IKA C 2000 basic Скачать руководство пользователя

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IKA



-WERKE C 2000 basic / control

Ver. 04 08.07

3DJH

Standard without titration

Standard with titration

Carbon: H2 input, without titration

Carbon: H2 input, with titration

Carbon: Volatile input, without titration

Carbon: Volatile input, with titration

Acid correction based on ASTM 1989

Acid correction based on ASTM 240

7KH FDUERQ FDOFXODWLRQ PRGHVPHQWLRQHG DUH XVHG H[FOXVLYHO\ IRU H[DPLQD

WLRQVRIWKHJURVVFDORULILFYDOXHRIFDUERQ

In addition to the heat of solution from the formation of acid, they also take into con-

sideration the percentage of ash and, depending on the carbon calculation mode

selected, calculate the percentage of water from the moisture level of the sample

and the percentage of volatile components.

Meaning of the parameters used:

4([WUDQ

Extraneous energy from combustion of the cotton thread or

other ignition aid; 70 J is automatically taken into account for

the electrical ignition energy.

4([WUDQ

Extraneous energy from the burning of additional combustion

aids.

+ 2(ODQD

The percentage of combustion water in the sample

6XOIXUDQ

The percentage of sulfur

1LWURJHQDQ

The percentage of nitrogen

+\GURJHQDQ

The percentage of hydrogen water in the combustion sample

%D2+

The titrated quantity of 0.1 N barium hydroxide solution (titra-

tion of distilled water with which the decomposition vessel was

washed out after the experiment)

1D &2

The quantity of sodium carbonate solution (in accordance with

DIN 20 ml 0.05 N) added in the decomposition vessel

+&O

The titrated quantity of 0.1 N hydrochloric acid (titration of dis-

tilled water with which the decomposition vessel was washed

out after the experiment)

1D2+

The titrated quantity in ml (0.0866 N)

6XUIPRLVWXUHUDZ

The percentage of water from the approximate moisture

$VKDQ

The percentage of ash

+\JUPRLVWXUHDQ

The percentage of water from the hygroscopic moisture

9RODWLOHVUDZ

The percentage of volatile components

VWDQGDUGFDOFXOD

WLRQPRGHV

FDUERQFDOFXOD

WLRQPRGHV

H[SHULPHQW

SDUDPHWHUV

Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com

Содержание C 2000 basic

Страница 1: ...service in house repair center WE BUY USED EQUIPMENT Sell your excess underutilized and idle used equipment We also offer credit for buy backs and trade ins www artisantg com WeBuyEquipment REMOTE IN...

Страница 2: ...01 a WERKE Calorimeter System C 2000 EDVLF C 2000 FRQWURO 23 5 7 1 16758 7 216 1 86 Reg No 4343 01 Vers 04 08 07 Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisant...

Страница 3: ...Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com...

Страница 4: ...clarons sous notre responsabilit que se prodiut est conforme aux r gle mentations 89 336 CEE et 2006 95 CEE et en conformit avec les normes ou documents normalis s suivant DIN EN IEC 61 010 1 et DIN E...

Страница 5: ...WKDW LV RI LPSRUWDQW WR HQVXUH SUREOHP IUHH WHFKQLFDO RSHUDWLRQ RI WKH GHYLFH Failure to observe this information may result in damage to the calorimeter system This symbol identifies information that...

Страница 6: ...2 HVFULSWLRQ RI WKH V VWHP FRPSRQHQWV 4 1 C 2000 EDVLF 4 1 4 2 C 2000 FRQWURO 4 3 4 3 Cooling 4 4 DORULPHWULF PHDVXUHPHQWV 5 1 Determination of gross calorific value 5 1 5 2 Corrections 5 2 5 3 Comple...

Страница 7: ...ion 9 4 SHULPHQW VLPXODWLRQ DUH DQG PDLQWHQDQFH 11 1 Maintenance menu 11 1 11 2 Inner vessel sieve 11 2 11 3 Dirt trap in the water supply line 11 2 11 4 Maintenance for the water circuit 11 3 11 5 Ch...

Страница 8: ...ion vessel to burst 7KH VWDQGDUG GHFRPSRVLWLRQ YHVVHOV PXVW QRW EH XVHG IRU H DPLQDWLRQV RQ VDPSOHV WKDW DUH FDSDEOH RI H SORGLQJ W LV DEVROXWHO HVVHQWLDO WR XVH D VSH FLDO KLJK SUHVVXUH GHFRPSRVLWLRQ...

