IKA C 6000 global standards Скачать руководство пользователя

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Source language: German

Page

Declaration of conformity

Explication of warning symbols

Safety instructions

Correct use

User instructions

System features

Warranty and liability

Transport and storage

Transport and storage conditions

Unpacking

Scope of supply

Description of system components

IKA

C 6000 calorimeter global standards/isoperibol

Hoses

Commissioning

Place of installation

Connection to the condenser

Connection to the water

Connection to the oxygen supply

Connection to the mains power supply

Connection of peripherals

On/off switch

Display and operating elements

Explanation of the screen display

Working with the IKA

C 6000 global standards/isoperibol calorimeter

Switching on the device

System test

Switching off the device

The standard calorimetric procedure

- Calorific value determination

- Corrections

- Note on the sample

- Complete combustion

- Calibration

(only

IKA

C 6000 global standards)

- Calibrating

- Instructions on calibration

Preparation for measurement

Charging the decomposition vessel

Calorimetric measurement without automatic decomposition vessel detection

Starting the measurement

Evaluation

Menu

(main overview)

Library

Method of operation, decomposition vessels and calibration

Servicing the decomposition vessel

Contents

Содержание C 6000 global standards

Страница 1: ...IKA C 6000 global standards IKA C 6000 isoperibol 20000004212 Operating instructions EN C6000_092016...

Страница 2: ......

Страница 3: ...als 14 On off switch 15 Display and operating elements 16 Explanation of the screen display 16 Working with the IKA C 6000 global standards isoperibol calorimeter 20 Switching on the device 20 System...

Страница 4: ...n 51 Checks 55 Accessories and consumables 56 Accessories 56 Technical data 57 Technical data IKA C 6000 global standards 57 Technical data IKA C 6000 isoperibol 59 DANGER WARNING This symbol indicate...

Страница 5: ...ition vessel risk of explosion If you are burn ing unknown samples leave the room or keep your distance from the calorimeter Benzoic acid may only be combusted in its pressed form Flammable dust and p...

Страница 6: ...is a category III pressure device The decomposition vessel has undergone an EC prototype test The CE declaration of con formity confirms that this decomposition vessel corresponds to the pressure dev...

Страница 7: ...gh them in order The section Transport storage is relevant for system reliability and for ensuring high measuring accuracy The section Description of system com ponents describes the system components...

Страница 8: ...anufacturer interfere with the appliance only original parts and original accessories are used for repairs The calorimeter system may be opened only by an authorised Service Agent or Customer Service...

Страница 9: ...nnection tube O2 Venting hose Mains connection cable Warranty card Water inflow pipe Water return pipe Operating instructions Unpacking Please unpack the system components carefully and check for any...

Страница 10: ...tion of system components Touch Screen Lift Stylus for operating the touch screen Calorimeter IKA C 6000 global standards isoperibol Decomposition vessel Water filter Water Oxygen Interfaces Mains pow...

Страница 11: ...For operation of the system the following must be available at the place of installation A power supply corresponding to the nameplates on the system components An oxygen supply 99 95 pure oxygen qua...

Страница 12: ...ipe to the IN port of the condenser The connection EMPTY is intended only for emptying the device e g for transport purposes In normal operation the discharge hose need not be inserted Rear view witho...

Страница 13: ...or connect it to a gas washing device Comply with the applicable safety regulations in this respect O2 connection tube IN max 4 MPa Venting hose IKA C 29 Combustion gases are haz ardous to health ther...

Страница 14: ...Baud rate 9600 Data bits 8 Stop bits 1 Parity none Handshake none RS232 BALANCE Interface for connecting scales Mettler Ohaus Sartorius Kern Standard setting Baud rate 1200 Data bits 7 Parity odd Stop...

Страница 15: ...off at the on off switch Lift moves upwards Switch the appliance off only by using the menu com mands Lift moves downwards Data may be lost if the appliance is switched off other than by follow ing th...

Страница 16: ...finger Explanation of the screen display Schematic representation of the display components Pos Designation A Tab C Arrow symbol tabs D Arrow symbol vertical scroll bar E Vertical scroll bar F Info li...

