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Monochromated X-Ray Source with XR5 Electron Gun 

Issue 5 

 

Monochromator and XR5 (HA600054)

15

4 Monochromator 

Operation 

The ESCALAB 250 small spot monochromator is entirely computer controlled. Once 
the monochromator has been degassed all the operator has to do is select the pre-set 
monochromator conditions required and the 

Avantage

 data system does the rest. 

This document covers basic operation of the monochromator, i.e. turning it on and off 
and selecting pre-set conditions. For full details on the Monochromator operation refer 
to the 

Avantage

 on-line manual. 

4.1

Avantage

 Data System Monochromator Controls 

The 'X-Ray Control' is addressed by inserting a 

“Source Object”

 in the 

“Experiment

Tree”

 , shown selected in Figure 4-1 may also be assessed from 

“Instruments”

 tab 

but normal operation is through inserting an experiment object. 

Figure 4-1: 

Avantage

 Properties Book 

Selection of the Monochromator source 

“Mono X-ray Gun”

 opens the 

“Control

Properties Book”

 which provides a menu of stored operating conditions for the Mono 

Source. A 

“Details”

 button opens a window displaying all the control parameters. 

The Control Properties Book permits the user to select preset operating conditions 
where most of the operating conditions have already been determined and the 
operator has only a few basic decisions to make before starting the source. 

Gun control is via a simple Control tab 

(

X-Ray mode

)

, an example of which is shown 

in Figure 4-2 

Figure 4-2: Control Properties Book 

Clicking on the 

Spot/Power

 drop down list presents the user with a number of 

predefined power and spot size settings. Once an appropriate 

Beam Size

 has been 

chosen the 

Apply

 button should then be selected. 

Monochromated X-Ray Source with XR5 Electron Gun

Monochromator and XR5 (HA600054) 

 

Issue 5  

16

4.1.1 

Errors and Warnings 

As the monochromator is ramping up to the desired operating point the data system 
will check for any problems and report these as a warning window.

If an Error does occur, the data system will display a warning dialogue and instruct the 
operator in what to do next. 

Occasionally  ‘pop up’ warning messages will appear. After taking note of the message 
select the OK button. Go into the “Details” window and look at the 

Trips / Interlocks

,

you will see a red

Fail

in the appropriate window. You will need to take the appropriate 

action to resolve the problem before setting the 

Reset

button (see Figure 4-3). 

Figure 4-3: Water flow fail light within the Trips  

4.2 

Different XR5 Operating Modes 

There are in total up to 20 pre-set operating modes. 11 of these have been assigned 
to different stages of degas and are therefore not used during normal operating 
conditions. These are discussed further in the maintenance section of this manual. A 
typical set of user modes follows, although individual cases may be tailored to 
individual systems or customers requirements 

Standby -500

P

m [10kV 60W] 

Default -120

P

m [15kV 22W] 

Default -150

P

m [15kV 30W] 

Default -200

P

m [15kV 45W] 

Default -250

P

m [15kV 55W] 

Default -320

P

m [15kV 75W] 

Default -400

P

m [15kV 100W] 

Default -500

P

m [15kV 150W] 

Default -650

P

m [15kV 200W] 

DEGAS_1-Keep_P_below_1e-7mb (10 min) 

DEGAS_2-Keep_P_below_1e-7mb (10 min) 

DEGAS_3-Keep_P_below_1e-7mb (20 min) 

DEGAS_4-Keep_P_below_1e-7mb (1hr) 

DEGAS_5-Keep_P_below_1e-7mb (10 min) 

DEGAS_6-Keep_P_below_1e-7mb (20 min) 

DEGAS_7-Keep_P_below_1e-7mb (1hr) 

DEGAS_8-Keep_P_below_1e-7mb (10hr) 

DEGAS_9-Keep_P_below_1e-7mb (1hr) 

DEGAS_10-Keep_P_below_1e-7mb (1hr) 

DEGAS_Large_spot [10kV 100W] 

Table 3: Typical Example Set of User Modes 

Содержание ESCALAB 250

Страница 1: ...Moving the XR5 Anode 12 3 6 Monochromator Fine Tuning 12 3 6 1 Alignment of the Analysis Centre and Microscope Cross Hairs 12 3 7 T352 NT Computer Controlled Power Supply 14 4 Monochromator Operation 15 4 1 Avantage Data System Monochromator Controls 15 4 1 1 Errors and Warnings 16 4 2 Different XR5 Operating Modes 16 4 3 Switching on the Re circulated Water 17 4 4 Observing the Monochromator Spot...

Страница 2: ...ing the online manual loaded with the software datasystem It does not include detail on the initial installation and setting up of the electron gun or crystals nor any troubleshooting or maintenance which would require the user to directly access high voltage It includes procedures for replacement of certain consumable items such as anodes and filaments which require the system to be vented and su...

