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HP 5890 Series II Скачать руководство пользователя страница 191

SVC 5- 29

Calibrate Oven Temperature

To maximize the precision of retention time information, particularly if retention times are to be com-
pared to that of other chromatographs, it may be necessary to calibrate the oven temperature control
circuitry using an independent temperature measuring device.

With the factory- set calibration difference value of 0 (zero), the displayed oven temperature is accurate
to within 1% of the actual temperature (which is expressed in

_

K (Kelvin)).

The HP 5890 Series II provides the means to reset oven temperature monitoring (if necessary) so that
the ACTUAL displayed temperature value accurately represents the correct temperature.

Calibration of the oven temperature control circuitry requires the operator to enter the difference (

delta

)

value (in

_

C) between an independently measured temperature and the corresponding displayed oven

temperature. For example, if the actual measured oven temperature is 148.73

_

C, while the correspond-

ing displayed temperature is 150.00

_

C, the delta value is - 1.27.

Correction Value = Measured Temperature (

_

C) - Displayed Temperature (

_

C)

Setting the Oven Calibration Value

Oven temperature calibration measurements should be made at a temperature in the mid- range of
those temperatures normally attained during operation. Allow ample time (up to 1/2- hour) for thermal
equilibration at the selected temperature. No drift should be observed.

1. Place the temperature sensing probe in the region of the oven which is occupied by the

column(s).

2. Set the oven temperature to the desired level, allowing ample time for thermal equilibration.

3. At the keyboard select the CALIB AND TEST MODE, function 1:

CLEAR

.

1

ENTER

4. CALIB will be displayed, followed by two values; the observed oven temperature (to 0.01

_

C),

and the current delta correction value. Record the current delta correction value. (If problems
occur during recalibration, the value may be re- entered.)

5. Assuming no drift has occurred, the new delta correction value may be entered using the nu-

meric keypad, followed by pressing

ENTER

.

6. CALIB DELTA will be displayed until

ENTER

is pressed again. Then the oven temperature cali-

bration occurs. Note that after oven calibration, the displayed oven temperature value should
closely match the value of the installed temperature measuring device.

NOTE

`

Any delta correction value may be entered within a range of

¦

10.00

_

C. If a value

beyond these limits is entered, the message CORRECTION TOO HIGH is

displayed.

`

Assuming the battery protecting the HP 5890 Series II memory is functional, the

new delta calibration value remains in effect even if the instrument is switched,

disconnected from its power source, or experiences a power failure.

Artisan Scientific - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisan-scientific.com

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Содержание 5890 Series II

Страница 1: ...nt Service Center Repairs Experienced Engineers and Technicians on staff in our State of the art Full Service In House Service Center Facility InstraView Remote Inspection Remotely inspect equipment before purchasing with our Innovative InstraView website at http www instraview com We bUy used equipment We also offer credit for Buy Backs and Trade Ins Sell your excess underutilized and idle used e...

Страница 2: ...ice Manual HP 5890 SERIES II Gas Chromatograph Manual Part No 05890 90320 Edition 1 March 1991 Printed in U S A Artisan Scientific Quality Instrumentation Guaranteed 888 88 SOURCE www artisan scientific com ...

Страница 3: ... Capillary Inlet SVC 2 8 SPLIT SPLITLESS CAPILLARY INLET SVC 2 12 Remove Replace Split Splitless Capillary Inlet SVC 2 12 PROGRAMMABLE COOL ON COLUMN INLET PCOC SVC 2 16 Remove Replace PCOC Inlet SVC 2 16 INJECTION PORT COOLING FAN SVC 2 20 Remove Replace Cooling Fan SVC 2 20 SECTION 3 FLOW PRESSURE CONTROL COMPONENTS SVC 3 1 FLOW PRESSURE CONTROL COMPONENTS SVC 3 1 PCOC EPC MPC Troubleshooting SV...

Страница 4: ... Block 19233A 19235A Versions SVC 4 49 ELECTRON CAPTURE DETECTOR G1223A G1224A VERSIONS SVC 4 53 Remove Replace ECD Cells Weldment and or Heated Block G1223A G1224A Versions SVC 4 53 Clean Anode ECD Cell Weldment G1223A G1224A Versions SVC 4 56 FLAME PHOTOMETRIC DETECTOR FPD SVC 4 58 Clean Replace Photomultiplier Tube PMT SVC 4 58 Clean Replace FPD Filter SVC 4 61 Remove Replace FPD Diode Bridge A...

Страница 5: ...s Remove Replace ECD G1223A G1224A VERSIONS SVC 6 31 Heater and Sensor Cartridges Remove Replace FPD Heater and Sensor Cartridges SVC 6 34 Remove Replace Valve Box Heater and Sensor Cartridges SVC 6 37 Replacing TCD Delta T Temperature Sensor Cartridges SVC 6 39 Remove Replace PCOC Inlet Cryogenic Cooling Cryo Blast Weldment SVC 6 42 Temperature Sensor Data SVC 6 45 SECTION 7 VALVES SVC 7 1 VALVES...

Страница 6: ...move Replace Power Cable SVC 11 11 APPENDIX A PCB CONNECTOR INFORMATION APX A 1 AC POWER PCB CONNECTORS APX A 3 120VAC BOARD APX A 3 220VAC SINGLE PHASE BOARD APX A 3 220VAC SPLIT PHASE BOARD APX A 4 MAIN PCB CONNECTORS APX A 5 P1 KEYBOARD CONNECTOR APX A 5 P2 DETECTOR A PCB CONNECTOR APX A 6 P3 DETECTOR B PCB CONNECTOR APX A 7 P4 ANALOG SIGNAL 1 OUTPUT CONNECTOR APX A 7 P5 ANALOG SIGNAL 2 OUTPUT ...

Страница 7: ...FERED INET PCB APX A 20 DICE PCB APX A 21 DICE CONNECTOR PCB APX A 22 ELECTRONIC FLOW SENSOR MODULE APX A 24 VALVE PCB CONNECTORS APX A 25 Artisan Scientific Quality Instrumentation Guaranteed 888 88 SOURCE www artisan scientific com ...

Страница 8: ...sponding to the employed inlet Maintenance procedures for most of the components are given in the following sections Procedures are supplied to remove replace and or clean various subassemblies based on the current maintenance philosophy i e to allow replacement of the lowest level compo nents applicable for a particular item Specific part numbers are not given in this portion of the service manua...

Страница 9: ...recautions In all nonelectrically oriented sections of this manual the standard Hazardous Voltage Warning strongly recommends turning off all of the power to the instrument However this section as well as most of Service Section requires that some electrical measurements be made on active energized circuits MEASUREMENTS AND OR TESTS THAT NEED TO BE MADE ON ELECTRICALLY ENERGIZED PORTIONS OF THE IN...

Страница 10: ...isolate and then correct the cause of the problem if it is power related The first important bit of information is about the fuses that are internal to the instrument The second bit is the normal sequence of events that oc curs as the instrument is energized Power On Sequence Fuse Information Fuses have been installed at several locations within the instrument for the protection of major power cir...

Страница 11: ...aster Oscillator for clocks begin to function As these other supplies begin the POWER ON PULSE and the CPU portion of the circuitry begin to initialize first themselves and then through the Data Bus and other portions of the instrument One of the initializations that occurs through the Data Bus is in the Triac Control section to produce the control signal for K3 zone power relay on the Main Board ...

Страница 12: ...t a problem with the Clock Section of the Main Board however the CPU Section could also cause this indication Replace Main Board FATAL ERR STACK ERR indicates that stack is beyond legal limits Suspect a problem in the CPU Sec tion of the Main Board Replace Main Board FATAL ERR RUN CNTL indicates that the Run Control task couldn t complete within 25 milliseconds Suspect a problem with the Clock Sec...

Страница 13: ...ature seems reasonable the problem is likely to be in the oven control circuitry FAULT ZONE NAME TEMP RDG where the ZONE NAME could be OVEN INJA INJB DETA DETB or AUX Any of these messages indicates that the specified zone or oven temperature reading was out of acceptable range This most often is the result of an inoperative sensor in the named zone FAULT OUTPUT NAME TEST where the OUTPUT NAME cou...

Страница 14: ...t was previously assigned to a particular signal is no longer recognized The instrument will reconfigure the signal This may occur as a result of detec tor boards having been removed during a repair If these boards have not been recently removed sus pect a failure and refer to Detector Problems later in this section WARN NO DETECTORS indicates that no detector boards are installed or that they are...

Страница 15: ...LEAR DOT 9 DISP TEMP DEMAND To escape from any of the CALIB AND TEST Clear Dot modes press any of the instrument function keys Calib and Test Clear Dot 4 Display Memory This diagnostic routine is initiated from the keyboard by pressing Upon entering this mode a single memory address ADDR and a value VAL will appear on the instrument front panel visual display At this time both the address and the ...

Страница 16: ...nal handling sections of the Main Board Note that the analog sensors i e temperature sensors are NOT tested at this time they are tested after the selftest How ever by linking the A D through the CPU to the D A and by looping the D A output back as an input to the A D most of the Main Board s signal handling circuits are checked The fourth and unless an error is found the final indication is the P...

Страница 17: ...st tallest peak having a height value of about 125 mV at 0 1 V analog output halfheight width of this peak is about 0 13 minutes Each cycle is about 1 5 min utes in length The chromatogram will continue to cycle until the STOP key is pressed The test chroma togram is useful as a troubleshooting aid in deciding whether a lost or noisy signal observed at a con nected integrating or chart recording d...

Страница 18: ...n static protective bags or containers Be certain to utilize these protective devices when storing items of this nature Generally since board or module replacement constitutes the majority of electronic repairs the only electronic test equipment necessary is a quality Volt Ohm Ampmeter The HP 5890 Series II GC contains a minimum of four and a maximum of nine electronic boards The four boards alway...

Страница 19: ...mblies within the instrument or external devices such as an integrator Refer to the main PCB diagrams pages SVC 1 13 and SVC 1 14 Refer to appendix a of this document for information on the main PCB connectors Artisan Scientific Quality Instrumentation Guaranteed 888 88 SOURCE www artisan scientific com ...

Страница 20: ...KS AND TIMING KEYBOARD DETECTORS DAC A D VALVES AND CRYO HEATED ZONES AND TRIACS MAIN PCB FUNCTIONAL ZONES AC POWER SUPPLY TEST POINTS TEST POINTS Artisan Scientific Quality Instrumentation Guaranteed 888 88 SOURCE www artisan scientific com ...

Страница 21: ... CRYO 4 HEATED ZONES 5th HEATED ZONE VALVE 1 2 TRANSFORMER MAIN SWITCH AC PCB OVEN TRIAC OVEN HEATER OVEN FAN MOTOR J1 J2 DETECTOR B PCB J2 J1 J12 J1 J1 ANALOG SIGNAL 1 OUTPUT ANALOG SIGNAL 2 OUTPUT REMOTE START STOP ZONE TEMP SENSORS INJECTION PORT FAN OVEN FLAP STEPPER MOTOR IGNITOR VLVA VLVB P10 J14 J9 LINE CORD Artisan Scientific Quality Instrumentation Guaranteed 888 88 SOURCE www artisan sci...

Страница 22: ... Heating of the inlet zones is not covered in this section For information on the zone heater sensor systems refer to Section 6 of the service portion of this document Zone Tem perature This document is not meant to provide instruction for first time installation of the inlet options discussed Add on sheets exist for just this purpose and should be referenced when performing a first time instal la...

Страница 23: ...hardware associated with the inlet s liner column liner nuts ferrules makeup gas adapt er etc 6 Remove the injection port cover by grasping its back edge and lifting it upward 7 Remove the two screws securing the left side panel along its bottom edge 8 Slide the left side panel towards the rear of the instrument and lift 9 Disconnect the Carrier Gas Inlet which con nects to a fitting either at the...

Страница 24: ... of the inlet Use caution to avoid sharp bends when bending tubing Sharp bends may crimp the tubing 16 If the inlet is to be replaced prepare the replacement inlet by pre bending its tubing into orien tations similar to that of the removed inlet 17 Slide the heater and sensor cartridges into the heated block of the inlet being installed 19 Replace any insulation that was removed from around the ba...

Страница 25: ... installed and in good condition 25 Turn off the supply gas 26 Remove the cap plug from the end of the inlet 27 Install the column and associated hardware removed in step 5 28 Restore the supply gas pressure 29 Install the left side panel and secure using two screws 30 Install the injection port cover 31 Restore power to the HP 5890 Series II SEPTUM NUT ASSEMBLY SEPTUM WELDMENT Artisan Scientific ...

