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Monochromated X-Ray Source with XR5 Electron Gun 

Issue 5 

 

Monochromator and XR5 (HA600054)

25

Refer to 

Figure 5-7: XR5 Emitter Cup Assembly

.

Use kit number PRT0001/UG, which comprises of : 

1 off Filament/Cathode Assembly. 
1 off Spacer 
3 off Clamps - (not required on this assembly) 
3 off Special Screws - (not required on this assembly) 
1 off Retaining Star Washer 

12. 

Using a jewellers small screwdriver or similar tool, carefully free the tangs of the 
star-washer, in circumferential sequence, from the retaining lip inside the emitter 
cup. The washer can be reused, if the tangs are straightened out first, but a new 
washer is supplied with the emitter components. 

13. 

Lift out the filament/cathode ceramic-button assembly. 

14. 

Discard any shim-ring(s) fitted between the cathode-button and the emitter cup.

15. 

Carefully fit the Filament/Cathode Assembly with the shim supplied in the kit into 
the emitter cup, making sure that the cathode connection-peg is placed 
diametrically opposite (away from) the large slot in the emitter-cup-flange. 

16. 

Gently press the star-washer into place, making sure that all of the tangs are 
trapped beneath the retaining lip of the cup. 

17. 

Make sure that the cathode peg and mating slot in the filament-button, and the 
mating slot in the star washer, are orientated symmetrically with respect to each 
other, to maximise break-down gaps between cathode and filament and both to 
ground.

18. 

Refit the cup assembly to the main flange, and before setting the cup-to-flange 
height, connect the filament and cathode leads to the pin-base. Check that all 
sockets are fully mated to the pin-base and on the correct pins. 

19. 

Screw in the spring-loaded screws until the correct height is set. 

20. 

Ensure the Focus spring-connection is located on its retaining ceramic "top-hat". 

21. 

Refit the flange assembly to the gun body initially with 3 or 4 bolts tightened 
gradually in sequence until metal-to-metal contact is made between flanges. 
Use a new FC64 copper gasket and make sure that the flange is offered to the 
gun in the correct orientation. The main flange is labelled 

"TOP"

 on its 

circumference adjacent to the focus connection. This should be in the top 
vertical position when refitted to the gun on the system. 

22. 

Check the pin base for filament and interlock continuity and all other pins for 
electrical isolation. 

23. 

Fully tighten the flange with all bolts fitted. 

24. 

Pump down and bake the system before use. 

Figure 5-7: XR5 Emitter Cup Assembly 

Discard Shims and 
replace with Shim 
supplied with kit 

Centralise
Filament/Cathode Assembly 
button slot with slot in Star 
Washer

View of Star Washer 
and Filament 
Cathode Button

Individual Filament and Cathode 
Assemblies replaced with a single 
Filament/Cathode Assembly

Star Washer

Monochromated X-Ray Source with XR5 Electron Gun

Monochromator and XR5 (HA600054) 

 

Issue 5  

26

The LENS assembly will need to be removed to cure either: 

1.   Anode scouring  

2.   Excessive HT "ticks" and breakdown 

Item 1. can be achieved without special jigs, whereas item 2 requires expertise and 
special jigs: see Ceramics Replacement 

Refer to 

Figure 5-5: XR5 Lens and Emitter Assemblies

.

First follow the instructions for Anode Replacement since the Lens assembly cannot 
be removed until the anode is removed. Any attempt to remove the lens assembly first 
will cause damage! 

Secondly, follow the initial steps for removal of the Emitter assembly, to expose the 
lens assembly. 

Figure 5-8: XR5 Lens Assembly 

Refer to 

Figure 5-8: XR5 Lens Assembly.

Figure 5-8: XR5 Lens AssemblyThe lens assembly is fitted into the main vacuum 
housing of the XR5, through the 114mm/FC70 source mounting flange. 

To assist in handling the lens assembly (weight ~1 Kg), 3-off M4 screws can be fitted 
in the 3 tapped holes in the lens-support flange. Do not attempt to screw these in fully 
until the clamping screws have been loosened (next step). 

1. 

Unscrew the 6-off M2 x 8 cheese-head screws that clamp the lens assembly 
into the vacuum housing. 

2. 

Carefully withdraw the lens assembly. 

Do not attempt to loosen any other screws before reading the section "Ceramics 
Replacement".

Содержание ESCALAB 250

Страница 1: ...Moving the XR5 Anode 12 3 6 Monochromator Fine Tuning 12 3 6 1 Alignment of the Analysis Centre and Microscope Cross Hairs 12 3 7 T352 NT Computer Controlled Power Supply 14 4 Monochromator Operation 15 4 1 Avantage Data System Monochromator Controls 15 4 1 1 Errors and Warnings 16 4 2 Different XR5 Operating Modes 16 4 3 Switching on the Re circulated Water 17 4 4 Observing the Monochromator Spot...

Страница 2: ...ing the online manual loaded with the software datasystem It does not include detail on the initial installation and setting up of the electron gun or crystals nor any troubleshooting or maintenance which would require the user to directly access high voltage It includes procedures for replacement of certain consumable items such as anodes and filaments which require the system to be vented and su...