Страница 3: ...nterlocks are displayed in the software within the Trips Interlocks display as in GREEN OK or RED FAIL for the state of the interlocks Typical Trips Interlocks displays are shown in Figure 2 1 Occasionally pop up warning messages will appear After taking note of the message select the OK button Go into the details window and look at the Trips Interlocks you will see a red FAIL in the appropriate w...

Страница 4: ... software they include x Temperature in T352 Power Supply rises to unacceptable levels x Current drawn from T352 Power Supply HV greater than 60 mA x Drain from HV through X ray water lines greater than 20 mA Monochromated X Ray Source with XR5 Electron Gun Monochromator and XR5 HA600054 Issue 5 8 3 Description 3 1 Introduction The Monochromated X Ray Source produces X Rays which have well defined...

Страница 5: ...uit uses mains water or a re circulator as its input and then increases the flow through the X Ray source by use of a booster pump The control of the booster pump and of the solenoid valves which switch the water flow between the twin anode if fitted and mono source is by the datasystem via the T352 NT power supply Both the twin anode and mono anode are floating at high voltage and have water flow...

Страница 6: ...e by 0 8 mm per turn The range of motion and the useful anode length are both 25 mm A fraction of a turn for example a half turn will usually be enough to expose a new aluminium film area 3 6 Monochromator Fine Tuning Complete alignment and set up of standard operating conditions will generally be carried out by Thermo Fisher Scientific service engineers and most operators will not need to be conc...

Страница 7: ...ing Ratings Main HT 15kV 60mA Normal operating or 20kV 20mA Source conditioning Monochromator Filament 2 5A Bombard 3000V Cathode 1200V Focus 3500V Table 2 Specification Outputs for the Monochromator Gun Control is entirely from the computer no manual controls are fitted except for the rear panel mains power switch The supply requires five interlock loops Vacuum Water flow Twin anode cover Mono co...

Страница 8: ...the Apply button should then be selected Monochromated X Ray Source with XR5 Electron Gun Monochromator and XR5 HA600054 Issue 5 16 4 1 1 Errors and Warnings As the monochromator is ramping up to the desired operating point the data system will check for any problems and report these as a warning window If an Error does occur the data system will display a warning dialogue and instruct the operato...

Страница 9: ...upplied from the system or from a separate mains circuit in the laboratory If this is not switched on then when an attempt is made to switch on the monochromator the booster pump will run dry be much louder than normal and possibly be damaged The monochromator gun will not turn on as the water flow interlock will have failed 4 4 Observing the Monochromator Spot For fine tuning of the monochromator...

Страница 10: ...nd converge as the sample is raised and lowered 4 Position each spot by moving the dispersive and non dispersive adjusters on the crystal manipulator do NOT adjust the heights of the crystal as this will change the energy of the X Ray spot from each crystal to coincide with the cross hairs on the viewing camera These adjusters are very sensitive so only small adjustments should be made Never adjus...

Страница 11: ...eplacing Anodes In general the anode will need replacing only when all the aluminium coating has been degraded sufficiently to attenuate the X Ray flux below acceptable levels along its entire length If the anode condition requires its replacement the vacuum system will have to be fully shut down and vented to dry nitrogen Figure 5 3 XR5 Anode Assembly Refer to Figure 5 3 XR5 Anode Assembly 1 Unpl...

Страница 12: ... vented to dry nitrogen As a further precaution disconnect the mains supply from the T352 NT X Ray power supply Refer to the Figure 5 5 XR5 Lens and Emitter Assemblies 1 Remove the M8 x 16 hex head bolt clamping the XR5 earth strap 2 Unplug the leads from the XR5 3 Do not unbolt the 70mm FC38 11 pin feedthrough flange This is unnecessary except when replacing the feedthrough 4 Remove all the M8 x ...

Страница 13: ...ges Use a new FC64 copper gasket and make sure that the flange is offered to the gun in the correct orientation The main flange is labelled TOP on its circumference adjacent to the focus connection This should be in the top vertical position when refitted to the gun on the system 22 Check the pin base for filament and interlock continuity and all other pins for electrical isolation 23 Fully tighte...

Страница 14: ...Issue 5 28 5 9 Fault Finding Symptom General Cause Specific Cause How to Rectify How to Fix Mains re circulated water supply switched off Booster pump will make excessive noise Check supply Look for warning messages on datasystem Switch on supply Insufficient water flow Warning message on datasystem Water flow not sufficient to satisfy flow requirement Check inlet and outlet flow Look for warning ...

Страница 15: ...n still runs correctly Loss of control of the gun from the datasystem Gun still running An HT tick has effected communication Reboot the datasystem Try the gun control again Table 4 Fault Finding 5 10 Fuses Information for Service Engineers Within the digital X ray PSU T352 NT there is an 800mA T fuse on the mains input Monochromated X Ray Source with XR5 Electron Gun Monochromator and XR5 HA60005...

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