Страница 26: ...mn liner nuts ferrules makeup gas adapt er etc 6 Remove the injection port cover by grasping its back edge and lifting it upward 7 Remove the two screws securing the left side panel along its bottom edge 8 Slide the left side panel towards the rear of the instrument and lift 9 Disconnect the Carrier Gas Inlet labelled C which connects to a fitting either at the EFS or at a mass flow controller mou...

Страница 27: ...k strap from the base weldment by removing two screws 18 Remove the top insert weldment and o ring from the base weldment Use caution to avoid sharp bends when bending tubing Sharp bends may crimp the tubing 19 If the inlet base weldment is to be replaced prepare the replacement by pre bending its tubing into orientations similar to that of the re moved inlet 20 Secure the heated block and heated ...

Страница 28: ...t the insulation to ensure that it is in good condition Replace if required 34 Install the bottom insulation and bottom insulation cover on the column oven wall 35 Tighten the two screws securing the bottom insulation cover to the column oven wall 36 Remove the septum nut assembly from the top insert weldment 37 Inspect the septum to insure that it is properly installed and in good condition Repla...

Страница 29: ... all gas supplies 5 At the bottom of the inlet s to be removed in side the column oven remove the column and hardware associated with the inlet s liner column liner nuts ferrules makeup gas adapt er etc 6 Remove the injection port cover by grasping its back edge and lifting it upward 7 Remove the two screws securing the left side panel along its bottom edge 8 Slide the left side panel towards the ...

Страница 30: ...he shell weldment 15 Loosen the two screws securing the insulation cover inside the column oven 16 Rotate the cover freeing it from its securing hardware and remove the cover and three pieces of lower insulation 17 Remove the reducing nut flat washer and anealed seal using a 1 2 inch wrench 18 Use a 3 4 inch wrench to loosen but not re move the retaining nut below the heated block 19 Use a Pozidri...

Страница 31: ...nstall the heated block onto the stem of the shell weldment 32 Install the retaining nut on the base of the shell weldment securing the heated block to the shell weldment 33 Install any removed insulation around the heated block within the cavity provided in the shell weldment 34 Carefully install the inlet securing it to the instrument with two Pozidriv screws NOTE To lessen the possibility of pr...

Страница 32: ...t tube on the shell weldment and secure using a 1 2 inch wrench 44 Install the liner in the shell weldment 45 Install a cap or plug on the end of the inlet in side the column oven 46 Restore the supply gas pressure 47 Check for leaks at all of the newly mated fittings 48 Turn off the supply gas 49 Remove the cap plug from the end of the inlet 50 Install the column and associated hardware removed i...

Страница 33: ...rn off all gas supplies 5 At the bottom of the inlet s to be removed in side the column oven remove the column and hardware associated with the inlet s liner column liner nuts ferrules makeup gas adapt er etc 6 Remove the injection port cover by grasping its back edge and lifting it upward 7 Remove the two screws securing the left side panel along its bottom edge 8 Slide the left side panel toward...

Страница 34: ...e shell weldment 15 Loosen the two screws securing the insulation cover inside the column oven 16 Rotate the cover freeing it from its securing hardware and remove the cover and three pieces of lower insulation 17 Remove the reducing nut flat washer and anealed seal using a 1 2 inch wrench 18 Use a 3 4 inch wrench to loosen but not re move the retaining nut below the heated block 19 Use a Pozidriv...

Страница 35: ...ll install the heated block onto the stem of the shell weldment 32 Install the retaining nut on the base of the shell weldment securing the heated block to the shell weldment 33 Install any removed insulation around the heated block within the cavity provided in the shell weldment 34 Carefully install the inlet securing it to the instrument with two Pozidriv screws NOTE To lessen the possibility o...

Страница 36: ...t tube on the shell weldment and secure using a 1 2 inch wrench 44 Install the liner in the shell weldment 45 Install a cap or plug on the end of the inlet in side the column oven 46 Restore the supply gas pressure 47 Check for leaks at all of the newly mated fittings 48 Turn off the supply gas 49 Remove the cap plug from the end of the inlet 50 Install the column and associated hardware removed i...

Страница 37: ...all gas supplies 5 At the bottom of the inlet s to be removed in side the column oven remove the column and hardware associated with the inlet s liner column liner nuts ferrules makeup gas adapt er etc 6 Remove the injection port cover by grasping its back edge and lifting it upward 7 Remove the two screws securing the left side panel along its bottom edge 8 Slide the left side panel towards the r...

Страница 38: ...embly or op tional manual injection assembly by rotating it counter clockwise Be careful not to loose the septum insert or PCOC insert spring which are installed under the injection assembly AUTO INJECTION ASSEMBLY OPTIONAL MANUAL INJECTION ASSEMBLY DUCKBILL SEPTUM SEPTUM PCOC INSERT SPRING AIR DEFLECTOR WELDMENT INSULATION CAVITY SLEEVE SCREW INSERT HEATER SENSOR CABLE ASSEMBLY 13 Remove the air ...

Страница 39: ... inlet enough to expose the heated block 17 If installed remove the cryo blast tube from the inlet weldment a b 18 Remove any insulation from around the inlet Use caution to avoid sharp bends when bending tubing Sharp bends may crimp the tubing 19 If the inlet is to be replaced prepare the replacement inlet by pre bending its tubing into orien tations similar to that of the removed inlet 20 Replac...

Страница 40: ...ock portion of the inlet 26 Install the air deflector and secure it to the weldment using one screw 27 Install the injection assembly septum PCOC insert spring and insert the injection assembly secures the other items to the inlet weldment 28 Install the liner and all other hardware except the column removed in step 5 29 Restore the supply gas pressure 30 Check for leaks at all of the newly mated ...

Страница 41: ...If an autosampler is installed on the instrument it will be necessary to remove it and its mount ing bracket to allow removal of the left side cov er as follows a Remove the autosampler tray from its mounting bracket by first simultaneous ly lifting and turning the two tray locks which hold it in position then sliding the tray away from the instrument b Lift the autosampler tray from its mount ing...

Страница 42: ...nector P7 on the main PCB exposed right side of instrument WHEN DISCONNECTING A PLUG PULL ON THE PLUG NOT ON ITS WIRES PULLING ON THE WIRES MAY CAUSE BREAKAGE 10 Disconnect connector P7 from its receptacle by pulling it straight off Heated zones corre sponding to sensor lead locations are labeled to the right of the P7 connector receptacle on the main PCB Q6 C9 P7 Q3 C10 1 3 5 7 9 11 13 2 OVEN 4 D...

Страница 43: ...ll on the wire to ensure that the pin is locked in the connector 15 Insert connector P7 into its corresponding receptacle on the main PCB 16 Install the new fan and fan cover and secure using two screws 17 Install the rear panel and secure it to the instrument using four screws 18 Install the right side panel and secure using four screws 19 Install the electronics carrier top cover 20 If removed i...

Страница 44: ... respectively This document is not meant to provide instruction for first time installation of any of the options dis cussed Add on sheets exist for just this purpose and should be referenced when performing a first time installation TABLE OF CONTENTS FLOW PRESSURE CONTROL COMPONENTS SVC 3 1 PCOC EPC MPC Troubleshooting SVC 3 2 Remove Replace Inlet Flow Control Components SVC 3 5 Remove Replace Sp...

Страница 45: ...ection port This will also yeild a 10 to 20 ml min septum purge vent flow Expected ranges of operation follow Temperature Control Range Ambient 4 Degrees C to 450 Degrees C Temperature Programming 0 to 100 Degrees c minute Typical Cooling Rate oven fan only Standard 10 5 mins CO2 Cryo Blast 7 5 mins LN2 Cryo Blast 4 5 mins Oven Track Mode Standard Injection prot temperature is adjusted real time t...

Страница 46: ...ent the injection port from reaching or maintaining pressure setpoint Leaks at the Septum Column fitting Septum Purge Control Column Head Pressure gage or Purge Vent restrictor could also make injection port pressure control difficult These leaks should be checked by capping off the injection port or suspected part to isolate it rather then using soap solution leak detection fluid The EPC uses a d...

Страница 47: ...short Pressure and Temperature are not controllable Configuration is wrong No flow and high zero 1 Pressure transducer probably defective Background Zero 6psi 1 Possible problem with either EPC pressure transducer or EPC control bd Artisan Scientific Quality Instrumentation Guaranteed 888 88 SOURCE www artisan scientific com ...

Страница 48: ...Manual Pressure Control MPC flow module A separate procedure also exists for replacement of the split splitless capillary inlet solenoid valve 1 Set the main power line switch to the off position 2 Disconnect the power cable from its receptacle 3 Allow time for the oven and heated zones to cool 4 When the heated zones are cool turn off all gas supplies 6 Remove the two screws securing the left sid...

Страница 49: ... and fittings ensure that all o rings are properly installed 11 Install the flow module in the instrument 12 Connect the plumbing removed in step 8 13 Restore all gas supplies 14 Leak check all installed fittings 15 If the system is leak free install the left side panel and secure using two screws 16 Restore power to the instrument FLOW MODULE BRACKET TYPICAL Artisan Scientific Quality Instrumenta...

Страница 50: ...ated zones to cool 4 When the heated zones are cool turn off all gas supplies 5 Remove the two screws securing the left side panel along its bottom edge 6 Slide the left side panel towards the rear of the instrument and lift 7 Remove the four screws securing the rear cover to the instrument 8 Slide the rear cover towards the rear of the instru ment 9 Remove the electronics carrier top cover above ...

Страница 51: ... Install the replacement solenoid valve in the same location and orientation as the old one 16 Secure the solenoid valve to the flow control bracket by tightening two screws 17 Trace and free the solenoid valve electrical leads along their path to the P8 connector at the upper right corner of the main PCB 18 Route the leads for the new solenoid valve along the same path securing them with plastic ...

Страница 52: ... lock ing lance to its proper height to ensure reten tion of the pin in the connector 21 Prepare the pins corresponding to the replace ment sensor cartridges by adjusting their lock ing lances using the lance reset portion of the tool 22 Insert the pins for the replacement sensor into their appropriate locations in the plug making sure the locking lance on each pin seats into its hole through the ...

Страница 53: ...tings ensure that all o rings are properly installed 25 Connect the plumbing to the new valve 26 Restore gas supplies to the instrument 27 Check for leakage at all installed fittings 28 If the system is leak free verify operation of the split splitless system by operating the solenoid valve via the keyboard Artisan Scientific Quality Instrumentation Guaranteed 888 88 SOURCE www artisan scientific ...

Страница 54: ... panel along its bottom edge 6 Slide the left side panel towards the rear of the instrument and lift 7 Disconnect the tubing nut from the PCOC pro portional control valve 8 Remove the plastic M8 nut securing the septum purge outlet from the inlet to the septum purge regulator 9 Remove the two 7 mm nuts securing the EPC flow control bracket to the front of the instru ment 10 Remove any hardware att...

Страница 55: ...acket 18 Remove the EPC cable from the EPC sensor PCB and the connector receptacle on the pro portional control valve 19 If the EPC sensor PCB is to be replaced remove it by removing the two nuts securing it to the EPC flow control bracket NOTE Steps 20 through xx refer to disassembly of the various components attached to the proportional control valve Skip to step xx if you wish to skip this 20 R...

Страница 56: ...y damaged or suspect components particularly o rings SCREW INLET BYPASS CLAMP PCOC INLET BRAZEMENT RESTRICTOR RESTRICTOR O RING O RING When connecting lines and fittings ensure that all o rings are properly installed 25 Assemble the EPC components in the reverse order of disassembly 26 Restore all gas supplies 27 Leak check all installed fittings 28 If the system is leak free install the left side...

Страница 57: ...ch to the off position 2 Disconnect the power cable from its receptacle 3 Allow time for the oven and heated zones to cool 4 When the heated zones are cool turn off all gas supplies 5 Remove the two screws securing the left side panel along its bottom edge 6 Slide the left side panel towards the rear of the instrument and lift 7 Disconnect plumbing fittings as necessary to remove the flow module f...

Страница 58: ...place the flow control component desired When connecting lines and fittings ensure that all o rings are properly installed 11 Assemble the MPC components in the reverse order of disassembly 12 Restore all gas supplies 13 Leak check all installed fittings 14 If the system is leak free install the left side panel and secure using two screws 15 Restore power to the instrument Artisan Scientific Quali...

Страница 59: ...its receptacle 3 Turn off all gas supplies 4 Remove the electronics carrier top cover 5 Remove the right side panel by removing four screws two each along its top and bottom edges The following steps require protection against ESD Electro Static Discharge Use a grounded wrist strap part no 9300 0969 large or 9300 0970 small connected to a suitable ground Failure to heed this caution may result in ...

