SCP SCIENCE MiniWAVE Скачать руководство пользователя страница 10 | Manualshive

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Version 3

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5

Operation

Compressed Air Requirements

At least 5 bar (80 psi) of pressure is required, with a flow rate of 1.5 Cubic meters per minute (50 cfm). The maximum pressure to the system
is 7.5 bar (110 psi). When the digestion is complete the system open the primary electronic air valve to rapidly cool the digestion vessels. The
cooling rate is approximately 3.5 minutes from 180 °C to 70 °C for 10 mls of sample. At the same time a baffle in the exhaust tube opens
under software control to ensure the proper air flow for the quantity of air being induced into the cavity.

Always use the preset pressure regulator provided.

The end point cooling temperature is not user definable. It is possible to open the lid after the digestion stops, but
the rack will could still be hot to warm. One may run 6 vessels at the same time or less than 6 by placing them
symmetrically in the rack. Deselect the channels to monitor the temperature on the digestion tab of the software.

Start

1. Connect a

Mini

WAVE

digestion module to a

Mini

WAVE

controller using a USB cable provided.

2.  Plug the controller to the appropriate wall receptacle (100-240V).
3.  Plug the module into the correct wall receptacle for either 115V or 230V.
4.  Power up the controller.
5.  Power up the module to start the system. The LED indicator on the front panel will change and then register a number

between 1 and 4. This number represents the module number in Module.

6. Compressed air is connected to the back of the each Module for fast cooling.

Before Digestion

1. Placing rack into cavity

When loading a rack into

Mini

WAVE

cavity, it is necessary to ensure that the rack handle is

aligned with the groove in the cover plate motor. Typically if the rack is placed in the system with
rack position 1 in front the rack will align easily.

If a rack is not placed correctly in the cavity the lid will not close
properly.

2. Top cover closing and locking

The cover plate closes by rotating towards the cavity. Rotate the locking mechanism forward to
lock the lid in place. Two interlocks will be engaged to allow the system to digest samples. The
opening handle should click into place when closed completely. The system will not operate if the
cover is not closed completely.

CAUTION

NOTE

WARNING

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Содержание MiniWAVE

Страница 1: ...User Manual www scpscience com MiniWAVE ...

Страница 2: ...z Vessels Cat 010 600 009 Rack for 75 ml Vessels May be used with Quartz or PFA vessels Cat 010 600 013 Teflon Plunger Liners For Microwave vessels Qty Pack of 6 Cat 010 600 032 Teflon Caps For quartz vessels Qty Pack of 6 Cat 010 600 060 Teflon Mixing Caps For Microwave vessels Qty Pack of 6 Cat 010 600 100 Racks Quartz Vessels Accessories Teflon Vessels 75 ml Quartz Vessels Calibrated at 45 and ...

Страница 3: ... 2009 EN 61000 4 3 2006 A1 2007 A2 2010 EN 61000 4 4 2012 EN 61000 4 5 2006 EN 61000 4 6 2009 EN 61000 4 11 2004 EN61000 3 2 2006 A1 2009 A2 2009 EN61000 3 3 2008 CISPR 11 2009 A1 2010 and FCC 47 CFR Part 18 Subpart C CSA C22 2 CSA SPE 1000 and UL1010 1 NEC code 2011 Power Density Test Report According to 21 CFR Par 1030 10 C 1 2 3 and IEC 61010 1 Clause 12 4 ICES 001 CISPR11 EN55011 and EN61326 1...

Страница 4: ...Software 11 ModuleTab 12 DigestionTab 16 MethodsTab 17 ReportsTab 19 UtilitiesTab 20 DiagnosticTab 22 Operation 22 LogoutTab 23 6 Cleaning MaintenanceofSystem 24 Cleaning ofVessels 24 Cleaning ofTeflon Liners Caps and Safety Pressure Caps 24 Pressure 24 Cleaning the Cavity 24 Cleaning the screen of the Controller 24 7 Warranty SafetyInformation 25 Toxic or hazardous substances and elements 26 8 Sp...

Страница 5: ...tion x Fume exhaust connection y Compressed Air connection Controller z On Off switch Power cord connection USB B connection Ethernet connection u v w x z USB Connection Cable Power Supply y Fume Exhaust connection Positive Pull 40 cfm 1 1 cmm or more Compressed air connection Minimum pressure 5 Atm 80 psi ...

Страница 6: ...p at a convenient height for easy rack insertion Set the controller near the module and connect them together with the USB cable provided Connect the power cable to each of the units finish reading the manual prior to continuing Connect an air supply to modulate sample temperature during the digestion The compressed air is also use to facilitate fast cooling of the samples Inspection Ensure all of...