Страница 9: ...SHULPHQW DXWRFODYHV and must be tested by a SUR IHVVLRQDOO WUDLQHG SHUVRQ each time before they are used An individual application is understood here to mean a series of experiments that are performed...

Страница 10: ...ents listed in 1 National regulations and laws for operating pressure containers must be observed Anyone who operates a pressure container must maintain it in proper condition must monitor it and perf...

Страница 11: ...IKA WERKE C 2000 basic control Ver 04 08 07 Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com...

Страница 12: ...value and how to calculate reference states Chapter 10 explains the option of simulating experi ments with the calorimeter system In Chapter 11 you will find some important notes on system upkeep and...

Страница 13: ...routinely used for determination of gross calorific values of solid and liquid substances The accessories of the system ensure cus tomized adaptation to laboratory tasks see Chapter 13 The system is...

Страница 14: ...see Chapter 4 3 Cooling water temperature Operating mode 12 C to 23 C isoperibolic 25 C 12 C to 23 C dynamic 25 C 23 C to 28 C isoperibolic 30 C 23 C to 28 C dynamic 30 C A monitor and external keyboa...

Страница 15: ...IKA WERKE C 2000 basic control Ver 04 08 07 Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com...

Страница 16: ...nt prerequisite in ensuring the high measurement precision of the system The following conditions must therefore be maintained at the set up location No direct sunlight No drafts for example next to w...

Страница 17: ...nt of the damage and send it to us by mail rail or special delivery 6FRSH RI GHOLYHU EDVLF FRQWURO HVFKUHLEXQJ 1x Grundger t Beilegeset Netzanschlusskabel Betriebsanleitung 1x Grundger t C 5040 CalWin...

Страница 18: ...nctions are also displayed as a line of text The results of the experiment are stored together with the experiment parameters and may be printed out whenever desired Communication with external periph...

Страница 19: ...paratus until the pressure set by the user has been reached 30 bar Water from an external pressure source a water faucet laboratory thermostat or cooler flows into the device and is heated up to the...

Страница 20: ...ut can take place via the interfaces of the peripheral devices or the PC keyboard The structure of the measuring cell and the experiment process are similar to de vices with a control panel basic I RX...

Страница 21: ...his by placing a pressure control valve for exam ple the IKA C 25 far enough forward in the circuit Another important characteristic value for connecting a cooler thermostat is the switch off level th...

Страница 22: ...containing hydrogen undergo combustion is present in a liquid state No oxidation of the atmospheric nitrogen has taken place The gaseous products after combustion consist of oxygen nitrogen carbon dio...

Страница 23: ...alorific value it is then possible to determine the quantity of heat that is introduced thereby The result of the experiment must be corrected by this amount of heat The C 14 disposable crucible is a...

Страница 24: ...all solid residues must be examined for any signs that combustion was not complete Normally solid substances can be burned directly in powder form Rapidly burning substances for example benzoic acid m...

Страница 25: ...erence substance undergoes combus tion in the decomposition vessel under the conditions of the experiment Since the gross calorific value of the reference substance is known it is possible after com b...

Страница 26: ...luded with delivery and connect the hose to your oxygen supply on the laboratory side On the pressure side the hose is designed with an R screw thread A NPT adapter piece is delivered with all hoses I...

Страница 27: ...r The built in dirt trap should be placed in the holder designed for it Now connect the water outlet line 4 to the water outlet adapter The lines are correctly connected if you overcome a distinct res...

Страница 28: ...water inflow line of the calorimeter with the output of the thermostat and connect the water outlet line with the input Secure both hoses so that they will not be unintentionally loosened with the hos...

Страница 29: ...onnection point with a pressure reducer smallest permitted bending radius 80 mm The C 29 reducer valve accessory for the oxy gen cylinder features an R inch thread for con necting the pressure hose Th...

Страница 30: ...ectronic scale or a printer were delivered with the calorimeter system they should now be connected A screen keyboard and or PC can also be connected now The connection sockets are located on the rear...

Страница 31: ...ccepting any data that may have been entered 4 HO NH if you have entered a character sequence in a dialog box for example the weight of the combustion sample you can delete the character to the left o...

Страница 32: ...9 RQWUDVW FRQWURO used to control the display contrast RFN VFUHZ by loosening the lock screw you can change the angle of inclina tion of the display To lock it in place the screw must be tightened aga...