Страница 60: ...t straight out 8 Install the pressure control PCB by sliding it into its mounting location on the main PCB 9 Restore all gas supplies to the instrument 10 Install the right side panel and secure using four screws 11 Install the electronics carrier top cover 12 Restore power to the HP 5890 Series II PRESSURE CONTROL PCB TYPICAL Artisan Scientific Quality Instrumentation Guaranteed 888 88 SOURCE www...

Страница 61: ...C B UP INLET A 1 DOWN INLET A0 DOWN MODE A DOWN EPC A DOWN DON T CARE CHOICE OF PID CONSTANTS FORWARD PRESSURE BACK PRESSURE ENABLE DISABLE EPC CHOICE OF PID CONSTANTS TYPICAL SWITCH SETTINGS FOR EPC MPC PCBs Artisan Scientific Quality Instrumentation Guaranteed 888 88 SOURCE www artisan scientific com ...

Страница 62: ...o cool 4 When the heated zones are cool turn off all gas supplies 5 Remove the two screws securing the left side panel along its bottom edge 6 Slide the left side panel towards the rear of the instrument and lift 7 Remove the four screws securing the rear cover to the instrument 8 Slide the rear cover towards the rear of the instru ment 9 Remove the electronics carrier top cover above the signal c...

Страница 63: ...e plug Re lease the locking tabs and pull the plug straight out from its receptacle Locking Tabs P11 WHEN DISCONNECTING A PLUG PULL ON THE PLUG NOT ON ITS WIRES PULLING ON THE WIRES MAY CAUSE BREAKAGE 14 Remove the EFS module from the instrument 15 Install the replacement EFS module in its compartment 16 Secure the EFS module to the instrument using two screws 17 Connect the plumbing to the EFS mo...

Страница 64: ...uggested that the flow rate through each channel be different in order to verify that the plumbing for the two channels has not been cross connected 20 If a flow rate value for either channel is displayed which does not correspond to the value ob tained using a bubble flow meter leak test the entire system If the system is completely leak free the EFS may require calibration Artisan Scientific Qua...

Страница 65: ...w through the channel to be calibrated will be interrupted detectors should be turned off particularly an NPD or TCD and the oven cooled to ambient temperature to protect columns D A flow measuring device is required accurate to better than 1 ml min D The EFS is calibrated to measure volumetric flow at standard temperature and pressure Flows measured at ambient temperature with a bubble flow meter...

Страница 66: ...hannel the GAIN calibration value must be set based upon a measured flow rate 1 At the keyboard press FLOW GAIN A or GAIN B is displayed followed by two values the observed flow rate through the channel and the current GAIN calibration value for the channel 2 Connect the gas supply to the channel being calibrated DO NOT connect the OUT fitting for the particular channel 3 Using a suitable flow mea...

Страница 67: ...cedure To enter specific ZERO and GAIN calibration values 1 Select CALIB AND TEST mode function 2 CLEAR 2 ENTER GAIN A or GAIN B is displayed followed by two values the observed flow rate through the channel and the current GAIN calibration value for the channel NOTE Note that Channel A is assumed by default If Channel B is to be calibrated instead press B 2 Enter the desired GAIN calibration valu...

Страница 68: ... position 2 Disconnect the power cable from its receptacle 3 Allow time for the oven and heated zones to cool 4 When the heated zones are cool turn off all gas supplies 6 Remove the two screws securing the left side panel along its bottom edge 7 Slide the left side panel towards the rear of the instrument and lift 8 Disconnect all plumbing from the block When removing the FID or FPD ignitor connec...

Страница 69: ...m the rear of the instrument The block fits on the panel over two standoffs in only one direction 14 Replace the mounting screw on the block and tighten it firmly 15 Connect the plumbing on the rear of the block The fittings are labelled on the block In addi tion D On an FID NPD replace the hydrogen and air tubes The hydrogen tube painted red con nects to the lower fitting The gas tube retainer fi...

Страница 70: ...supplied to the system and leak check all installed fittings 17 If the system is leak free reinstall panels and covers and restore power Artisan Scientific Quality Instrumentation Guaranteed 888 88 SOURCE www artisan scientific com ...

Страница 71: ...nfor mation on the zone heater sensor systems refer to Section 6 of the service portion of this document Zone Temperature This document is not meant to provide instruction for first time installation of the detector options dis cussed Add on sheets exist for just this purpose and should be referenced when performing a first time installation TABLE OF CONTENTS REPLACING DETECTOR COMPONENTS SVC 4 1 ...

Страница 72: ...sions SVC 4 53 Clean Anode ECD Cell Weldment G1223A G1224A Versions SVC 4 56 FLAME PHOTOMETRIC DETECTOR FPD SVC 4 58 Clean Replace Photomultiplier Tube PMT SVC 4 58 Clean Replace FPD Filter SVC 4 61 Remove Replace FPD Diode Bridge Assembly SVC 4 63 Clean Replace FPD Heat Shield Windows SVC 4 66 Replace FPD Jet Assembly and First Heat Shield Window SVC 4 70 Replace Fused Silica Liner SVC 4 76 Repla...

Страница 73: ...C 1 TEST is indicated suspect faulty main PCB Otherwise sus pect a faulty cable or exter nal device 4 Instrument has two detec tors installed but only rec ognizes one 1 Swap detector PCBs 2 If problem persists swap back original detector PCBs to starting configura tion and refer to probable cause b 3 If problem follows the swapped PCB replace the suspect PCB with a known good PCB a Faulty detector...

Страница 74: ...o the off position 2 Disconnect the power cable from its receptacle 3 Allow time for the oven and heated zones to cool 4 When the heated zones are cool turn off all gas supplies 5 At the bottom of the detector s to be removed inside the column oven remove the column and hardware associated with the detector s liner column liner nuts ferrules makeup gas adapter etc 6 If the detector is not going to...

Страница 75: ...CD disconnect the TCD to FID jumper tube from the TCD oven re turn exhaust vent port 14 Remove the two screws securing the detector to the instrument and then lift the block up enough to expose the heater and sensor car tridge wires 15 Carefully slide the three cartridges out of the block The two smaller cartridges are the sen sors and must be handled gently in order to prevent breakage 16 Trace t...

Страница 76: ...ented similarly to those on the detector just removed 19 If a new detector is being installed ensure that the base and vent port of the new detector are capped to prevent contamination 20 Install the heater temperature sensor and delta t sensor cartridges into the heated block 21 Carefully install the detector securing it to the instrument with two screws When installing tubing at the solenoid val...

Страница 77: ...n around the detector block 28 Install the electronics carrier top cover Use caution not to crimp the filament and delta t sensor leads when installing the TCD detector cover 29 Install the TCD detector cover and secure using two screws 30 Install column and any other hardware removed in step 5 of this procedure 31 Restore supply pressure 32 Restore power to the instrument 33 Run a TCD Test Sample...

Страница 78: ... zones are cool turn off all gas supplies 5 Lift the hinged top cover at its front edge exposing the detector area 6 Remove the electronics carrier top cover above the signal cable plugs and receptacles to expose the top edge of the TCD detector PCB 7 Remove the right side panel by removing four screws two each along its top and bottom edges 8 Locate the solenoid valve to be replaced OFF ON RED O ...

Страница 79: ... free the fittings Note the solenoid valve fitting where each tube is attached Corresponding tubes on the new detector must be connected to the same fittings Top View Two TCD Detectors Installed N C N C N O COM COM N O FRONT OF INSTRUMENT 13 Remove the solenoid valve and bracket as a unit by removing the two screws securing the solenoid valve bracket to the instrument 14 Remove the solenoid valve ...

Страница 80: ...install the right side panel and secure using four screws 22 Install the electronics carrier top cover Ensure that all gas supplies are on and all connections are made before applying power to the instrument If flow is interrupted while the TCD is on damage to the detector will occur 23 Restore power to the HP 5890 Series II 24 Verify operation of the TCD solenoid switching valve by turning on the...

Страница 81: ...d top cover at its front edge exposing the detector area 5 Disconnect the ignitor wire lead connector at the mating connection adjacent to the ignitor 6 Use a wrench to remove the ignitor from the FID ignitor castle 7 Ensuring that the washer is in place between the ignitor castle and the threads of the ignitor install the new ignitor tightening it to a snug fit 8 Connect the ignitor wire lead con...

Страница 82: ...r as follows a Remove the autosampler tray from its mounting bracket by first simultaneous ly lifting and turning the two tray locks which hold it in position then sliding the tray away from the instrument b Lift the autosampler tray from its mount ing bracket and set it aside c Remove the autosampler bracket by removing the 6 screws securing it to the instrument 5 Remove the two screws securing t...

Страница 83: ...sembly to its connector at the FID flow manifold 16 Connect the diode bridge assembly spade lug ground cable to the instrument by placing it be neath and tightening the screw that secures it 17 Thread the ignitor wire lead along its path from the diode bridge assembly to the detector igni tor connector 18 Connect the ignitor wire lead connector to the mating connection of the diode bridge assembly...

Страница 84: ...DETECTORS USE HYDROGEN GAS AS FUEL BE SURE ALL HYDROGEN GAS IS TURNED OFF AT ITS SOURCE BEFORE REPLACING ANY FLOW COMPONENTS 1 Set the main power line switch to the off position 2 Disconnect the power cable from its receptacle 3 Allow time for the oven and heated zones to cool 4 When the heated zones are cool turn off all gas supplies 5 Lift the hinged top cover at its front edge exposing the dete...

Страница 85: ...e collector nut over the ignitor castle and spring washer and onto the collector housing hand tight m If employed install the optional PTFE chimney 7 TO REPLACE COLLECTOR ASSEMBLY AS A UNIT a Remove the electronics carrier top cover b Remove the right side panel by removing four screws two each along its top and bottom edges OPTIONAL PTFE CHIMNEY COLLECTOR NUT SPRING WASHER IGNITOR CASTLE IGNITOR ...

Страница 86: ...l lector mount to the thermal strap g Remove the collector mount and collector assembly as a unit The following steps require protection against ESD Electro Static Discharge Use a grounded wrist strap part no 9300 0969 large or 9300 0970 small connected to a suitable ground Failure to heed this caution may result in damage to the instrument When storing or in between handling of PCBs Printed Circu...

Страница 87: ...or at the mating connection adjacent to the ignitor n Install the right side panel and secure using four screws o Install the electronics carrier top cover 8 Restore all gas supplies 9 Restore power to the HP 5890 Series II Artisan Scientific Quality Instrumentation Guaranteed 888 88 SOURCE www artisan scientific com ...

Страница 88: ...om its receptacle 3 Turn off all gas supplies 4 Lift the hinged top cover at its front edge exposing the detector area 5 Remove the electronics carrier top cover 6 Remove the right side panel by removing four screws two each along its top and bottom edges 7 Disconnect the ignitor wire lead connector at the mating connection adjacent to the ignitor 8 Loosen the screws securing the clamps holding th...

Страница 89: ...or mount to the thermal strap 11 Remove the collector mount and collector as sembly as a unit 12 At the bottom of the detector being serviced inside the column oven remove the column and hardware associated with the detector s liner column liner nuts ferrules makeup gas adapter etc 13 Use a 1 4 inch nut driver to remove the jet from the detector weldment 14 Use an inert gas to blow out the detecto...

Страница 90: ...nclosures 20 Install the FID detector PCB by sliding it into its mounting location on the main PCB at the right side of the instrument Installation of the PCB will insert the interconnect into the thermal strap Use caution to avoid damaging the spring at the end of the interconnect 21 Tighten the screws on the clamps which secure the interconnect to the thermal strap 22 Install the collector mount...

Страница 91: ...es 5 At the bottom of the detector s to be removed inside the column oven remove the column and hardware associated with the detector s liner column liner nuts ferrules makeup gas adapter etc NOTE If an autosampler is installed the injection port cover will not be present 6 Remove the injection port cover by grasping its back edge and lifting it upward 7 Lift the hinged top cover at its front edge...

Страница 92: ...t in position then sliding the tray away from the instrument b Lift the autosampler tray from its mount ing bracket and set it aside c Remove the autosampler bracket by removing the 6 screws securing it to the instrument 13 Remove the two screws securing the left side panel along its bottom edge 14 Slide the left side panel towards the rear of the instrument and lift 15 Remove the electronics carr...

Страница 93: ...e collector mount and collector assembly as a unit 22 Use a 1 4 inch nut driver to remove the jet from the detector weldment 23 Use a 1 and 1 4 inch socket to remove the base spanner nut from the detector weldment 24 Remove the thermal strap by removing the five screws securing it to the instrument 25 Remove the two screws securing the detector weldment to the instrument 26 Slide the insulation pl...