Страница 3: ...nterlocks are displayed in the software within the Trips Interlocks display as in GREEN OK or RED FAIL for the state of the interlocks Typical Trips Interlocks displays are shown in Figure 2 1 Occasionally pop up warning messages will appear After taking note of the message select the OK button Go into the details window and look at the Trips Interlocks you will see a red FAIL in the appropriate w...

Страница 4: ... software they include x Temperature in T352 Power Supply rises to unacceptable levels x Current drawn from T352 Power Supply HV greater than 60 mA x Drain from HV through X ray water lines greater than 20 mA Monochromated X Ray Source with XR5 Electron Gun Monochromator and XR5 HA600054 Issue 5 8 3 Description 3 1 Introduction The Monochromated X Ray Source produces X Rays which have well defined...

Страница 5: ...uit uses mains water or a re circulator as its input and then increases the flow through the X Ray source by use of a booster pump The control of the booster pump and of the solenoid valves which switch the water flow between the twin anode if fitted and mono source is by the datasystem via the T352 NT power supply Both the twin anode and mono anode are floating at high voltage and have water flow...

Страница 6: ...e by 0 8 mm per turn The range of motion and the useful anode length are both 25 mm A fraction of a turn for example a half turn will usually be enough to expose a new aluminium film area 3 6 Monochromator Fine Tuning Complete alignment and set up of standard operating conditions will generally be carried out by Thermo Fisher Scientific service engineers and most operators will not need to be conc...

Страница 7: ...ing Ratings Main HT 15kV 60mA Normal operating or 20kV 20mA Source conditioning Monochromator Filament 2 5A Bombard 3000V Cathode 1200V Focus 3500V Table 2 Specification Outputs for the Monochromator Gun Control is entirely from the computer no manual controls are fitted except for the rear panel mains power switch The supply requires five interlock loops Vacuum Water flow Twin anode cover Mono co...

Страница 8: ...the Apply button should then be selected Monochromated X Ray Source with XR5 Electron Gun Monochromator and XR5 HA600054 Issue 5 16 4 1 1 Errors and Warnings As the monochromator is ramping up to the desired operating point the data system will check for any problems and report these as a warning window If an Error does occur the data system will display a warning dialogue and instruct the operato...

Страница 9: ...upplied from the system or from a separate mains circuit in the laboratory If this is not switched on then when an attempt is made to switch on the monochromator the booster pump will run dry be much louder than normal and possibly be damaged The monochromator gun will not turn on as the water flow interlock will have failed 4 4 Observing the Monochromator Spot For fine tuning of the monochromator...

Страница 10: ...nd converge as the sample is raised and lowered 4 Position each spot by moving the dispersive and non dispersive adjusters on the crystal manipulator do NOT adjust the heights of the crystal as this will change the energy of the X Ray spot from each crystal to coincide with the cross hairs on the viewing camera These adjusters are very sensitive so only small adjustments should be made Never adjus...

Страница 11: ...eplacing Anodes In general the anode will need replacing only when all the aluminium coating has been degraded sufficiently to attenuate the X Ray flux below acceptable levels along its entire length If the anode condition requires its replacement the vacuum system will have to be fully shut down and vented to dry nitrogen Figure 5 3 XR5 Anode Assembly Refer to Figure 5 3 XR5 Anode Assembly 1 Unpl...

Страница 12: ... vented to dry nitrogen As a further precaution disconnect the mains supply from the T352 NT X Ray power supply Refer to the Figure 5 5 XR5 Lens and Emitter Assemblies 1 Remove the M8 x 16 hex head bolt clamping the XR5 earth strap 2 Unplug the leads from the XR5 3 Do not unbolt the 70mm FC38 11 pin feedthrough flange This is unnecessary except when replacing the feedthrough 4 Remove all the M8 x ...

Страница 13: ...ges Use a new FC64 copper gasket and make sure that the flange is offered to the gun in the correct orientation The main flange is labelled TOP on its circumference adjacent to the focus connection This should be in the top vertical position when refitted to the gun on the system 22 Check the pin base for filament and interlock continuity and all other pins for electrical isolation 23 Fully tighte...

Страница 14: ...Issue 5 28 5 9 Fault Finding Symptom General Cause Specific Cause How to Rectify How to Fix Mains re circulated water supply switched off Booster pump will make excessive noise Check supply Look for warning messages on datasystem Switch on supply Insufficient water flow Warning message on datasystem Water flow not sufficient to satisfy flow requirement Check inlet and outlet flow Look for warning ...

Страница 15: ...n still runs correctly Loss of control of the gun from the datasystem Gun still running An HT tick has effected communication Reboot the datasystem Try the gun control again Table 4 Fault Finding 5 10 Fuses Information for Service Engineers Within the digital X ray PSU T352 NT there is an 800mA T fuse on the mains input Monochromated X Ray Source with XR5 Electron Gun Monochromator and XR5 HA60005...

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