Страница 33: ...table the option can activated in the selected line identified by x or can be deactivated again identified by with the space bar 7DE ends work in the table and activates the next dialog element 2 ends...

Страница 34: ...the splash screen or if you do not then automatically after 10 sec onds the system check is started The system check verifies whether the cooling water is flowing through the calorimeter at least 30 s...

Страница 35: ...WH RI WKH FDORULPHWHU 1R PHDVXUHPHQWV PD EH UXQQLQJ DQG WKH LQQHU YHVVHO PXVW QRW EH ILOOHG KHQ XVLQJ WKH FRROHU 9 SOHDVH WDNH FDUH WKDW WKH EDWK LV ILOOHG WR WKH XSSHU OHYHO PP EHORZ WKH XSSHU HGJH R...

Страница 36: ...ystem check is continued with DFN If the system check still does not permit operation in the set operating mode after 3 minutes it is possible to adjust the system to the appropriate mode correspondin...

Страница 37: ...l menu and dialog windows You can reach part with the menu line that is called with the 0HQX key or the HO key With the arrow keys you can move the cursor through the menu line and with the RZQ DUURZ...

Страница 38: ...example March 03 D day of the month RXU hour entry 0 midnight 0LQXWH minute entry 6HFRQG second entry e Compare the entries with the current date and time and correct the entries as ap propriate If yo...

Страница 39: ...rating mode the experiment initialization the reference gross calorific value and the unit of measure of the gross calorific value To do this place the cursor in the menu line on RQI open the menu and...

Страница 40: ...essel must be re moved from the measuring cell and suspended again 8VU GHI QDPH Here you can specify whether you will enter the 6DPSOH QDPH yourself in the 6DPSOH QDPH entry field or in the 6DPSOH dia...

Страница 41: ...ulation based on a shortened dynamic procedure The temperature of the outer vessel is 25 C This mode can run with cooling water temperatures of from 12 C to 23 C QDPLF DW Measurement and calculation b...

Страница 42: ...ergy is set to 50 J 0 J without with combustible crucible and the 8VHU entry field and 6DPSOH SURSHU in the 6DPSOH dialog box remain empty 8QLWV configuration field The unit of measure of the caloric...

Страница 43: ...ed may be connected 3RUW configuration field No entries are possible in the 3RUW field The scale is always connected to COM1 DXG configuration field The data transmission rate between the scale and th...

Страница 44: ...s energy is already entered in this dialog box R J DLG configuration field In combination with the configuration field ZLWK FRPE DLG the gross calorific value of the combustion aid must be entered in...

Страница 45: ...IKA WERKE C 2000 basic control Ver 04 08 07 Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com...

Страница 46: ...VVHO WKH KHDW FDSDFLW RI WKH V VWHP PXVW EH GHWHUPLQHG E FDOLEUDWLRQ IRU HDFK GH FRPSRVLWLRQ YHVVHO GHFRPSRVLWLRQ YHVVHO PD RQO EH XVHG LQ WKH PHDV XULQJ FHOO LQ ZKLFK LW KDV DOVR EHHQ FDOLEUDWHG 7KH...

Страница 47: ...WV PXVW QRW EH H FKDQJHG EHWZHHQ WKH YDULRXV GHFRPSRVLWLRQ YHVVHOV VHH WKH HQJUDYLQJ RQ WKH LQGLYLGXDO SDUWV Substances of which the combustion behavior is not known must be examined for their combust...

Страница 48: ...en into consideration with 4 WUDQ The amount of combustion aid should be as little as possible Almost all substances to be analyzed contain sulfur and nitrogen Under the condi tions that prevail durin...

Страница 49: ...WKHPVHOYHV VHH VWDPSLQJ LQGLYLGXDO SDUWV The decomposition vessel should be prepared with the following steps c Unscrew the cap screw and remove the cover by using the handle 1 cap screw 2 oxygen valv...

Страница 50: ...KHUZLVH GDPDJH PD RFFXU WR WKH GHFRPSRVLWLRQ YHVVHO DPDJHG GHFRPSRVLWLRQ YHVVHOV DUH DW ULVN RI EXUVWLQJ 3OHDVH REVHUYH WKH 2SHUDWLQJ QVWUXFWLRQV IRU WKH GHFRPSRVLWLRQ YHVVHO KHQ ZRUNLQJ ZLWK XQNQRZQ...

Страница 51: ...le decomposition vessels With 7DE you can move the cursor to the following input fields The meaning of the remaining input fields 4 WUDQ Correction for the thermal energy from the cotton thread used a...