Страница 94: ...lock exposed left side of the instrument The specific desti nations of the two tubes depends upon the function of each tube and upon whether the detector base is located in the A or B detec tor position 34 Disconnect the tubes by removing the tube outlet fitting plate from the manifold block When bending tubing do not make sharp bends which may crimp the tubing 35 Prepare the replacement detector ...

Страница 95: ...stru ment CONNECTING THE HYDROGEN INLET TUBE AT THE WRONG LOCATION ON THE FLOW MANIFOLD BLOCK WILL RESULT IN LEAKAGE CREATING A FIRE AND EXPLOSION HAZARD When installing tubing in the flow manifold block ensure that all o rings are positioned properly 43 Connect the tubes from the new detector weld ment to the flow manifold block The hydrogen tube is painted RED Make sure each tube is installed at...

Страница 96: ...lure to heed this caution may result in damage to the instrument WhenstoringorinbetweenhandlingofPCBs PrintedCircuit Boards alwaysplacethemin static control envelopes or enclosures 53 Install the FID detector PCB by sliding it into its mounting location on the main PCB at the right side of the instrument Installation of the PCB will insert the interconnect into the thermal strap Use caution to avo...

Страница 97: ... side panel and secure using two screws 64 Install the right side panel and secure using four screws 65 Install the electronics carrier top cover 66 Install the hinged top cover and secure using a screw and washer 67 Connect the ground strap to the hinged top cover using a screw 68 Restore all gas supplies 69 Restore power to the instrument IGNITOR DETECTOR PCB INTERCONNECT CLAMPS THERMAL STRAP CO...

Страница 98: ...wer line switch to the off position 2 Disconnect the power cable from its receptacle 3 Allow time for the oven and heated zones to cool 4 When the heated zones are cool turn off all gas supplies 5 Lift the hinged top cover at its front edge exposing the detector area 6 Remove the electronics carrier top cover by grasping it at the rear and lifting upwards until its catch releases then pulling it t...

Страница 99: ...traction lance tool 8710 1542 to remove the interlock ing side covers from the plug The plug is made up of two connectors one is for the to roid bead power the other is for the active con trol element 11 Loosen the screws securing the detector PCB interconnect clamps to the thermal strap DETECTOR COVER COLLECTOR INTERCONNECT CLAMP SCREW TO NPD TRANSFORMER TOP PART OF CONNECTOR TO NPD BEAD POWER CO...

Страница 100: ...e collector inside the collector assembly Do not handle the collector with bare hands Use needle nose pliers when handling the collector to avoid contaminating it with finger oils and or other contaminants 14 Use needle nose pliers inserted through the opening in the top of the detector cover to re move the collector by forcing it down from in side the top of the collector assembly 15 Remove the t...

Страница 101: ...t only the heat shrink tubing not the bare wire contacts the cover 27 Secure the collector assembly to the detector cover using two Pozidriv screws Do not handle the collector with bare hands Use needle nose pliers when handling the collector to avoid contaminating it with finger oils and or other contaminants 28 Use needle node pliers to install the collector into the collector assembly from the ...

Страница 102: ...s always place them in static control envelopes or enclosures 35 Install the NPD detector PCB by aligning the PCB with the guide slots Press the board into its connector on the circuit board NPD power control plugs installed in the wrong position will permanently damage the NPD detector PCB 36 Insert the bead power cable and active element power control cable plug into its connector re ceptacle on...

Страница 103: ...eated zones are cool turn off all gas supplies 5 Lift the hinged top cover at its front edge exposing the detector area 6 Use a Pozidriv screwdriver to remove the three screws securing the detector cover to the ther mal strap 7 Use a 1 5 mm hex wrench to loosen the two set screws which secure the collector inside the collector assembly Do not handle the collector with bare hands Use needle nose pl...

Страница 104: ...tor assembly in accordance with the illustration below 11 When properly aligned secure the collector inside the collector assembly by tightening two set screws 12 Place the detector cover over the detector base and secure it with the three screws previously removed 13 Restore all gas supplies 14 Restore power to the instrument COLLECTOR BODY NOTE POSITION OF COLLECTOR NPD ACTIVE ELEMENT NPD COLLAR...

Страница 105: ...power line switch to the off position 2 Disconnect the power cable from its receptacle 3 Turn off all gas supplies 4 Lift the hinged top cover at its front edge exposing the detector area 5 Remove the electronics carrier top cover 6 Remove the right side panel by removing four screws two each along its top and bottom edges 7 Loosen the screws securing the clamps holding the detector PCB interconne...

Страница 106: ...he column and hardware associated with the detector s liner column liner nuts ferrules makeup gas adapter etc 10 Use a Pozidriv screwdriver to remove the three screws securing the detector cover to the ther mal strap 11 Remove the detector top cover and all at tached components from the thermal strap and set aside 12 Use a 1 4 inch nut driver to remove the jet from the detector weldment 13 Use an ...

Страница 107: ...trol envelopes or enclosures 19 Install the NPD detector PCB by sliding it into its mounting location on the main PCB at the right side of the instrument Installation of the PCB will insert the interconnect into the thermal strap Use caution to avoid damaging the spring at the end of the interconnect 20 Tighten the screws on the clamps which secure the interconnect to the thermal strap 21 Install ...

Страница 108: ...gainst ESD Electro Static Discharge Use a grounded wrist strap part no 9300 0969 large or 9300 0970 small connected to a suitable ground Failure to heed this caution may result in damage to the instrument 5 Disconnect the NPD bead power cable from the detector PCB by pulling it straight off 6 Use the side edge of an AMP pin extraction lance tool 8710 1542 to remove the interlock ing side covers fr...

Страница 109: ...970 small connected to a suitable ground Failure to heed this caution may result in damage to the instrument 14 Install the interlocking side covers on the two connectors which make up the connector to be installed in the NPD detector PCB 15 Insert the plug into its connector on the NPD detector PCB 16 Remove the 1 2 inch nut from the new poten tiometer assembly 17 Install the new potentiometer as...

Страница 110: ... screws around the outside of the brass collar 23 Mount the control knob by pushing it on to the control shaft 24 Install the right side panel and secure using four screws 25 Install the electronics carrier top cover 26 Restore power to the instrument Artisan Scientific Quality Instrumentation Guaranteed 888 88 SOURCE www artisan scientific com ...

Страница 111: ...ies 5 At the bottom of the detector s to be removed inside the column oven remove the column and hardware associated with the detector s liner column liner nuts ferrules makeup gas adapter etc NOTE If an autosampler is installed the injection port cover will not be present 6 Remove the injection port cover by grasping its back edge and lifting it upward 7 Lift the hinged top cover at its front edg...

Страница 112: ...ket by removing the 6 screws securing it to the instrument 13 Remove the two screws securing the left side panel along its bottom edge 14 Slide the left side panel towards the rear of the instrument and lift 15 Remove the electronics carrier top cover above the signal cable plugs and receptacles to expose the top edge of the TCD detector PCB 16 Remove the right side panel by removing four screws t...

Страница 113: ...e the base spanner nut from the detec tor weldment 23 Remove the thermal strap by removing the five screws securing it to the instrument 24 Remove the two screws securing the detector weldment to the instrument 25 Slide the insulation plate out from over the de tector weldment 26 If the detector is to be reused cap the detector weldment at its upper opening using a detec tor cap and at its lower o...

Страница 114: ...ect the tubes by removing the tube outlet fitting plate from the manifold block When bending tubes do not make sharp bends which may crimp the tubing 34 Prepare the replacement detector weldment by bending its tubes until they are oriented similar ly to those on the weldment just removed 35 Position the replacement detector over the opening where it is to be installed 36 Slide the heater and senso...

Страница 115: ...E FLOW MANIFOLD BLOCK WILL RESULT IN LEAKAGE CREATING A FIRE AND EXPLOSION HAZARD When installing tubing in the flow manifold block ensure that all o rings are positioned properly 42 Connect the tubes from the new detector weld ment to the flow manifold block The hydrogen tube fitting is painted RED Make sure each tube is installed at the correct location on the flow manifold block 43 If the PCOC ...

Страница 116: ...d tighten using a spanner wrench part no 19301 00150 46 Remove the cap from the detector weldment top opening 47 Use an inert gas to blow out the detector weld ment cleansing it of any debris 48 Ensure that there is no debris in the detector weldment 49 Install a new jet in the detector weldment Al though installation of a new jet is highly recom mended the old jet may be cleaned and in stalled at...

Страница 117: ...ldment inside the column oven 55 Install the column and any other associated hardware removed in step 5 of this procedure 56 Install the detector top cover and all attached components on the thermal strap 57 Use a Pozidriv screwdriver to secure the detec tor cover to the thermal strap with three screws 58 Restore all gas supplies to the instrument and check for leaks at all installed fittings 59 I...

Страница 118: ...ft is referred to as the 19233A 19235A variety The newer version shown to the right of the 19233A 19235A version is referred to as the G1223A G1224A variety Instructions for disassembly and maintenance are given for both versions of the ECD detector ALL VERSIONS OF ECD DETECTOR WELDMENTS CELLS CONTAIN RADIOACTIVE MATERIAL EXPOSURE TO RADIOACTIVE MATERIAL IS HAZARDOUS TO HUMAN HEALTH UNDER NO CIRCU...

Страница 119: ...es 5 At the bottom of the detector to be removed inside the column oven remove the column and hardware associated with the detector s liner column liner nuts ferrules makeup gas adapter etc 6 Remove the injection port cover by grasping its back edge and lifting it upward 7 Lift the hinged top cover at its front edge exposing the detector area 8 Remove the 1 4 inch screw and washer securing the cov...

Страница 120: ...osen the screws securing the clamps which hold the interconnect in place The following steps require protection against ESD Electro Static Discharge Use a grounded wrist strap part no 9300 0969 large or 9300 0970 small connected to a suitable ground Failure to heed this caution may result in damage to the instrument When storing or in between handling of PCBs Printed Circuit Boards always place th...

Страница 121: ...ully slide the two cartridges heater sensor out of the block The smaller of the two car tridges is the sensor and must be handled gently in order to prevent breakage 30 Remove the heated block 31 Slide heater and sensor cartridges into the new block 32 Install the new heated block in its mounting position 33 Secure the heated block to the instrument using two screws 34 Mount the new weldment makin...

Страница 122: ...e the detector cover to the thermal strap with three screws 44 Remove the cap from the base of the detector inside the column oven 45 Install any hardware removed in step 5 of this procedure liner column liner nuts ferrules makeup gas adapter etc 46 Disconnect any tubing attached to the detector exhaust vent tube 47 Plug the detector exhaust vent tubing 48 Restore supply pressure and check for lea...

Страница 123: ... 5 At the bottom of the detector to be removed inside the column oven remove the column and hardware associated with the detector s liner column liner nuts ferrules makeup gas adapter etc 6 Remove the injection port cover by grasping its back edge and lifting it upward 7 Lift the hinged top cover at its front edge exposing the detector area 8 Remove the 1 4 inch screw and washer securing the cover...

Страница 124: ...from the detec tor 19 Cap the base of the detector inside the column oven to avoid damage or contamination of the detector 20 Remove the two Pozidriv screws securing the detector weldment to the upper and lower heated blocks 21 Remove the weldment and upper heated block from the lower heated block 22 Remove any insulation from around the base of the weldment NOTE Perform steps 23 through 31 only i...

Страница 125: ... anode and install it on the detector 38 Slide the locking tab on the ECD cover forward capturing the cover over the anode shaft of the cell weldment 39 Tighten the locking screw on the ECD cover 40 Connect the cell collector lead from the cell anode to the PCB interconnect 41 Position the detector cover over the detector 42 Secure the detector cover to the instrument with a screw 43 Install any h...

Страница 126: ... gas supplies 5 Lift the hinged top cover at its front edge exposing the detector area 6 Using a Pozidriv screwdriver remove the screw securing the detector top cover to the thermal strap 7 Remove the detector top cover 8 Disconnect the cell anode lead from the PCB interconnect by sliding it off the end of the anode 9 Loosen the locking screw on the ECD cover 10 Slide the locking tab on the ECD co...

Страница 127: ...rrule until it bottoms 20 Tighten the nut and ferrule to secure the anode in place 21 Carefully slide the ECD cover over the anode shaft and anode and install it on the detector 22 Slide the locking tab on the ECD cover forward capturing the cover over the anode shaft of the cell weldment 23 Tighten the locking screw on the ECD cover 24 Connect the cell collector lead from the cell anode to the PC...

