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ADA5000 Automatic Distillation Analyzer 

Operation and Instruction Manual 

ADA5000-Manual 

18 -

 

The automatic nitrogen fire extinguishing 

system will inject a 3.0 second burst of nitrogen 
gas into the compartment to remove all oxygen 
from the heater compartment thus extinguishing 
the flame. The spilled volume is collected in the 
stainless steel collection pan just below the 
heater assembly. This liquid can then be drained 
out of the pan by opening the stopcock on the 
left side of the instrument. Instead of nitrogen, a 
CO

2

 supply can also be used. 

 

CAUTION! 

The stop cock should be kept in the closed 
position during normal operation. Take care 
not to burn yourself when removing spilled 
materials from the catch pan. 

 

 

  

The nitrogen supply can be connected to the 

valve behind the distillation compartment.  To 
access this area, remove the top panel. 

 

Connect the nitrogen supply where the yellow 
plug is shown in the above photo. 
 

6 Maintenance 

 
WARNING. 

Disconnect power to the unit 

before servicing to avoid exposure to high 
voltages and/or temperatures which may result 
in personal injury or death. If you have any 
questions about maintaining your equipment, 
please do not hesitate to contact the Koehler 
technical service department. 
 

6.1 Routine 

Maintenance 

 
The Koehler Automatic Distillation Analyzer 

requires routine maintenance to provide many 

years of continuous service. Over the course of 
time, some instrument parts may need to be 
replaced. 

 

6.2 Replacement 

Parts 

 
When ordering replacement part(s), please 

provide the model number, serial number, and 
product shipment date of your equipment so that 
we can ensure you will receive the proper 
replacement part(s). 

 

Part Number 

Replacement Part 

354-040-003 

TRIAC 40A 

300-000-002 

Emitter Diode 

300-000-001 

Receiver Diode 

K45601-03014 

Wiper for condenser tube 

K45650 

Resistance Thermometer 
PT100 with cable & plug for 
detection of distillation 
temperature 

K45658 

Heating coils for flask heater 

K45658-A 

Ceramic Coil Supports (set of 
four (4)) 

K45651-D 

(Thiokol) Viton O-ring for use 
with K45651-E 

K45614 

Stepper Motor PC Board 

K45623 

Main Power Supply PC Board 

K45681 

Power PC Board w/ Heat Option 

469-005-001 

Infrared Emitter Sensor 

354-002-010 

Power Resistor, 10

, Aluminum 

481-004-002 

Fuse Base for Heater 

K45630 

1.0A, time lag  

K45631 

0.63A, time lag 

K45662-A 

6.3A, time lag 

K45663 

1.6A, time lag 

Содержание ADA5000

Страница 1: ...venue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 http www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing Analysis...

Страница 2: ......

Страница 3: ...3 1 Packing List 3 3 2 Unpacking 3 3 3 Instrument Installation 3 3 4 Software Installation 3 4 Operation 7 4 1 Description of Instrument Controls 7 4 2 Instrument Operation 7 4 3 Communication Manage...

Страница 4: ...o are experienced in both petroleum products testing and instrument service to better understand your requirements and provide you with the best solutions You can depend on Koehler for a full range of...

Страница 5: ...e analyzer must be disconnected from the main power supply otherwise electrical hazards may be experienced Be extremely careful because of electrical shock and danger of personal injury Unit Design Th...

Страница 6: ...different models are K45603 K45703 TS 120VAC 5 50 60Hz 20A K45604 K45704 TS 230VAC 5 50 60Hz 10A Nitrogen Nitrogen must be available in order for the automatic fire extinguishing system to work Conne...

Страница 7: ...nt by clicking on the Yes button Confirm that the computer meets these minimum requirements and click on the Next button Enter the name and company information of the user To utilize the software as a...

Страница 8: ...ext button to continue Verify that all each box of the four components are checked and click on the Next button Select or create a folder the add program icons to Click Next to continue Review the pro...

Страница 9: ...arious paths please consult with Koehler technical service To change the units for temperature 1 and pressure 2 select the desired units by clicking on the corresponding radio buttons Registration 3 F...

Страница 10: ...amber 4 2 Instrument Operation 1 Power Turn on the main power switch to the unit Turn on the power switches on the PC and printer if applicable Note the internal computer on the K457XX TS models has a...

Страница 11: ...correct position Place the silicone stopper over the side arm of the distillation flask and then place it into the condenser tube 13 Move the heater carefully under the flask 14 Place the dropping pl...

Страница 12: ...e the status of an analyzer from the PC select the View option and then Unit Data Select unit 1 Select a connected analyzer to see all the important values of this analyzer Analog 2 Temperature shown...

Страница 13: ...sible to change the path of the database program form and results form For a normal installation you can use this standard directory If a PC is connected to a network it s possible to have the databas...

Страница 14: ...ults Form Select this item to change a result form Be careful when changing a form A backup of these forms can be found on the installation CD in directory Backup Results Comparison To compare up to 4...

Страница 15: ...ram Unit Select analyzer Load Select item to load a new program from the database Attention Program will be sent automatically to selected analyzer and overwrite an existing previous run If desired st...

Страница 16: ...Koehler Comment Sample Program Method ASTM D86 Distillation Group SG4 Condenser temp 40 0 C Receiver temp 30 0 C Expected volume 98 0 mL Preheat 1 29 1 Preheat time 3 0 min Preheat 2 28 2 Extended Fi...

Страница 17: ...finished min 30 mL are necessary microprocessor system of distillation analyzer will calculate optimized value According to the distillation group a heating rate will be calculated to get a time for...

Страница 18: ...fix temperatures are stored in a memo field of the database and are online available Program Extended Fix Temps Final Results All important values are shown online here That means if the IBP was detec...

Страница 19: ...since start is shown Cool Time Timer for cooling device Condenser Shows actual temperature of condenser tube Volume Shows actual volume of selected analyzer Receiver Shows actual temperature of recei...

Страница 20: ...wing sections 5 1 Flask Heater Compartment and Auto Fire Extinguisher The design of the flask heater compartment makes this instrument one of the safest automatic distillation units available The phys...

Страница 21: ...in personal injury or death If you have any questions about maintaining your equipment please do not hesitate to contact the Koehler technical service department 6 1 Routine Maintenance The Koehler A...

Страница 22: ...s been properly installed operated and maintained Koehler Instrument Company must be advised in writing of the malfunction and authorize the return of the product to the factory The sole responsibilit...

Страница 23: ...ADA5000 Automatic Distillation Analyzer Operation and Instruction Manual ADA5000 Manual 20 Notes...

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