Страница 17: ...eld Clicking in the dark area and dragging it allows you to move continu ously through the display as does clicking on the arrow symbols and maintaining the selection Note Greyed out fields cannot be...

Страница 18: ...e Preparation for mea surement dialogue the most important actions are explained below Weighted sample Permits manual input of a weight value using the virtual keyboard Calibration Selection field for...

Страница 19: ...ch as Designation Here again the entire area is available to be clicked A complete virtual keyboard is opened Note The maximum input is 23 characters After the virtual keyboard has been closed with OK...

Страница 20: ...whether the temperature of the cooling waters is correct for the selected function of the IKA C 6000 global standards isoperibol ap prox 60 to 180 seconds If any one of these steps is not performed su...

Страница 21: ...ifferent function from those currently available Make sure however that the system conditions are stable The following are the default modes that are set Adiabat 22 IKA C 6000 global standards Isoperi...

Страница 22: ...tion products of the sample Solid substances may be formed for example ash Often however the combustion products that form the basis of the standards are not the only products that are formed In such...

Страница 23: ...ton thread The crucible is in direct contact and is ig nited by the fixed ignition wire of the decomposi tion vessel The sample is weighed directly into the disposable crucible In most cases no additi...

Страница 24: ...capsules see Accessories and undergo com bustion together with the capsules For substances with low flammability or low calorific substances use combustion aids see Accessories Before the capsules or...

Страница 25: ...respective tempera ture range 22 C 25 C or 30 C is necessary Adjustment must be performed in the following cases When first commissioning the calorimeter and when its place of installation has been ch...

Страница 26: ...thermal capacity may require performance of several measurements Using various statistical criteria the average value is calculated and is used as the thermal capacity for subsequent determina tions...

Страница 27: ...ubstance directly into the crucible with an accuracy of 0 1 mg If necessary put some distilled water or a solution into the decomposition vessel The maximum acceptable weight of the sample that is add...

Страница 28: ...mented by one You can stop the use of the user specific desig nation again every time call up the Designati on dialogue delete the designation and click on OK Highlight the Calibration field if you wi...

Страница 29: ...Preparation for measurement screen has not yet been opened open it The weights are in put in the following sequence Weight of combustion aid 2 if defined Weight of the sample Weight of combustion aid...

Страница 30: ...s it passes over the sensor area For this the decomposition vessel is passed over the sensor area A beep sounds when detection has been successful You can then click on the Start button Note When work...

Страница 31: ...e cal culated thermal capacity also appear here You can cancel the measurement at any time by clicking on Cancel After a measurement the screen switches auto matically to the Measurements tab You can...

Страница 32: ...these para meters and the relevant calculation formulae for the complete results can be found in the respec tive standard The screens are adapted to suit the standard that was selected When you have c...

Страница 33: ...easurements currently displayed is printed not in combination with se rial printer C1 50 Sample Rack A tab with the assignment and status of the sample rack accessories is dis played see page 46 Delet...

Страница 34: ...s and months Within each month the right hand window then displays the measurement organi sed by days Select the desired day and click on the Evaluati on button The list of the measurements on the sel...

Страница 35: ...calibration and the number of ignitions are displayed Click on the Check calibration for selected de composition vessels and functions button Three additional tabs appear listing the calibration a che...

Страница 36: ...statistics button to print the complete statistics on a connected printer Press the Delete statistics button to delete the selec tion from the statistics that are referred to during calibration Click...

Страница 37: ...asurements UCL mean value 3 x sigma sqrt N UWL mean value 2 x sigma sqrt N LWL mean value 2 x sigma sqrt N LCL mean value 3 x sigma sqrt N If you click on Show all all calibrations not just those sele...

Страница 38: ...hose settings in a screen with seven tabs Evaluation tab Default evaluation NAfter a measurement has been completed as a rule the results are exten ded and corrected in accordance with the appli cable...

Страница 39: ...process the first two calorific values are checked to ensure they fall within 120 J If the difference between them is greater than 120 J a warning appears that a third measurement is required The thi...

