VSTAR NPUSB Methods 10 per channel 40 total Communication Ports RS232 bidirectional USB...

Страница 117: ...mber VSTAR PH pH Range 2 000 to 20 000 Resolution 0 1 0 01 0 001 Relative Accuracy 0 002 Calibration Points Up to 6 Calibration Editing Yes Adjustable ISO Point Yes Input Impedance 10 12 ohms mV RmV R...

Страница 118: ...ble Relative Accuracy 0 2 mV or 0 05 of reading whichever is greater Units ppm Molar mg L ppb none Calibration Points Up to 6 Calibration Editing Yes Adjustable ISO Point Yes Advanced Features Segment...

Страница 119: ...mV Mode Yes EH ORP Mode Yes Temperature manual or automatic with ATC probe Range 5 to 105 C 22 to 221 F Resolution 0 1 C 0 1 F Relative Accuracy 0 1 C 0 1 F Offset Calibration 1 point Source Options...

Страница 120: ...ing Yes TDS Range 0 001 to 200 0 ppm Resolution 0 001 ppm minimum auto ranging up to 4 significant digits Relative Accuracy 0 5 of reading 1 digit TDS Factor Linear 0 02 to 9 99 or ISO EN 27888 Salini...

Страница 121: ...metric Pressure Correction 450 to 850 mmHg automatic using built in barometer or manual entry Salinity Factor Correction 0 to 45 ppt automatic using conductivity module and probe or manual entry Calib...

Страница 122: ...R PH 8302BNUMD ROSS Ultra Triode glass refillable pH ATC electrode 096019 Meter powered stirrer probe 810199 ROSS pH buffer and storage solution kit VSTAR13 Versa Star Pro meter with electrode stand u...

Страница 123: ...e 810199 ROSS pH buffer and storage solution kit VSTAR40B Versa Star Pro meter with electrode stand universal power adapter literature USB computer cable and meter test certificate 2 Versa Star pH ISE...

Страница 124: ...n kit VSTAR90 Versa Star Pro meter with electrode stand universal power adapter literature USB computer cable and meter test certificate Versa Star pH ISE measurement module VSTAR ISE Versa Star condu...

Страница 125: ...ered stirrer probe 810199 ROSS pH buffer and storage solution kit 011007 1413 S conductivity standard 5 x 60 mL 080513 DO probe maintenance kit BOD adapter funnel and stirrer VSTAR94 Versa Star Pro me...

Страница 126: ...llable pH electrode BNC connector 8165BNWP ROSS Sure Flow epoxy body refillable pH electrode BNC connector 8302BNUMD ROSS Ultra Triode glass body refillable pH ATC electrode BNC MiniDIN connectors 815...

Страница 127: ...ndard premixed with TISAB II 475 mL 040907 Orion 2 ppm fluoride standard premixed with TISAB II 475 mL 040908 Orion 10 ppm fluoride standard premixed with TISAB II 475 mL 9707BNWP Orion nitrate ion se...

Страница 128: ...acters long The entered sample ID will be recorded with subsequent measurements and saved to the data log or exported to an external device depending on the meter communication settings in the Instrum...

Страница 129: ...lect Automatic Smart averaging for faster measurement stability or Off for no measurement averaging once the stability criteria is met Alarms The Limit Alarm allows the operator to set a high limit va...

Страница 130: ...l 59 mV 12 46 264 to 382 mV 5th buffer value Theoretical 59 mV 6th buffer value Theoretical 59 mV Testing a pH Electrode for Automatic Buffer Recognition Use the following procedure to verify that the...

Страница 131: ...opotential point is known or can be determined experimentally entering this value makes temperature compensation for an ISE possible when a one or two point calibration is performed Determining an Iso...

Страница 132: ...sing the adjacent pair of calibration points For example in a five point calibration four slopes and four E0 values are calculated to correspond to the four line segments that connect the calibration...

Страница 133: ...d on the assumption of Nernstian electrode behavior Multi point calibrations at the lower limit of detection are desirable when the response of an ion selective electrode is non linear and cannot be c...

Страница 134: ...the slope value for the electrode may be outside the range of values normally considered acceptable during an ordinary calibration For best results calibration standards should be close in range to t...

Страница 135: ...milar decrease in resistance with increasing temperature To maximize LogR performance and accuracy a ROSS Ultra or ROSS pH electrode is recommended LogR Resistance vs Temperature Graph LogR Temperatur...

Страница 136: ...e Available Replacement 8202BN 8102BNUWP 8102BN 9202BN 9102BNWP 8203BN 8103BNUWP 8103BN 9203BN 9103BNWP 8235BN 8135BNUWP 8135BN 9206BN 9106BNWP 8256BN 8156BNUWP 815600 9256BN 9156BNWP 8272BN 8172BNWP...

Страница 137: ...e instructions in the electrode user manual Perform the initial electrode check when the electrode is ready Initial Electrode Check For the most pH electrode diagnostics benefits from the Versa Star P...

Страница 138: ...given temperature it is often an indication of a crack in the bulb or shorting of the electrode leading to a total failure in function If you see this type of change in the resistance reading most lik...

Страница 139: ...139 Electrode Diagnostics Log Electrode Model Electrode Serial Date Temp Resistance Change in Resistance Notes 8102BNWP example PV1 27726 1 6 14 24 5 C 340 M Initial Check 8102BNWP example PV1 27726...

Страница 140: ...iption Measurement Range Nominal Cell Constant 013005MD Orion DuraProbe 4 cell conductivity probe with built in temperature 1 5 meter cable 1 S cm to 200 mS cm K 0 475 cm 1 013010MD Orion DuraProbe 4...

Страница 141: ...008 S cm 0 65 10 7 135 776 81 54 1 66 84 7 344 799 83 56 2 68 59 7 555 822 86 58 3 70 35 7 768 846 88 59 4 72 12 7 983 870 91 61 5 73 91 8 200 894 93 63 6 75 70 8 418 918 96 64 7 77 50 8 638 943 98 66...

Страница 142: ...115 9 13 35 1468 153 104 28 117 9 13 59 1496 156 106 29 120 0 13 84 1524 159 108 30 122 0 14 09 1552 161 110 31 124 1 14 34 1580 164 112 32 126 2 14 59 1608 167 114 33 128 3 14 85 1636 170 117 34 130...

Страница 143: ...5 C to 50 C Temperature Coefficient C Sugar Syrup 5 64 Ultra Pure Water 4 55 98 Sulfuric Acid 2 84 Salt NaCl 2 12 Dilute Ammonia 1 88 5 NaOH 1 72 10 HCl 1 32 5 Sulfuric Acid 0 96 nLFn non linear ultra...

Страница 144: ...standard method of determining TDS involves evaporating a sample to dryness at 180 C and weighing the residue The TDS factor is calculated by taking the residue weight and dividing it by the sample co...

Страница 145: ...e meter uses the conductivity value read by the conductivity probe to calculate the salinity correction factor and applies the factor to dissolved oxygen readings reported as mg L Manual salinity corr...

Страница 146: ...5 6778 6876 Find out more at thermofisher com water For Research Use Only Not for use in diagnostic procedures 2017 Thermo Fisher Scientific Inc All rights reserved RDO is a registered trademark of In...

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