Страница 128: ... power line switch to the off position 2 Disconnect the power cable from its receptacle 3 Remove the thumb screw holding the detector cover to the top of the HP 5890 4 Facing the instrument rotate the detector cover to your right until the tab on the bottom left edge of the cover comes free 5 Raise the back of the cover and slide it towards the rear of the instrument OFF ON RED O VISIBLE Artisan S...

Страница 129: ...there is any evidence of chips scratches or cracks in its window surface area A damaged tube must be replaced before continuing to operate the instrument 11 If the PMT is to be replaced carefully remove the PMT from the socket associated with the re sistor network cable assembly in the end cap 12 Dispose of the old tube in a safe manner 13 Carefully remove the new PMT from its packing case and ins...

Страница 130: ...end cap Seat the end cap hand tight 16 Slide the PMT tube assembly onto the detector assembly 17 Secure the resistor network cable assembly to the PMT assembly using a cable tie 18 Secure the PMT assembly to its support bracket using the extension spring 19 Install the FPD cover on the instrument and secure using a thumbscrew 20 Restore power to the instrument Artisan Scientific Quality Instrument...

Страница 131: ...osition 2 Disconnect the power cable from its receptacle 3 Turn off the hydrogen air or oxygen and aux iliary gas supply to the detector by means of the manifold on off valves 4 Allow time for the detector module to cool 5 Remove the thumb screw holding the detector cover to the top of the HP 5890 6 Facing the instrument rotate the detector cover to your right until the tab on the bottom left edge...

Страница 132: ...y evidence of chips scratches or cracks in its surface area 13 Install the cleaned new filter in the flange adapter If the filter is silvered on one side the sil vered side must face toward the flame If the filter has a indicator arrow on its edge the ar row must point towards the PMT 14 Slide the PMT tube assembly onto the detector assembly 15 Secure the PMT assembly to its support bracket using ...

Страница 133: ...he cover comes free 5 Raise the back of the cover and slide it towards the rear of the instrument 6 If an autosampler is installed on the instrument it will be necessary to remove it and its mount ing bracket to allow removal of the left side cover as follows a Remove the autosampler tray from its mounting bracket by first simultaneously lifting and turning the two tray locks which hold it in posi...

Страница 134: ... drip tube from the exhaust tube at the top of the detector 13 Remove the exhaust tube from the detector us ing a 9 16 inch wrench 14 Remove the chimney assembly by removing the two screws securing it to the chimney back 15 Disconnect the ignitor wire lead connector at the mating connection on the detector weld ment by removing the screw which secures it to the glo plug assembly SCREWS SCREWS CHIM...

Страница 135: ...nitor wire lead along its path from the diode bridge assembly to the detector igni tor connector 24 Connect the ignitor wire lead connector to the glo plug on the detector weldment and secure using a screw 25 Install the chimney assembly over the detector weldment and secure using two screws 26 Install the exhaust tube on the detector weldment through the opening in the top of the chim ney and tig...

Страница 136: ... off position 2 Disconnect the power cable from its receptacle 3 Turn off the hydrogen air or oxygen and aux iliary gas supply to the detector by means of the manifold on off valves 4 Allow time for the detector module to cool 5 Remove the thumb screw holding the detector cover to the top of the HP 5890 6 Facing the instrument rotate the detector cover to your right until the tab on the bottom lef...

Страница 137: ... Tip the exposed end of the flange adapter down to prevent loss of the second heat shield win dow and associated o rings and remove it the heat shield window o rings and the flange ring from the detector 14 Remove the four screws and associated lock washers securing the stainless steel coupling clamp heat shield disk first heat shield window and heat shield gasket to the detector weld ment 15 Tip ...

Страница 138: ...e not going to be replaced wipe them clean using a lint free lens tissue Be careful not to scratch the surface of the windows If necessary clean the windows with a solution of soft soap and warm water Rinse with distilled water NOTE During assembly of the detector always use new seals o rings gaskets and discard the old ones 17 Assemble the heat shield gasket new first heat shield window heat shie...

Страница 139: ...cure the PMT assembly to its support bracket using the extension spring 23 Install the FPD cover on the instrument and secure using a thumbscrew 24 Restore power to the instrument Artisan Scientific Quality Instrumentation Guaranteed 888 88 SOURCE www artisan scientific com ...

Страница 140: ...ary nitrogen supplies to the detector at the flow control panel 4 Allow time for the heated zones to cool 5 Remove the thumb screw holding the detector cover to the top of the HP 5890 6 Facing the instrument rotate the detector cover to your right until the tab on the bottom left edge of the cover comes free 7 Raise the back of the cover and slide it towards the rear of the instrument 8 Lift the d...

Страница 141: ...detector 14 Remove the exhaust tube from the detector using a 9 16 inch wrench 15 Remove the chimney assembly by removing the two screws securing it to the chimney back 16 Loosen the three screws which secure the clamp which secure the detector to the chim ney back PMT ASSEMBLY CHIMNEY AND BRACKETRY REMOVED FOR CLARITY SULPHUR FILTER CHIMNEY SCREW CLAMP SECURING SCREWS Artisan Scientific Quality I...

Страница 142: ...RING 0905 1104 FLANGE ADAPTOR FLANGE RING O RING 0905 1103 CLAMP SCREW WELDMENT HEAT SHIELD GASKET 19256 80040 FIRST HEAT SHIELD WINDOW HEAT SHIELD DISK STAINLESS STEEL COUPLING LOCK WASHER SCREW 21 Remove the flange adapter and flange ring by removing the four screws securing them to the stainless steel coupling 22 Remove the second heat shield window and two associated o rings from the stainless...

Страница 143: ... be replaced Also if chipping or breakage occurs use an inert gas to blow any fragments out of the detector weldment and clean the weldment with an approved solvent 26 Remove the heat shield gasket from the detector weldment 27 Clean the detector weldment with an approved solvent 28 Blow out any particles or contaminants using an inert gas 29 If a PCOC fan is installed remove the back cov er of th...

Страница 144: ...e base of the de tector weldment NOTE During assembly of the detector always use new seals o rings gaskets and discard the old ones 38 Install a new heat shield gasket on the detector weldment 39 Install a new first heat shield window 40 Assemble the heat shield disk stainless steel coupling and clamp to the detector weldment and secure using four screws and four lock washers Tighten screws evenly...

Страница 145: ...him ney and tighten using a 9 16 inch wrench 47 Install the drip tube on the exhaust tube 48 Install the o ring for the sulphur filter in the flange adapter 49 Install the sulphur filter in the flange adapter 50 Slide the PMT tube assembly onto the detector assembly 51 Secure the PMT assembly to its support bracket using the extension spring 52 Install the FPD cover on the instrument and secure us...

Страница 146: ...er cable from its receptacle 3 Turn off the hydrogen air or oxygen and aux iliary nitrogen supplies to the detector at the flow control panel 4 Allow time for the heated zones to cool 5 Remove the thumb screw holding the detector cover to the top of the HP 5890 6 Facing the instrument rotate the detector cover to your right until the tab on the bottom left edge of the cover comes free 7 Raise the ...

Страница 147: ...cure the clamp which secure the detector to the chim ney back 15 Use a 9 16 inch wrench to loosen the nut hold ing the weldment exit tube to the jet assembly It will be necessary to hold the jet assembly with a 1 2 inch wrench to prevent rotation 16 Pull the heater and sensor from the detector weldment assembly 17 Carefully lift the detector vertically from the transfer tube so as not to damage th...

Страница 148: ...Vespel by pulling them out of the bottom of the trans fer tube weldment 24 Install a new liner and ferrule by feeding the liner through the o ring at the top of the transfer tube being careful not to damage the o ring The silica liner should extend above the top of the transfer tube approximately 6 7mm NOTE The fused silica liner and ferrule Vespel are combined as Part No 19256 80690 25 Carefully ...

Страница 149: ...tening the nut which secures the weldment with a 9 16 inch wrench 32 Install the chimney assembly and secure using two screws 33 Install the exhaust tube on the detector weldment through the opening in the top of the chim ney and tighten using a 9 16 inch wrench 34 Install the drip tube on the exhaust tube 35 Install the sulphur filter in the flange adapter 36 Slide the PMT tube assembly onto the ...

Страница 150: ...f the hydrogen air or oxygen and aux iliary nitrogen supplies to the detector at the flow control panel 4 Allow time for the heated zones to cool 5 Remove the thumb screw holding the detector cover to the top of the HP 5890 6 Facing the instrument rotate the detector cover to your right until the tab on the bottom left edge of the cover comes free 7 Raise the back of the cover and slide it towards...

Страница 151: ... ney back 15 Use a 9 16 inch wrench to loosen the nut hold ing the weldment exit tube to the jet assembly It will be necessary to hold the jet assembly with a 1 2 inch wrench to prevent rotation 16 Pull the heater and sensor from the detector weldment assembly 17 Carefully lift the detector vertically from the transfer tube so as not to damage the fused silica liner 18 Inside the oven remove the c...

Страница 152: ... Unscrew the transfer tube weldment from the detector base weldment 22 Lift the transfer tube weldment containing the fused silica liner and ferrule vertically off of the base weldment 23 Remove the fused silica liner and ferrule Vespel by pulling them out of the bottom of the trans fer tube weldment 24 Remove the two screws securing the detector base weldment to the instrument 25 Lift the detecto...

Страница 153: ...f the instru ment When installing tubing in the applicable flow control component ensure that all o rings are positioned properly 31 Connect the tube from the new detector base weldment to the flow manifold block The hy drogen tube fitting is painted RED Make sure that the tube is installed at the correct location on the flow manifold block 32 If the PCOC fan and cover were removed in stall them a...

Страница 154: ... the detector weldment 41 Secure the weldment exit tube to the jet assembly with by holding the jet weldment with a 1 2 inch wrench and tightening the nut which secures the weldment with a 9 16 inch wrench 42 Install the chimney assembly and secure using two screws 43 Install the exhaust tube on the detector weldment through the opening in the top of the chim ney and tighten using a 9 16 inch wren...

Страница 155: ... along its top and bottom edges NOTE Noise will appear only about 2 3 as large on analog signal paths than on digital due to the high band pass filtering of signal on analog channels HAZARDOUS VOLTAGES ARE PRESENT IN THE INSTRUMENT WHEN THE POWER CORD IS CONNECTED AVOID A POTENTIALLY DANGEROUS SHOCK HAZARD BY FOLLOWING ALL REQUIRED SAFETY PROCEDURES WHEN WORKING ON THE INSTRUMENT The following ste...

Страница 156: ...erification analysis Reset the voltage and perform another analysis Continue this sequence until the maximum sensitivity is attained greatest area counts for a given amount of sample injected divided by noise 7 Install the right side panel and secure using four screws 8 Install the electronics carrier top cover SIGNAL CABLE HIGH VOLTAGE CABLE HIGH VOLTAGE REFERENCE HIGH VOLTAGE ADJUSTMENT Artisan ...

Страница 157: ... off position 2 Disconnect the power cable from its receptacle 3 Turn off all gas supplies 4 Lift the hinged top cover at its front edge exposing the detector area 5 Remove the electronics carrier top cover 6 Remove the right side panel by removing four screws two each along its top and bottom edges 7 Lift the hinged top cover at its front edge exposing the detector area If an FPD detector is inst...

Страница 158: ...lock on the detector PCB Use a small flat blade screwdriver to press each wire lead release located adjacent to each connection FID Loosen the screws securing the clamps holding the detector PCB interconnect in place NPD a Use a Pozidriv screwdriver to remove the three screws securing the detector cover to the thermal strap b Disconnect the NPD bead power cable from the detector PCB by pulling it ...

Страница 159: ...trap b Remove the detector top cover c Disconnect any tubing attached to the de tector purge and vent tubes d Disconnect the cell anode lead from the PCB interconnect e Loosen the screw securing the detector PCB interconnect clamp to the thermal strap FPD a Disconnect the signal cable from its con nector on the FPD detector PCB b Disconnect the high voltage cable from its connector on the FPD dete...

Страница 160: ...loyed Installation of the PCB will insert the interconnect into the ther mal strap Use caution to avoid damaging the spring at the end of the interconnect 11 In order to install the detector PCB the components which retain the interconnects or other wiring must be tightened installed and or connected as applicable for a particular detector TCD Connect the detector filament and delta t temperature ...

Страница 161: ... in place b Connect the cell collector lead from the PCB interconnect c Install the detector cover and secure using three screws G1223A G1224A ECD a Tighten the screw securing the detector PCB interconnect clamp to the thermal strap s Connect the cell anode lead from the PCB interconnect c Connect any tubing that was previously attached to the detector purge and vent tubes d Install the detector t...