Страница 40: ...lected igniti on aid Click on Add to add a new ignition aid to the list with the data that were input Click on Cancel to make no changes Ignition aids Add new ignition aid decomposition The venting of...

Страница 41: ...ry you can change the values for Baud rate parity data bits and stop bits Click on OK to use all the changed settings for the subsequent calorimetric procedures Click on Cancel to leave all the settin...

Страница 42: ...B printers which the use the PCL printer language to the C 6000 We recommend the HP Business Inkjet 1200 or its successor models Network printer When you have selected a network printer you must then...

Страница 43: ...43 Sound Activation of the speakers...

Страница 44: ...avigate the left hand selection field further to obtain more information Click on the desired topic then click on the right hand field with the arrow symbol Here you can obtain detailed information on...

Страница 45: ...ition vessel can be read Click on Stop to stop the function test Hardware details In addition you can switch to the Hardware de tails tab This tab shows you all the information about the digital input...

Страница 46: ...the Print button on the balance Pressing the Print button automatically opens the preparation dialogue box and the weighted sample value is entered automatically If External Energy 2 is not set to use...

Страница 47: ...lance key can be used to assign the weighted sample values to the appropriate input fields The balance value is always entered into the cor responding field In order to close the dialogue box the cru...

Страница 48: ...btain from IKA or can download a version for printing from the IKA website at www ika com If your appliance requires repair return it in its ori ginal packaging Storage packaging is not suffici ent wh...

Страница 49: ...rimeter is open and has been ven ted and emptied the error message is displayed once again this time with the Confirm button Troubleshooting Cleaning Switch the device off Switch the cooling water sup...

Страница 50: ...er initiates a system test directly the Confirm button is clicked Af ter you have taken the actions described in the Help or in the operating instructions click on the Restart button to start the syst...

Страница 51: ...ction cannot be perfor med The selected function cannot be used because the temperature of the cooling water has not reached the required values Acknowledge the alarm Check the cooling water flow Chec...

Страница 52: ...ignition system Measurement was cancelled by the user This error message is triggered in the Close Run Open conditions if the user the presses the Can cel button Acknowledge the error message to rever...

Страница 53: ...position vessel Contact IKA Customer Service xxxxxxxxxxx This Rfid ID cannot be assigned The Rfid value detected does not match any of the decomposition vessel registered at the C 6000 Acknowledge the...

Страница 54: ...r work using the calorime ter can be performed only once the system test has been com pleted successfully Acknowledge the error message in order to switch to the System Check status Press the Restart...

Страница 55: ...performance of the ser vicing actions Click on Confirm to acknowledge performance of the servicing actions The acknowledgement is saved and can be checked by the Service En gineers If you click on th...

Страница 56: ...length C 710 8 Cotton wool threads cut to length thick C 16 Parafilm 1000x50 C 17 Paraffin liquid 30 ml C 15 Paraffin strips 600 pieces package C 9 Gelatine capsules 100 pieces C 10 Acetobutyrate cap...

Страница 57: ...ing temperature max C 30 Temperature measurement resolution K 0 0001 Cooling medium temperature min C 12 Cooling medium temperature max C 27 Cooling medium permissible operating pressure bar 1 5 Cooli...

Страница 58: ...max C 30 Perm humidity rel 80 Protection to DIN EN 60529 IP 20 RS 232 interface yes USB interface yes Rated voltage V 220 240 Rated voltage V 100 120 Frequence Hz 50 60 Power consumption W 1700 Fuses...

Страница 59: ...ature min C 12 Cooling medium temperature max C 27 Cooling medium permissible operating pressure bar 1 5 Cooling medium water quality tap water Type of cooling continuous flow Flow rate min l h 60 Flo...

Страница 60: ...max C 30 Perm humidity rel 80 Protection to DIN EN 60529 IP 20 RS 232 interface yes USB interface yes Rated voltage V 220 240 Rated voltage V 100 120 Frequence Hz 50 60 Power consumption W 1700 Fuses...

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Страница 64: ...IKA Werke GmbH Co KG Janke Kunkel Str 10 D 79219 Staufen Tel 49 7633 831 0 Fax 49 7633 831 98 sales ika de www ika com 20005022c...

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