Страница 7: ...ized constant voltage AC power supply and the voltage must be within 5 of the specified level 5 Compressed air supply must be dry and oil free 5 Atms or 80 psi It is important to ensure that the exhaust hose is connected to laboratory exhaust Precautions to Avoid Possible Exposure to Excessive Microwave Energy a Do not attempt to operate this instrument with the lid open since open lid operation c...

Страница 8: ...sed to emphasize information pertaining to procedures that if not strictly followed may result in damage or destruction to the instrument or improper instrument operation WARNING A warning is used to emphasize information about dangerous or hazardous conditions relating to the operation cleaning or maintenance of the instrument that may result in personal injury NOTE A note is used to emphasize pr...

Страница 9: ...essel and tapered edges of the Teflon cap The Teflon cap is held into place when the Safety Pressure Cap is screwed into place Place the vessels in the MiniWAVE Rack Place the vessel in microwave tube extender and place under the safety Pressure Cap Hold the vessel by hand during the process Tighten the safety pressure cap until the bottom of the cap is snug plus an 1 8 of a turn Or use the torque...

Страница 10: ...iniWAVE controller using a USB cable provided 2 Plug the controller to the appropriate wall receptacle 100 240V 3 Plug the module into the correct wall receptacle for either 115V or 230V 4 Power up the controller 5 Power up the module to start the system The LED indicator on the front panel will change and then register a number between 1 and 4 This number represents the module number in Module 6 ...

Страница 11: ... to reboot the software after an upgrade of software USER LEVEL Tab Button Administrator Operator Service Module Re Scan Y Y Y Start Digestion Y Y Y Digestion Operational after the Start Digestion button is pressed Stop Y Y Y Methods Delete Y N Y New Y N Y Copy Y N Y Edit Y N Y view Y Y Y Reports Delete y N Y Save to USB Y Y Y Utilities Calibration Y N Y Users Y N Y User Group Y N Y Change Passwor...

Страница 12: ...icant temperature difference for one vessel either higher or lower than the other vessels for a certain time the system will stop the digestion and identify the suspected position Re Scan is used to update the controller when new modules are connected The controller can monitor and control up to 4 modules simultaneously This only needs to be done at initial installation and after any disconnection...

Страница 13: ...e check mark should correspond to the actual sample in the rack i e if sample in Position 1 un tick all the mark except position 1 In case of running 2 vessels The vessels should be placed in the rack in a symmetrical way i e Positions 1 and 4 positions 2 and 5 Positions 3 and 6 also un tick the positions not being run ...

Страница 14: ...Version 3 14 In case of running 3 vessels Vessels should be placed in the rack symmetrically i e Position 1 3 and 5 or Position 2 4 and 6 Be sure to un tick the samples not being placed in the rack ...

Страница 15: ...sels should be loaded symmetrically too i e Positions 1 2 4 and 5 or Positions 2 3 5 and 6 Similar to the cases specified before be sure to un tick the empty positions In case of running 5 vessels it is very important to un tick the empty position ...

Страница 16: ... is coming to temperature The black number 175 in picture above represents the set point temperature and the white number is displayed the current average temperature 21 When the set point temperature is reached the bar graph turns green for the hold time of the method selected The bar graph turns blue when the method has reached the end of time This graphical representation is shown in real time ...

Страница 17: ... or a user method to be copied The method name must be changed to be saved Edit allows a user defined method to be modified when done in the service or administrator access level View allows any operator to view the parameters in any method Save to USB save the method to an installed USB stick on the back of the controller Name is a required field to be filled out as method are stored by name Desc...

Страница 18: ...ers is used to add a 2nd or 3rd temperature profile of time to temperature and time at temperature The set point temperature must also be inputted Save is used to save the method Cancel will return to the main page without saving the values Save to USB will save the information on a USB stick if one is installed in the 5th USB connector on the back of the controller It saves the information in PDF...

Страница 19: ... during the run Rack is the name of the rack and is user definable on the Module tab Tube is the ID of the sample inputted prior to starting the digestion on the Module 1 tab Delete is used to delete the report from the reports file Save to USB allows one to save the digestion report on a USB stick in PDF format for archiving MSN Module Serial Number Is the actual serial number of the module the d...

Страница 20: ...tion procedure when the equipment is connected Send To Module is used to update the CPU on the module after verification of the software Save to USB is used to download the current information to a USB stick Save is used to save the data in controller User Tab User s Group is used to select the user group either operator or administrator from the pull down menu Change Password is used to set and c...