Страница 162: ...e FPD detector PCB 23 Restore all gas supplies to the instrument 24 Install the right side panel and secure using four screws 25 Install the electronics carrier top cover 26 Restore power to the HP 5890 Series II SIGNAL CABLE HIGH VOLTAGE CABLE Artisan Scientific Quality Instrumentation Guaranteed 888 88 SOURCE www artisan scientific com ...

Страница 163: ...s well as individual part replacement in the event that the shroud assembly is not available in a timely manner etc Specific part numbers are not given in this section For all replacement part numbers refer to Section 6 of the IPB portion of this document Oven Assembly This document is not meant to provide instruction for first time installation of the options discussed Add on sheets exist for jus...

Страница 164: ...wer supply PCB 2 If problem persists reinstall original power supply PCB and go to probable cause d 1 Check both fuses d Faulty main PCB PCB 2 Using the same sample and conditions on this and other chromatographs the retention times of this GC differ a Oven needs calibration 1 Calibrate oven per proce dure in this section 3 Oven does not control a Faulty main PCB 1 Replace main PCB 4 Oven temperat...

Страница 165: ...ght side panel by removing four screws two each along its upper and lower edges 7 Remove the two screws securing the left side panel along its bottom edge 8 Slide the left side panel towards the rear of the instrument and lift 9 Remove the four screws securing the rear cover at its upper rear portion 10 Slide the rear cover towards the rear of the instrument 11 Remove columns and other hardware fr...

Страница 166: ...PULLING ON THE WIRES MAY CAUSE BREAKAGE 14 At the rear of the instrument disconnect the two heater element leads at the AC power supply PCB HEATER ELEMENT CONNECTION TERMINALS 15 From inside the oven draw the heater leads through the opening in the rear of the oven Artisan Scientific Quality Instrumentation Guaranteed 888 88 SOURCE www artisan scientific com ...

Страница 167: ...ng to the sensor cartridge of the replacement shroud by adjust ing their locking lances using the lance reset portion of the tool 20 Feed the sensor cartridge pins through the opening in the oven and ready them for installa tion into the main board connector shell 21 Insert the pins for the replacement sensor into their appropriate locations in the plug making sure the locking lance on each pin se...

Страница 168: ...hes anything while turning If so open the shroud and make any necessary adjust ments 28 Replace the panels removed at the beginning of this procedure 29 Install any columns and associated hardware removed at the beginning of this procedure 30 Connect any gas supplies disconnected in step 4 of this procedure TURN OFF THE POWER TO THE INSTRUMENT IMMEDIATELY IF THERE IS EVIDENCE OF THE FAN BLADES CON...

Страница 169: ...off all gas supplies 5 Remove the four screws securing the rear cover to the instrument 6 Slide the rear cover towards the rear of the instrument 7 Remove columns and other hardware from any installed inlets and detectors which pre vents free access to the heater shroud 8 Locate the four screws securing the oven heater fan shroud and the two screws secur ing the heater standoffs 9 Remove the six s...

Страница 170: ...t may be replaced at the same location 11 Loosen the retainer clamp sufficiently to free the sensor HEATER STANDOFFS SENSOR HEATER ELEMENT HEATER ELEMENT AS VIEWED FROM REAR OF SHROUD 12 Remove the two screws securing the heater to its standoffs Artisan Scientific Quality Instrumentation Guaranteed 888 88 SOURCE www artisan scientific com ...

Страница 171: ...ted length and allow it to contract back to an approximate 720 mm length Table 4 1 Preparing Replacement Oven Heater Element INSTRUMENT RESISTANCE UNSTRETCHED STRETCHED CONTRACTED VOLTAGE ohms LENGTH mm LENGTH mm LENGTH mm 120 1 9 05 0 05 136 975 720 220 2 30 42 0 17 180 1110 720 240 3 36 20 0 20 214 1185 720 17 Route the new heater through insulators so that its ends terminate at the connection l...

Страница 172: ...termine if the fan touches anything while turning If so open the shroud and make any necessary adjust ments 23 Install any columns and associated hardware removed at the beginning of this procedure 24 Connect any gas supplies disconnected in step 4 of this procedure 25 Restore power to the instrument 26 Ensure that the oven functions properly at a given temperature e g 100_C Artisan Scientific Qua...

Страница 173: ...right side panel by removing four screws two each along its upper and lower edges 7 Remove the two screws securing the left side panel along its bottom edge 8 Slide the left side panel towards the rear of the instrument and lift 9 Remove the four screws securing the rear cover at its upper rear portion 10 Slide the rear cover towards the rear of the instrument 11 Remove columns and other hardware ...

Страница 174: ...ficiently to free the sensor HEATER STANDOFFS SENSOR HEATER SENSOR AS VIEWED FROM REAR OF SHROUD 16 Withdraw the faulty sensor from the retainer 17 Remove the sensor through the opening in the rear of the oven Some insulation will come out with the sensor 18 Remove any insulation remaining in the sensor guide and save it for later use Artisan Scientific Quality Instrumentation Guaranteed 888 88 SO...

Страница 175: ... PCB 22 Use the lance release tip of an AMP pin extrac tion lance reset tool 8710 1542 to remove the appropriate pins from connector P7 The tool features a lance release tip and a lance reset tip The lance release tip is used to depress the pin locking lance to extract the pin from a connector The lance reset tip positions a lock ing lance to its proper height to ensure reten tion of the pin in th...

Страница 176: ...acle on the main PCB 27 Install the insulation removed earlier in the sensor guide around the sensor wire leads 28 Replace the panels removed at the beginning of this procedure 29 Install any columns and associated hardware removed at the beginning of this procedure 30 Connect any gas supplies disconnected in step 4 of this procedure 31 Restore power to the instrument 32 Ensure that the oven opera...

Страница 177: ...ies 5 Remove the four screws securing the rear cover to the instrument 6 Remove the rear cover by sliding it towards the rear of the instrument 7 Inside the oven remove columns and other hardware preventing free access to the heater 8 Remove the four screws securing the oven heater fan shroud to the instrument 9 Carefully swing the left edge of the shroud towards the front of the instrument 10 Wit...

Страница 178: ...tacle J28 on the AC power board WHEN DISCONNECTING A PLUG PULL ON THE PLUG NOT ON ITS WIRES PULLING ON THE WIRES MAY CAUSE BREAKAGE 14 Disconnect connector J28 from its receptacle by pulling it straight up while squeezing its ribbed sides 15 Locate and remove the fan motor ground wire by removing the nut securing it to the instrument 16 Remove the three nuts and six associated washers securing the...

Страница 179: ...lat portion of the shaft 23 Tighten the setscrew 24 Install the oven heater fan shroud and secure with four screws 25 Feed a screwdriver through a hole in the shroud and gently spin the fan 26 Listen to determine if the fan touches anything while turning 27 If any noise is heard open the shroud and repeat steps 4 through 7 and 18 through 22 adjust ing the position of the fan on the motor shaft 28 ...

Страница 180: ...NG OPERATION AND OR IF THERE IS UNDUE VIBRATION VIBRATION MAY INDICATE BENT FAN BLADES AND OR A BENT MOTOR SHAFT 31 Restore power to the instrument 32 Check that the oven controls properly at some selected temperature e g 100_C Artisan Scientific Quality Instrumentation Guaranteed 888 88 SOURCE www artisan scientific com ...

Страница 181: ...ool turn off all gas supplies 5 Remove the four screws securing the rear cover to the instrument 6 Slide the rear cover towards the rear of the in strument 7 Remove the electronics carrier top cover by grasping it at the rear and lifting upwards until its catch releases then pulling it towards the rear of the instrument 8 Remove the right side panel by removing four screws two each along its upper...

Страница 182: ...uring the flapper bracket to the instru ment 13 Lift the flapper bracket assembly from the instrument 14 Use a hex wrench to loosen the motor shaft setscrew on the flexible coupling closest to the flap motor 15 Use a small Pozidriv screwdriver to remove the motor from the bracket 16 Insert the shaft of the new stepper motor into the flexible coupling on the flapper assembly 17 Secure the motor to ...

Страница 183: ...th used by the old harness and secure it with plastic wire ties OVEN FLAP PINS 1251 5963 SCREW M4 x 8 mm 0515 0910 FLAPPER BUSHING 05890 20730 FLAPPER BRACKET 05890 00440 FLEXIBLE COUPLING 1500 0671 SCREW M3 x 6 mm 0515 0055 STEPPER MOTOR 05890 60940 LOCK WASHER 2190 0468 Artisan Scientific Quality Instrumentation Guaranteed 888 88 SOURCE www artisan scientific com ...

Страница 184: ... PCB The plug is keyed and can only be in serted one way 27 Replace the panels removed at the beginning of this procedure 28 Connect any gas supplies disconnected in step 4 of this procedure 29 Restore power to the instrument SMALL PARTICLES OF DEBRIS MAY BE BLOWN OUT OF THE OVEN WHEN THE FLAP IS OPEN USE PROPER EYE PROTECTION WHEN OBSERVING THE OVEN FLAPS THROUGH THE BACK PANEL TO PREVENT POSSIBL...

Страница 185: ...e electronics carrier top cover by grasping it at the rear and lifting upwards until its catch releases then pulling it towards the rear of the instrument 6 Remove the right side panel by removing four screws two each along its upper and lower edges 7 Remove the two screws securing the left side panel along its bottom edge 8 Slide the left side panel towards the rear of the instrument and lift 9 R...

Страница 186: ...s and as sociated washers from around the edge of its mounting bracket NOZZLE TYPICAL NUT WASHER MOUNTING BRACKET SCREW 17 Withdraw the valve assembly from the side of the instrument being careful not to bend or dam age the nozzle assembly 18 Separate the valve body from its mounting bracket by removing two screws 19 If only the cryogenic nozzle is being replaced proceed as follows a Remove the no...

Страница 187: ...embly or optional manual injection assembly by rotating it counter clockwise Be careful not to loose the septum insert or PCOC insert spring which are installed under the injection assembly AUTO INJECTION ASSEMBLY OPTIONAL MANUAL INJECTION ASSEMBLY DUCKBILL SEPTUM SEPTUM PCOC INSERT SPRING AIR DEFLECTOR WELDMENT INSULATION CAVITY SLEEVE SCREW INSERT HEATER SENSOR CABLE ASSEMBLY 1 4 INCH SCREW AND ...

Страница 188: ...ment using two screws Handle the heater and sensor cartridges with care to prevent breakage The cartridges particularly the smaller sensor cartridge are fragile j Carefully slide the heater and sensor cartridges into the heated block portion of the inlet k Install the air deflector and secure it to the weldment using one screw l Install the injection assembly septum PCOC insert spring and insert t...

Страница 189: ... ensure it is fully bottomed and to ensure the pin lock ing lance is released d Holding the body of the tool firmly in place fully inserted into the plug depress the plunger to eject the pin from the connector e Remove the tool from the plug 25 Insert pins from the new valve into their appropriate locations in the plug making sure the locking lance on each pin seats into the plug 26 Gently pull on...

Страница 190: ... at the beginning of this proce dure 32 Connect any gas supplies disconnected in step 4 of this procedure 33 Restore power to the instrument 34 Check that the oven controls properly at some selected subambient temperature e g 10_C and that no cryogenic fluid flows into the oven at a selected temperature above ambient e g 100_C Artisan Scientific Quality Instrumentation Guaranteed 888 88 SOURCE www...

Страница 191: ...le time up to 1 2 hour for thermal equilibration at the selected temperature No drift should be observed 1 Place the temperature sensing probe in the region of the oven which is occupied by the column s 2 Set the oven temperature to the desired level allowing ample time for thermal equilibration 3 At the keyboard select the CALIB AND TEST MODE function 1 CLEAR 1 ENTER 4 CALIB will be displayed fol...

Страница 192: ...es The HP 5890 Series II also uses an optional cryogenic valve to cool the PCOC inlet While the cryogen ic valve is discussed with oven components in Section 5 of the service portion of this document remov al of the PCOC nozzle which carries the cooling gas from the valve to the inlet is discussed in this sec tion Specific part numbers are not given in this section For replacement part numbers ref...

Страница 193: ...emove Replace ECD 19233A 19235A VERSIONS SVC 6 28 Heater and Sensor Cartridges Remove Replace ECD G1223A G1224A VERSIONS SVC 6 31 Heater and Sensor Cartridges Remove Replace FPD Heater and Sensor Cartridges SVC 6 34 Remove Replace Valve Box Heater and Sensor Cartridges SVC 6 37 Replacing TCD Delta T Temperature Sensor Cartridges SVC 6 39 Remove Replace PCOC Inlet Cryogenic Cooling Cryo Blast Weldm...

