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Sample configuration of ASM 2.2L with valve

Assistant ASM 2.2L

Instructions

Document no.: V6803

Содержание Azura Assistant ASM 2.2L

Страница 1: ...Sample configuration of ASM 2 2L with valve Assistant ASM 2 2L Instructions Document no V6803...

Страница 2: ...il support knauer net KNAUER Wissenschaftliche Ger te GmbH Hegauer Weg 38 14163 Berlin Phone 49 30 809727 0 Fax 49 30 8015010 Internet www knauer net E Mail info knauer net Article number V6803 Versio...

Страница 3: ...3 2 3 Operator responsibility 3 2 4 Personal safety equipment 4 2 5 Safety features on the device 4 2 6 Working with solvents 5 2 6 1 General requirements 5 2 6 2 Contamination by health threatening s...

Страница 4: ...e cables 24 8 2 3 Configuring the router 24 8 2 4 Integrating the LAN into the company network 24 8 2 5 Controlling several systems separately in the LAN 25 8 2 6 Mobile Control Setting a static IP ad...

Страница 5: ...nsportation 41 13 Transport and storage 42 13 1 Taking the device out of operation 42 13 2 Packing the device 42 13 3 Transporting the device 42 13 4 Storing the device 43 14 Disposal 43 14 1 AVV Mark...

Страница 6: ...oad these and other instructions from the KNAUER web site www knauer net library 1 2 Signal words Possible dangers related to the device are distinguished in personal and material damages Symbol Meani...

Страница 7: ...amage In case you notice any damage inform the technical support and the shipping company within three workdays 1 4 3 Warranty conditions For information on warranty please refer to our general terms...

Страница 8: ...sion protection Contact the KNAUER Customer Support for more information 2 2 User qualification The user is qualified to handle the device if all of the following points apply He has at least a basic...

Страница 9: ...ty equipment The protective measures required in the laboratory must be observed and the following protective clothing worn during all work on the device Safety glasses with side protection Protective...

Страница 10: ...quids could get onto hot surfaces in the interior Degas solvents before use and observe their purity 2 6 2 Contamination by health threatening solvents Contamination with toxic infectious or radioacti...

Страница 11: ...ecommended or prescribed by the manufacturer Spare parts and accessories Only use original parts and accessories made by KNAUER or a company authorized by KNAUER PEEK fittings Use PEEK fittings only f...

Страница 12: ...paragraph space requirements Bruising danger Damage to the device by carrying or lifting it on protruding housing parts The device may fall and thus cause injuries Lift the device only centrally on th...

Страница 13: ...les next to the device or in a solvent tray Moisten the cleaning cloth only slightly Component defect Damage to the flow cell due to incorrect lifting possible Lift the detector only on the side of th...

Страница 14: ...head in case running in procedure was not per formed correctly Set the correct backpressure and flowrate for the running in procedu re of the pump head Specific running in parameters and the general...

Страница 15: ...ns symbols and labels which are used on the device or the device modules in the software or in the instructions Symbol Meaning Device fulfills the requirements of the Conformit Europ enne which is con...

Страница 16: ...ed in analytical prepara tive and continuous liquid chromatography The concept of flexible combi nation of device modules combines highest functionality with minimal space requirements Equipped with u...

Страница 17: ...it possible to adapt the assistant to individual requirements The plug in modules can be easily released and replaced by other devic modules see chapter 5 8 Exchange of the device modules on page 18...

Страница 18: ...e operated with up to two empty modules 5 5 Exceptions to the configuration The following exceptions apply to the configuration of the assistant 1 A maximum of one UV detector is allowed in an assista...

Страница 19: ...UVD 2 1S detector is supplied with a test cell For the use of the detector a flow cell has to be installed Note A maximum of one UV detector is allowed in an assistant 5 6 1 1 Performance features Si...

Страница 20: ...ology Liquid transport with stable flow rate and high flow accuracy Long service life 10 ml and 50 ml pump head selectable With or without pressure sensor for use with high pressure HPLC or low pressu...

Страница 21: ...information on the valve drive VU 4 1 can be found in the AZURA Valve Unifier VU 4 1 Instructions document number V6855 www knauer net uvd2 1s manual 5 6 3 1 Mounting the valve onto the valve drive Be...

Страница 22: ...g 4 The port 1 of the valve has to point up 3 Using the screwdriver tighten the screws 1of the adapter 5 7 Sample configuration ASM 2 2L as AZURA educational system article no A46002 Fig 7 Compact HPL...

Страница 23: ...e system 5 8 Exchange of the device modules Hot surface The detector module can become warm during operation Allow the detector module to cool for 20 minutes before removing it from the assistant Comp...

Страница 24: ...e 7 The assistant automatically detects the device modules and checks the configuration according to the chapter 5 4 Device overview on page 13 6 Scope of delivery Note Only use original parts and acc...

Страница 25: ...ft air conditioning Protect the assistant from strong draft Avoid placing the assistant next to machines that cause ground vibra tion Avoid vibration Keep the assistant away from high frequency source...

Страница 26: ...nnect the device to the mains supply Make sure that the power plug on rear of the device is always accessi ble so that the device can be disconnected from the power supply Note Make sure that the powe...

Страница 27: ...aping liquids flow into a waste bottle If there is too much liquid the red LED starts flashing Both the device and the data acquisition via chromatography software are stopped Remove the front cover P...