Страница 21: ...guage is not operation at this time Network is implemented but not turned on at this time as one requires a software program to pass through your fire wall Please contact SCP SCIENCE for further information The number of days should be customized as per protocol for a specific laboratory s data storage Update Update from Server is used to update the software from the server if the system has been ...

Страница 22: ...top is to suspend the acquisition of data Operation The commands on this tab are to be used by factory trained personnel only with the exception of reading the IR temperature sensor when the unit is not performs a digestion XB Speed Control is used to run the exhaust fan Programmed in percent of full speed PID Control is used to query the current PID values Control Read Filament is used to query t...

Страница 23: ...e current IR temperature reading Only works when the module is not being operated Logout Tab Use this tab to safely shut down the controller at the end of each day Exit returns one back to the main screen where user level is selected Open Desktop is used to access the BIOS of the operating software and to calibrate the touch mask of the controller Reboot reboots the system and returns one to the m...

Страница 24: ... factory They can be validated in the field with our Field pressure testing unit It is highly recommended that Safety Caps be tested every 6 months Safety Pressure Cap can be calibrated only by SCP SCIENCE s trained service personnel Cleaning the Cavity Under normal operating conditions if a tube vents during the digestion the fumes are typically whisked away by the exhaust blower If the rack is w...

Страница 25: ...e solely responsible for the safe operation handling and use of these products A minimum of safety considerations must be followed when working with the MiniWAVE microwave digestion system in order to maintain good laboratory practice Do not place the MiniWAVE on a surface containing flammable material MiniWAVE requires a clearance of minimum 6 in 15 cm space in the back towards the wall MiniWAVE ...

Страница 26: ...ards O O O O O Magnetrons O O O O O Applicators O O O O O Co axial cable O O O O O Touch Screen O O O O O Ribbon Cables O O O O O Housings O O O O O O Indicates that the toxic or hazardous substance contained in all the homogenous materials for this part according to EIP A EIP B EIP C is below the limit requirement in SJ T11363 2006 X Indicates that the toxic or hazardous substance contained in al...

Страница 27: ...10 1 Certified CSA NEC code 2011 Radiation Hazard Power Density Tested according to 21 CFR Par 1030 10 C 1 2 3 and IEC 61010 1 Clause 12 4 21 CFR1030 report filed for FDA Electrical MiniWAVE Module Voltage 110 and 220 volts Current 100 125VAC 50 60Hz 13A Uses a C19 detachable power cord 200 240VAC 50 60Hz 7A Uses a C19 detachable power cord Watts 1000 Compressed Air or Inert Gas 90 psi at 50 cfm p...

Страница 28: ...his message is not seen at power up there could be a segment malfunction There is no self detection for correct segments drive so the user only can see an indicator fault After this message the system tests many hardware peripherals and the following error messages could be seen LE Line frequency Error there is no AC signal activity detected CE Calibration Error Calibration tables are empty or inc...

Страница 29: ... 4 Holding stage The hold phase has another animation pattern alternating between two symbols a u and a n meaning that hold temperature over under shoot is meant to be under tight control The segments sequence is ABF CDE and repeats 5 Digestion fail If any critical anomaly shows during digestion the digestion has to be halted In addition to the controller display emergency message the message F a ...

Страница 30: ...oltage 4 The line frequency of Module 1 is out of range Power line has a problem Digestion stops Check power line frequency 5 Module 1 has Filament problem Digestion stops 6 Module 1 has High Voltage problem Digestion stops 7 Module 1 has IR Sensors COM problem Module 1 has internal communication problem Digestion stops 8 Module 1 has IR Sensors Error Problem of Infrared sensor Digestion stops 9 M...

Страница 31: ... digestion 18 Magnetron of Module 1 is approaching overheat User decides to continue or stop digestion 19 Screen lost Keep Alive from Module 1 Either Module 1 stopped working or communication problem User decides to continue or stop digestion If the reason for the safety message is unclear contact SCP SCIENCE Service Department or your local distributor ...

Страница 32: ...ists CORPORATE HEADQUARTERS USA France Germany Phone 1 800 361 6820 Fax 1 800 253 5549 Phone 1 800 361 6820 Fax 1 800 253 5549 Phone 33 0 1 69 18 71 17 Fax 33 0 1 60 92 05 67 Phone 49 0 8342 89560 61 Fax 49 0 8342 89560 69 Corporate Phone 1 514 457 0701 Fax 1 514 457 4499 www scpscience com sales scpscience com ...

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