Страница 194: ...ed to chassis grounded 1 Replace heater and sensor b Faulty main PCB 1 Replace main PCB refer to Section 9 3 None of the heated zones will heat but the oven is ok a Faulty F3 fuse on main PCB 1 Check main PCB fuse F3 replace if required b Faulty main PCB 1 Replace main PCB refer to Section 9 4 None of the heated zones will heat and the oven will not heat a Faulty main PCB 1 Replace main PCB refer ...

Страница 195: ...e Sensor Wiring on Main PCB HAZARDOUS VOLTAGES ARE PRESENT IN THE INSTRUMENT WHEN THE POWER CORD IS CONNECTED AVOID A POTENTIALLY DANGEROUS SHOCK HAZARD BY DISCONNECTING THE POWER CORD BEFORE WORKING ON THE INSTRUMENT 1 Set the main power line switch to the off position 2 Disconnect the power cable from its receptacle 3 Turn off all gas supplies 4 Remove the four screws securing the rear cover to ...

Страница 196: ... P7 on the main PCB at the upper right corner of the PCB All heater cartridge leads terminate at connector receptacle J9 on the main PCB at the right side of the PCB 9 Route the replacement heater or sensor cartridge leads along the same path 10 Disconnect or cut any plastic cable ties securing the old heater sensor cable assembly along its path 11 Secure the leads of the replacement heater sensor...

Страница 197: ...ltage cover from the upper right portion of the main PCB 14 Disconnect connector J9 from its receptacle by squeezing its ribbed size and pulling the plug straight out of the receptacle 15 An AMP pin extraction tool 8710 0614 is re quired to properly remove pins from connector J9 The tool features a sleeve to release the pin locking lance and a plunger to eject the pin from the plug The following s...

Страница 198: ...nto the plug 17 Gently pull on the wire to ensure it is locked in the plug 18 Insert the plug into the J9 receptacle 19 Replace the high voltage cover on the right side of the main PCB 20 Insert connector P10 into its receptacle on the main PCB When disconnecting a plug pull on the plug not on its wires Pulling on the wires may cause breakage 21 Disconnect connector P7 from its receptacle by pulli...

Страница 199: ...ug making sure the locking lance on each pin seats into its hole through the side of the plug 25 Gently pull on the wire to ensure that the pin is locked in the connector 26 Insert connector P7 into its corresponding receptacle on the main PCB 27 After the leads have been exchanged in the appropriate connectors proceed to the heater sen sor cable assembly removal replacement procedure applicable t...

Страница 200: ...ase of the inlet 4 Remove the injection port cover by grasping its back edge and lifting it upward 5 Remove any insulation from around the top of the inlet 6 Use a Pozidriv screwdriver to remove the two screws securing the inlet and insulation plate to the instrument Depending on the age of the instrument the insulation plate may be flat as shown at the left or may be a box as shown below 7 Lift t...

Страница 201: ...h two Pozidriv screws 13 Replace any insulation that was removed from around the inlet 14 Remove the cap plug from the end of the inlet 15 Install the liner and all other hardware removed during step 2 16 Restore the supply gas pressure 17 Install the injection port cover 18 Install the right side panel and secure using two screws 19 Install the electronics carrier top cover 20 Slide the rear cove...

Страница 202: ...ward 5 Remove the two screws in the top of the inlet top cover these screws secure the inlet base weldment to the inlet top cover 6 Use a Pozidriv screwdriver to remove the two screws securing the top cover to the instrument 7 Lift the inlet top cover off of the inlet 8 Remove any insulation from around the top of the inlet 9 Lift the inlet enough to expose the heated block and heater sensor wirin...

Страница 203: ...instrument using two screws 17 Remove the cap plug from the end of the inlet 18 Install the column and associated hardware removed in step 2 19 Install the right side panel and secure using two screws 20 Install the electronics carrier top cover 21 Slide the rear cover onto the instrument 22 Secure the rear cover to the instrument by installing and tightening four screws 23 Install the injection p...

Страница 204: ...ove the insert assembly from the shell weldment using a inch wrench 6 Detach and remove the tubing nut from the fit ting on the shell weldment 7 Loosen the two screws securing the insulation cover inside the column oven 8 Rotate the cover freeing it from its securing hardware and remove the cover and three pieces of lower insulation 9 Remove the reducing nut flat washer and anealed seal using a 1 ...

Страница 205: ...thin the cavity provided in the shell weldment 20 Carefully install the inlet securing it to the in strument with two Pozidriv screws NOTE To lessen the possibility of pressure leaks always install a new anealed seal when the old seal has been removed 21 Tighten the retaining nut at the base of the shell weldment 22 Install the reducing nut flat washer and anealed seal onto the base of the retaini...

Страница 206: ...the inlet 34 Install the column and associated hardware removed in step 2 35 Install the right side panel and secure using two screws 36 Install the electronics carrier top cover 37 Slide the rear cover on to the instrument 38 Secure the rear cover to the instrument by installing and tightening four screws 39 Install the injection port cover 40 Restore power to the HP 5890 Series II Artisan Scient...

Страница 207: ...two screws securing the left side panel along its bottom edge 5 Cap the base of the inlet inside the column oven 6 Remove the auto injection assembly or op tional manual injection assembly by rotating it counter clockwise Be careful not to loose the septum insert or PCOC insert spring which are installed under the injection assembly AUTO INJECTION ASSEMBLY OPTIONAL MANUAL INJECTION ASSEMBLY DUCKBI...

Страница 208: ...ing one screw 11 Install the injection assembly septum PCOC insert spring and insert the injection assembly secures the other items to the inlet weldment 12 Remove the cap plug from the end of the inlet 13 Install the liner and all other hardware removed in step 2 14 Restore the supply gas pressure 15 Install the right side panel and secure using two screws 16 Install the electronics carrier top c...

Страница 209: ...e detector base 4 Lift the hinged top cover at its front edge exposing the detector area 5 Remove the TCD detector cover by removing two screws one from each side of the detector cover 6 Cap the TCD vent port on the top of the detector This is not be required on a series con nected TCD 7 Remove the preformed thermal insulation from around the detector to expose the two screws securing the detector...

Страница 210: ...uring it to the instrument with two screws 13 Remove the caps from the detector base and the vent port When installing insulation usecare not to plug the vent port If flow is interrupted while the TCD is on it will shorten its life dramatically 14 Taking care not to block the vent port install insulation around the detector block Use caution not to crimp the filament and delta t sensorleads when i...

Страница 211: ...alled the injection port cover will not be present 3 Remove the injection port cover by grasping its back edge and lifting it upward 4 Lift the hinged top cover at its front edge exposing the detector area 5 Remove the screw securing the ground strap to the hinged top cover 6 Remove the 1 4 inch screw and washer securing the cover at its right side hinge point 7 At the lower right edge of the cove...

Страница 212: ...he collector mount to the thermal strap 13 Remove the collector mount and collector assembly as a unit 14 Use a 1 and 1 4 inch socket to remove the base spanner nut from the detector weldment 15 Remove the thermal strap by removing the five screws securing it to the instrument 16 Remove the two screws securing the detector weldment to the instrument 17 Slide the insulation plate out from over the ...

Страница 213: ...ing steps require protection against ESD Electro Static Discharge Use a grounded wrist strap part no 9300 0969 large or 9300 0970 small connected to a suitable ground Failure to heed this caution may result in damage to the instrument When handling PCBs Printed Circuit Boards always place them in static control envelopes 31 Install the FID detector PCB by sliding it into its mounting location on t...

Страница 214: ...re the rear cover to the instrument by installing and tightening four screws 42 Install the right side panel and secure using four screws 43 Install the electronics carrier top cover 44 Install the hinged top cover and secure using a screw and washer 45 Connect the ground strap to the hinged top cover using a screw 46 Restore all gas supplies 47 Restore power to the instrument IGNITOR DETECTOR PCB...

Страница 215: ...e injection port cover by grasping its back edge and lifting it upward 4 Lift the hinged top cover at its front edge exposing the detector area 5 Remove the 1 4 inch screw and washer securing the cover at its right side hinge point 6 Remove the ground strap from the hinged top cover by removing a screw 7 At the lower right edge of the cover press from right to left until the right side hinge relea...

Страница 216: ...the base spanner nut from the detec tor weldment 14 Remove the thermal strap by removing the five screws securing it to the instrument 15 Cap the weldment openings at the top over the jet aperture and bottom inside the column oven to prevent damage and or contamination 16 Remove the two screws securing the detector weldment to the instrument 17 Slide the insulation plate out from over the detector...

Страница 217: ...sing a spanner wrench part no 19301 00150 The following steps require protection against ESD Electro Static Discharge Use a grounded wrist strap part no 9300 0969 large or 9300 0970 small connected to a suitable ground Failure to heed this caution may result in damage to the instrument When handling PCBs Printed Circuit Boards always place them in static control envelopes 30 Install the NPD detect...

Страница 218: ... procedure 36 Use a Pozidriv screwdriver to secure the detector cover to the thermal strap with three screws 37 Install the rear panel and secure using four screws 38 Install the right side panel and secure using four screws 39 Install the electronics carrier top cover 40 Install the hinged top cover and secure using a screw and washer 41 Connect the ground strap to the hinged top cover using a sc...

Страница 219: ...ck edge and lifting it upward 4 Lift the hinged top cover at its front edge exposing the detector area 5 Remove the 1 4 inch screw and washer securing the cover at its right side hinge point 6 At the lower right edge of the cover press from right to left until the right side hinge releases 7 Remove the screw securing the ground strap to the hinged top cover 8 With the lower right side of the cover...

Страница 220: ...ea along its outer edge and pulling it straight out This will draw the interconnect out of the detec tor clamps on the thermal strap 15 Remove the five screws securing the thermal strap and shield to the instrument 16 Remove the shield from the thermal strap by carefully working it over the collector lead and exhaust vent tube Depending on the detec tor s location it may be necessary to bend the s...

Страница 221: ...lure to heed this caution may result in damage to the instrument When handling PCBs Printed Circuit Boards always place them in static control envelopes 36 Install the detector PCB at the right side of the instrument This will feed the interconnect in to the detector clamps on the thermal strap 39 Tighten the screws securing the clamps which hold the interconnect in place 40 Connect the cell colle...

Страница 222: ...ck edge and lifting it upward 4 Lift the hinged top cover at its front edge exposing the detector area 5 Remove the 1 4 inch screw and washer securing the cover at its right side hinge point 6 At the lower right edge of the cover press from right to left until the right side hinge releases 7 Remove the screw securing the ground strap to the hinged top cover 8 With the lower right side of the cover...

Страница 223: ...nt to the upper and lower heated blocks 18 Remove the weldment and upper heated block from the lower heated block 19 Remove any insulation from around the base of the weldment NOTE Perform steps 23 through 31 only if it is desired to remove the ECD heated block Otherwise proceed to step 32 20 If required remove the two Pozidriv screws se curing the heated block to the instrument 21 Lift the heated...

Страница 224: ...b on the ECD cover forward capturing the cover over the anode shaft of the cell weldment 33 Tighten the locking screw on the ECD cover 34 Connect the cell collector lead from the cell anode to the PCB interconnect 35 Position the detector cover over the detector 36 Secure the detector cover to the instrument with a screw 37 Install any hardware removed in step 2 of this procedure liner column line...

Страница 225: ...tate the detector cover to your right until the tab on the bottom left edge of the cover comes free 4 Raise the back of the cover and slide it towards the rear of the instrument 5 Lift the detector top cover to expose the FPD detector weldment 6 Release the extension spring securing the PMT assembly to its support bracket 7 Remove the photomultiplier tube PMT assem bly and sulphur filter from the ...

Страница 226: ...be so as not to damage the fused silica liner Handle the heater and sensor cartridges with care to prevent breakage The cartridges particularly the smaller sensor cartridge are fragile 15 Remove the second heater cartridge from the lower heater block 16 Install the replacement heater cartridge in the lower heater block 17 Install the assembled detector weldment as sembly vertically onto the transf...

Страница 227: ...e PMT tube assembly onto the detector assembly 25 Secure the PMT assembly to its support bracket using the extension spring 26 Install the FPD cover on the instrument and secure using a thumbscrew 27 Install the rear cover and secure using four screws 28 Install the right side panel and secure using four screws 29 Install the electronics carrier top cover 30 Restore all gas supplies 31 Restore pow...

Страница 228: ... 8 Pull any securing tape from around the heater and temperature sensor cables 9 Remove the heater and sensor cartridge s from the valve block s 10 Install the replacement heater and or sensor cartridges into the valve block s 11 Replace the securing tape around the replace ment heater and sensor cartridges 12 Secure the valve box to the instrument using the two standoffs previously removed 13 Sec...