Страница 52: ...surement If you do not edit the name the sample number will stay the same for all measurements Example of a 6DPSOH QDPH 6052401 6 Year digit 6 1996 05 Month 1 12 05 May 24 The day of the month here Ma...

Страница 53: ...the decomposition vessel into the filler head of the open measuring cell cover until it catches in place OZD V KROG WKH GHFRPSRVLWLRQ YHVVHO VHFXUHO RQ WKH WRS E WKH FDS VFUHZ The decomposition vessel...

Страница 54: ...pect decomposition vessel or contact IKA service This indicates that the decomposition vessel has reached a maintenance point and that a safety check must be carried out Confirm this message by pressi...

Страница 55: ...the outer vessel is ensured Otherwise the measurement must be inter rupted After this the measuring cell cover closes The decomposition vessel is filled with oxygen for about 60 sec After the tempera...

Страница 56: ...DPSOH SURWHFWLYH JORYHV EUHDWKLQJ PDVN HWF VKRXOG EH ZRUQ ZKHQ ZRUNLQJ ZLWK WKHVH PDWHULDOV 5HVLGXH RI FRPEXVWLRQ WKDW LV KD DUGRXV WR KHDOWK RU GDQJHURXV WR WKH HQYLURQPHQW PXVW EH GLVSRVHG RI DV VS...

Страница 57: ...IKA WERKE C 2000 basic control Ver 04 08 07 Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com...

Страница 58: ...open the RPEV dialog box e Use 7DE and 8S DUURZ RZQ DUURZ to place the cursor on the number of the de composition vessel with which you wish to perform the upcoming calibration experi ments f Open th...

Страница 59: ...LEUDWLRQV FDQ ODWHU EH UHPRYHG IURP WKH OLEUDU RQO E D VHUYLFH WHFKQLFLDQ The calibration experiments are listed in the dialog box The meaning of the col umns in the list of experiments is as follows...

Страница 60: ...rsor on the button and confirm with 2 or press The average value of the selected calibration experiments will thus be assigned to the calorimeter system as the system heat capacity or C value If you p...

Страница 61: ...IKA WERKE C 2000 basic control Ver 04 08 07 Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com...

Страница 62: ...d experiments into two groups Today s experiments and Library Today s experiments are those experiments that have been performed since the system was turned on The library is long term storage 3URFHVV...

Страница 63: ...nts in the list Exception Experiments with status FDO and 3UHS 3UL Prints the list of experiments HO Deletes the experiments that have previously been marked with 6HO or OO Exception FDO 3UHS QIR Open...

Страница 64: ...ments that are stored in the library If VHDUFK PDVN remains empty the display shows the list of the last search procedure The GG option adds the list of the new search procedures to the list of the la...

Страница 65: ...DGH LQ WKH ZLQGRZ OLVW RI FDOLEUDWLRQV 6HH 6HFWLRQ YDOXDWLQJ FDOLEUDWLRQV Several input modes are available for these calculations from which you can select the one that corresponds to your existing s...

Страница 66: ...ich one is used depends on the evaluation pro cedure 1 Evaluation procedure ASTM D1989 D240 D5865 D4809 D5468 E711 A window opens in which the ASTM standard used can be selected and the neces sary eva...

Страница 67: ...hat were determined in the state in which the sample was delivered are identified with raw and parameters from the reference state of analysis moisture are marked with an The dialog box provides input...

Страница 68: ...ous energy from the burning of additional combustion aids 2 O DQD The percentage of combustion water in the sample 6XOIXU DQ The percentage of sulfur 1LWURJHQ DQ The percentage of nitrogen GURJHQ DQ T...

Страница 69: ...EDU after which you can exit the protocol window with 2 You can browse through the protocol with the arrow keys Meaning of the individual parameters VK DQ The percentage of ash in the fuel sample in t...

Страница 70: ...e of the combustion sample in the water and ash free reference state X UDZ The specific heat value of the combustion sample in delivery state X DQ The specific heat value of the combustion sample in t...

Страница 71: ...st reference state 6XOIXU UDZ The percentage of sulfur in the fuel sample in the delivery state 6XUI PRLVWXUH UDZ The percentage of approximate moisture in delivery state 7RWDO ZDWHU UDZ The percentag...

Страница 72: ...f you accidentally perform a calibration instead of a determination of gross calorific value or vice versa By using the increase in tem perature of the incorrectly interpreted measurement it can be co...