Страница 28: ...r configure the router to set up the network 4 Install the chromatography software from the data storage device 5 Switch on the device and run the chromatography software 8 2 1 Configuring the LAN set...

Страница 29: ...the router to the mains power sys tem 8 2 3 Configuring the router The router is preset at the factory Informationen zu IP Adresse Benutzer name und Passwort finden Sie im Handbuch des Routers www kna...

Страница 30: ...s Note The basic module of the assistant and the modules have the same IP address The differentiation of the individual devices takes place via the IP ports The basic module is the IP port 10001 the l...

Страница 31: ...connection between the Mobile Control and the device has been established 1 In Mobile Control choose Settings 2 On the General tab choose the device name 3 Under Network Settings choose DHCP 1 4 Clic...

Страница 32: ...ice connection settings opens Enter serial number of the device into the text field Target device serial number 1 3 Choose option Use the following IP address 2 4 Enter the IP address into the text fi...

Страница 33: ...ation To set an IP address via APIPA configuration the PC and the LAN control must be set to DHCP mode If no DHCP server can be detected the device switches into APIPA configuration and receives an IP...

Страница 34: ...ctor Finish the installation Bring the device into operation 8 3 2 Pin header assignments Fig 14 Pin header assignments Connection Function GND Reference point of the voltage at the signal inputs ANA...

Страница 35: ...evice START IN TTL compatible input Low active Secure switching threshold at least 10 mA The start of a module can be triggered by a signal short circuit to GND from an external device ERROR OUT TTL o...

Страница 36: ...veral options for controlling the device with chromatography software with Mobile Control To operate the device with software you have to establish a connection between the LAN port and a computer A l...

Страница 37: ...rror message Check the system Shortly press the switch to deactivate the error message red Serious error Restart the device If the operating condition does not change call the technical support green...

Страница 38: ...the installed device modules are read by the ASM 2 2L You can read the individual GLP data in the instructions of the respective device module www knauer net en Support User manuals 9 3 Startup Use t...

Страница 39: ...has been switched off Note Malfunctioning system after repeated standby possible After repeatedly using the standby switch off the power switch and back on again to reset the data storage Procedure F...

Страница 40: ...on the functionality of the device The Operation Qualification includes an extensive functionality test ac cording to KNAUER standard OQ documents The Operation Qualification is a standardized docume...

Страница 41: ...outer settings Is the router set to DCHP server Is the IP address range sufficient for all the connected devices 3 Check all connections Are the patch cable connected to the LAN ports and not the WAN...

Страница 42: ...ect the flow cell assembly 2 Fasten the knurled head screws on the flow cell to prevent incursion from interfering light or an electronics error 3 Exchange the defective flow cell 4 Inspect the servic...

Страница 43: ...alves Valve leaks Tighten the connections Pressure variations caused by leaking valve head Exchange the rotor seals Inform the technical support of KNAUER 11 3 System messages If other system messages...

Страница 44: ...r device which is defective Detector grating drive failed Replace step motor of the grating drive Replace the mainboard Detector low light Check lamp Clean flow cell Detector not calibrated Activate c...

Страница 45: ...ice will ensure successful analyses and reproducible results In this chapter you find the information relevant for maintenance care and storage Additionally you find instructions for maintenance tasks...

Страница 46: ...aries have been emptied or filled with flushing solution e g isopropanol before storage To prevent algae formation do not use pure water We recommend the same ambient conditions temperature range and...

Страница 47: ...the power plug out of the socket and then out of the device 2 Pack the power cable together with the device Disconnect all electrical connections Remove the accessories and pack the device for transp...

Страница 48: ...arked as waste elec trical and electronic equipment 160214 14 2 WEEE registration number KNAUER as a company is registered by the WEEE number DE 34642789 in the German Elektroaltger teregister EAR The...

Страница 49: ...OC 5 V 24 V Analog outputs Integrator output detector signal pump pressure 15 2 General Power supply 100 240 V 50 60 Hz maximum 130 W Dimensions 361 x 208 x 523 mm width x height x depth Weight of th...

Страница 50: ...ure sensor P 2 1S 10 ml stainless steel APG92EA P 2 1S 10 ml Hastelloy C APG92EC P 2 1S 10 ml ceramic APG92EB P 2 1S 50 ml stainless steel APG92FA P 2 1S 50 ml Hastelloy C APG92FC P 2 1S 50 ml ceramic...

Страница 51: ...spare parts Name Order number AZURA Click for attaching IFU 2 1 airsensor pressure control A70089 Accessory kits AZURA accessories kit FZA02 Accessory kit AZURA P 2 1S and P 4 1S FPGA Accessory kit AZ...

Страница 52: ...o 40 C unless stated otherwise Please note that higher temperatures can signifi cantly affect the stability of different materials 17 2 Plastics Polyetheretherketone PEEK PEEK is a durable and resista...

Страница 53: ...lene POM POM H TF POM is a semi crystalline high molecular thermoplastic material which stands out due to its high stiffness low friction value and thermic stability It can even substitute metal in ma...

Страница 54: ...terized by a high hardness a low coefficient of friction and thus low wear In addition it is highly biocompatible DLC is inert against all acids alkalis and solvents commonly used in HPLC Ceramic Cera...

Страница 55: ...e used or with a mixture of higher compatibil ity They are inert against almost all solvents Exceptions are biological appli cations which are metal ion sensible and applications with extreme cor rosi...

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