Страница 73: ...for the simulated combustion g Confirm the dialog box with 2 You can post process the simulated experiment in the normal manner with the YDOXDWLRQ dialog box see Chapter 9 Evaluation of gross calorifi...

Страница 74: ...easuring cell cover RROLQJ ZDWHU Water flows through the outer vessel and the cooling water temperature is displayed in a window The check can be ter minated manually with 2 or will be terminated auto...

Страница 75: ...he device LUW WUDS LQ WKH ZDWHU VXSSO OLQH If the filter in the water feed line is partially blocked the flow of water in the unit may be reduced This will reduce the regulation quality of the system...

Страница 76: ...ivate the DQFHO function key during the preliminary ex periment after filling the inner vessel The measuring cell cover opens and the water is pumped in the inner vessel While the water is being pumpe...

Страница 77: ...enance menu to purge the system The 7HPS HTXDOL menu item results in overall temperature equalization for the calorimeter which is particularly advantageous for the following messages YHQWLQJ VFUHZ XV...

Страница 78: ...omposition vessel into the filling head of the measuring cell cover and check to make sure it is properly positioned In the Maintenance menu activate the item 2 ILOO The seal washer is now located on...

Страница 79: ...eaning IKA devices use only these cleaning agents that are approved by IKA 7 SH RI GLUW OHDQLQJ DJHQW Paint Isopropanol Construction materials Water with detergent isopropanol Cosmetics Water with det...

Страница 80: ...WK PHVVDJH LQ WKH GLVSOD 0HVVDJH DXVH 5HPHG 1R DVVLJQPHQW SRVVLEOH The decomposition vessel cannot be assigned The system displays the malfunction and interrupts the measurement Other decomposition ve...

Страница 81: ...ot reached in the inner vessel within 240 sec The system displays the mal function and interrupts the measurement Repeat the experiment Check the external water supply for cor rect functionality the f...

Страница 82: ...and look at the temperature displays 7HPS and 7HPS If Temp1 or Temp2 do not change within 60 sec onds there is an error in tempera ture recording Both values are constant In the Maintenance menu exec...

Страница 83: ...his error message is displayed if ignition capability can no longer be ensured during a measure ment The experiment is stopped Check the ignition wire the ignition wire fastening the electrodes in the...

Страница 84: ...xamine the decomposition vessel to be certain it is snugly in place see Section 7 4 the condition of the seal on the filling piston see Section 11 5 the seal of the decomposition vessel C 5010 5012 Op...

Страница 85: ...e output pressure to 1 max 1 5 bar Contact the Technical Service De partment 1R ZDWHU IORZWKURXJK LQ GHYLFH VWDWHV 6WDELOL H 2 ILOOLQJ 7HPS HTXDOL Water supply is interrupted The connections of the in...

Страница 86: ...500 Cooler unit RQVXPDEOHV 2UGHULQJ GHVFULSWLRQ C 710 4 Cotton thread cut to length 500 pieces C 5010 3 Ignition wire replacement 5 pieces C 5012 3 Pt ignition wire replacement 2 pieces C 5003 1 Aqua...

Страница 87: ...IKA WERKE C 2000 basic control Ver 04 08 07 Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com...

Страница 88: ...ng mode Isoperibolic 25 C Isoperibolic 30 C Dynamic 25 C Dynamic 30 C Isoperibolic measuring time About 22 min Dynamic measuring time About 10 min Oxygen operating pressure 30 bar Oxygen test pressure...

Страница 89: ...IKA WERKE C 2000 basic control Ver 04 08 07 Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com...

Страница 90: ...of solution 5 3 Improper functionality 12 1 Interface parameter 6 17 isoperibolic 6 15 Language 6 13 Library 9 1 Liquid substances 7 2 0 Main screen 6 11 Malfunction situations 12 1 Measurement protoc...

Страница 91: ...IKA WERKE C 2000 basic control Ver 04 08 07 Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com...

Страница 92: ...Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com...

Страница 93: ...04 8940 E Mail sales ika com my DSDQ RUHD 0 1 2 293 1 Kobayashi cho 1710 Anyang Trade Center Yamato Koriyama Shi Nara 1107 Buhung dong 639 1026 Japan Dongan gu Tel 81 743 58 4611 Anyang City Kyeonggi...

Страница 94: ...service in house repair center WE BUY USED EQUIPMENT Sell your excess underutilized and idle used equipment We also offer credit for buy backs and trade ins www artisantg com WeBuyEquipment REMOTE IN...

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