Страница 229: ... 38 18 Install the electronics carrier top cover 19 Restore all gas supplies 20 Restore power to the instrument Artisan Scientific Quality Instrumentation Guaranteed 888 88 SOURCE www artisan scientific com ...

Страница 230: ...5 At the bottom of the detector s to be removed inside the column oven remove the column and hardware associated with the detector s liner column liner nuts ferrules makeup gas adapter etc 6 If the detector is not going to be replaced with a new detector cap the detector base 7 Lift the hinged top cover at its front edge exposing the detector area 8 Remove the TCD detector cover by removing two sc...

Страница 231: ...from the TCD oven re turn exhaust vent port 14 Remove the two screws securing the detector to the instrument and then lift the block up enough to expose the heater and sensor car tridge wires 15 Carefully slide the three cartridges out of the block The two smaller cartridges are the sen sors and must be handled gently in order to prevent breakage 20 Install the heater temperature sensor and replac...

Страница 232: ...r base and the vent port When installing insulation use care not to plug the vent port If flow is interrupted while the TCD is on it will shorten its life dramatically 27 Taking care not to block the vent port install insulation around the detector block 28 Install the electronics carrier top cover Use caution not to crimp the filament and delta t sensor leads when installing the TCD detector cove...

Страница 233: ...ones to cool 4 When the heated zones are cool turn off all gas supplies 5 At the bottom of the inlet s to be removed in side the column oven remove the column and hardware associated with the inlet s liner column liner nuts ferrules makeup gas adapt er etc 6 Remove the injection port cover by grasping its back edge and lifting it upward 7 Remove the two screws securing the left side panel along it...

Страница 234: ...BILL SEPTUM SEPTUM PCOC INSERT SPRING AIR DEFLECTOR WELDMENT INSULATION CAVITY SLEEVE SCREW INSERT HEATER SENSOR CABLE ASSEMBLY 13 Remove the air deflector using a Pozidriv screwdriver to remove the screw securing the air de flector to the inlet weldment 14 Use a Pozidriv screwdriver to remove the two screws securing the inlet to the instrument 15 Lift the inlet enough to expose the heated block 1...

Страница 235: ...eflector and secure it to the weldment using one screw 28 Install the liner and all other hardware except the column removed in step 5 29 Restore the supply gas pressure 30 Check for leaks at all of the newly mated fittings 31 Turn off the supply gas 32 Remove the cap plug from the end of the inlet 33 Install the column and associated hardware removed in step 5 34 Install the left side panel and s...

Страница 236: ...200O 150O 250O TEMPERATURE SENSOR RESISTANCE VS TEMPERATURE TEMPERATURE SENSOR DATA To figure the approximate resistance of a temperature sensor use the following equation R 100O 35 t O Artisan Scientific Quality Instrumentation Guaranteed 888 88 SOURCE www artisan scientific com ...

Страница 237: ... options dis cussed The add on sheets which accompany the various options exist for just this purpose and should be referenced when performing a first time installation TABLE OF CONTENTS VALVES SVC 7 1 INTRODUCTION SVC 7 2 VALCO VALVES 18900F SVC 7 2 General Purpose Valves GPVs SVC 7 4 Adjustable Restrictors SVC 7 5 Gas Sample Loops SVC 7 5 LIQUID SAMPLE VALVES LSVs SVC 7 6 Troubleshooting and Mai...

Страница 238: ...id or gas sample 4 Contaminating the system with samples noneluting materials or poor quality support gases VALCO VALVES 18900F Basically valves are composed of four assemblies a driver valve body rotor and preload assembly P Right Stop Left Stop Port 4 Port 1 Rotor Type Ident Letter Port 5 Port 6 Mounting Hole Port 2 Port 3 Mounting Hole The valve body is made of Nitronic 60 This is a high chromi...

Страница 239: ...ill prevent leakage around the rotor and between nonselected ports The rotor assembly is an integral molded and machined conical hub necessary for proper seating The sample will contact either Teflon low temperature or polyimide high temperature as well as the stainless steel of the valve The rotor fits precisely into the body and nests in the conical seat It is held in place by a preload assembly...

Страница 240: ...types in the same system HP offers only the 6 10 port GSV s and the 4 port LSV 1 16 inch Teflon rotor valves 0 to 175 degrees C 1 16 inch polyimide rotor valves 100 to 350 degrees C Adjustable restrictor valves ambient to 225 degrees C Liquid Sample Valves see Liquid Sample Valves this section The HP 5890 Series II was designed to accept valves heated in their own compartments because valves opera...

Страница 241: ...ves 1 6 5 4 3 2 1 6 5 4 3 2 Adjustable Restrictors This restrictors are not designed for temperatures greater than 225 degrees C Gas Sample Loops A 0 25cc sample loop is included with all valve systems configured for gas sampling 10cc and 5cc loops occupy one valve position limiting the number of valves that can be housed in a valve compartment Artisan Scientific Quality Instrumentation Guaranteed...

Страница 242: ...mple valves have 1 16 inch fittings and are classified by the sample size of the installed rotor 0 2mL 0 5mL or 1mL capacity The two types of valves available are standard or low pressure 1000 psig and high pressure 5000 psig in the four port single purpose liquid sampling valve Whenever a liquid sample valve is used an adjustable restrictor is employed on the sample outlet line to maintain intern...

Страница 243: ...salignments cause most problems Check that adequate air about 482 kPa or 70 psi is supplied Check if the valve is rotating at all If the valve rotates check for proper alignment of the actuator or mechanical binding or slippage of connect ing parts Check for blocked flow paths with valve in both positions BASELINE UPSETS Frequently baseline upsets may be seen on chromatograms when valves are switc...

Страница 244: ...ssarily isolate the leak one of the leak check methods may be needed to locate the leak specifically Note that each valve in a system has two flow paths ON and OFF A leak sometimes occurs in only one of these two positions Check both To do so perform the following 1 Disconnect the detector from the valve system 2 Cap the valve system at its outlet and pressurize to 689 kPa 100 psi Allow 2 to 5 min...

Страница 245: ...85 ________________________________________________________________ Liquid Sampling Valves ________________________________________________________________ Ports Volume Pressure Valve 4 0 2ul 1000 0101 0636 4 0 5ul 1000 0101 0637 4 1 0ul 1000 0101 0638 4 0 5ul 5000 0101 0639 ________________________________________________________________ The body assembly and its component parts are made from Nit...

Страница 246: ... prevents rotation beyond either stop of the index lip Valve ports are connected by the grooves only when the index pin is close to or against either stop of the index lip Any intermediate position results in shutoff of flow through the valve and possible valve damage if left in this position General Purpose Valves GPVs The standard general purpose valves have 1 16 inch zero dead volume fittings T...

Страница 247: ...this adjust able restrictor is NOT compatible with high temperature valves Gas Sample Loops A 1 0cc sample loop is included with all valve systems configured for gas sampling 10 0cc and 5 0cc loops occupy one valve position limiting the number of valves that can be housed in a valve compart ment Six port General Purpose Configurations Liquid sampling valves are designed for use with liquefied gase...

Страница 248: ...__________ High Pressure Standard Pressure _________________________________________________________________________ Temperature Range From To From To Ambient 80_C Ambient 100_C Ambient 150_C Ambient 175_C _________________________________________________________________________ LSV Pressure Range _________________________________________________________________________ High Pressure Standard Pres...

Страница 249: ...rotate or one that ro tates improperly Other than obvious component failures i e solenoid actuator etc generally im proper adjustments and misalignments cause most problems D Check that adequate air about 482 kPa or 70 psi is supplied D Check the valve Is it rotating D If the valve rotates check for proper alignment of the actuator mechanical binding or slippage of connecting parts D Check for blo...

Страница 250: ...in the flow path Since this method does not necessarily isolate the leak other leak check methods may be needed to locate the leak specifically Note Each valve in a system has two flow paths ON and OFF A leak sometimes occurs in only one of these two positions Check both 1 Disconnect the detector from the valve system 2 Cap the valve system at its outlet and pressurize to 689 kPa 100 psi Allow 2 t...

Страница 251: ...s are present remove their mounting hardware in the following order two M4 screws hex nut and mounting bracket for each restrictor valve 8 Remove two valve box top assembly mounting screws one located near the left front corner and one along the right side edge near the middle Lift the valve box top assembly straight off the valve box Be careful not to move the valve rotor index pin from its at re...

Страница 252: ... install the screws The quick release pin should be installed in the 90 degree position for the 6 port valves and in the 60 degree position for the 10 port valves 5 Gently rotate and push the coupling shaft assembly with a blade type screwdriver until the slot on the coupling fully engages the valve rotor index pin Repeat this procedure for each valve installed 6 Make sure that all solenoid valves...

Страница 253: ...ver it is desirable via keyboard entry or more conveniently the valves can be switched ON once and OFF once during a run via the HP 5890 s timed events table NOTE If the valve is already in the position where a command instructs it to switch no action will occur The designated channels A or B are determined solely by the wiring connections to the valve box Artisan Scientific Quality Instrumentatio...

Страница 254: ...ure drop e g to balance flow Arrows indicate the direct ion of flow Loops have a spe cified volume 5 Jumper volume is not specified Fixed restrictors cannot be adjusted Union Fit ting Column 6 3 2 5 4 1 6 3 2 5 4 1 Artisan Scientific Quality Instrumentation Guaranteed 888 88 SOURCE www artisan scientific com ...

Страница 255: ...6 5 4 3 2 Column 2 Column 1 Detector or Valve Carrier Adj Restr Custom Plumbing Diagram Required Option 200 or 230 Gas Sampling Option Option 201 or 231 Column Isolation Option 202 or 232 Temperature limited to 235 C by micrometering needle valve Artisan Scientific Quality Instrumentation Guaranteed 888 88 SOURCE www artisan scientific com ...

Страница 256: ... 4 3 2 1 6 5 4 3 2 OFF ON 1 6 5 4 3 2 1st Carrier 2nd Carrier Vent Detector Column Precolumn Two Stream Selection Requires Gas Sampling Option 203 or 233 Backflush to Detector Option 204 or 234 Backflush a Precolumn to Vent Option 205 or 235 Artisan Scientific Quality Instrumentation Guaranteed 888 88 SOURCE www artisan scientific com ...

Страница 257: ... Detector Column 2 Column 1 1 6 5 4 3 2 OFF ON 1 6 5 4 3 2 Carrier Detector Column 2 Column 1 Column Selection Unused Column Isolated Option 206 or 236 Sequence Reverse Option 207 or 237 Sequence Reverse with Backflush of Column 1 Option 208 or 238 Artisan Scientific Quality Instrumentation Guaranteed 888 88 SOURCE www artisan scientific com ...

Страница 258: ...rier Loop 1 2 3 4 5 6 7 8 9 10 1 2 3 4 5 6 7 8 9 10 OFF ON Detector or 2nd Valve Carrier Column Sample In Out Loop Custom Plumbing Diagram Required Option 400 or 430 Gas Sampling with Backflush of Precolumn to Vent Option 401 or 431 Gas Sampling with Backflush to Detector Option 402 or 432 Artisan Scientific Quality Instrumentation Guaranteed 888 88 SOURCE www artisan scientific com ...

Страница 259: ...Out Column 1 Loop OFF ON 1 2 3 4 8 9 10 1 2 3 4 5 6 7 8 9 10 Carrier Column 2 Sample In Out Column 1 Loop Detector or 2nd Valve 5 6 7 Gas Sampling of Alternate Streams Option 403 or 433 Gas Sampling with Sequence Reverse Option 404 or 434 Gas Sampling with Sequence Reverse and Backflush of Column 1 Option 405 or 435 Artisan Scientific Quality Instrumentation Guaranteed 888 88 SOURCE www artisan sc...

Страница 260: ...S P C Carrier 1 6 5 4 3 2 Column 2 Detector Adj Restr OFF Carrier 1 6 5 4 3 2 Sample In Out OFF Column 1 Loop Column Selection with Backflush to Vent Option 406 or 436 Liquid Sampling Options 151 152 153 and 162 Gas Sample and Column Isolation Option 601 Artisan Scientific Quality Instrumentation Guaranteed 888 88 SOURCE www artisan scientific com ...

Страница 261: ...OFF Carrier Column 1 Sample In Out Loop 1 6 5 4 3 2 Column 2 Detector Adj Restr OFF Gas Sample Backflush and Column Isolation Option 602 Artisan Scientific Quality Instrumentation Guaranteed 888 88 SOURCE www artisan scientific com ...

Страница 262: ...s associated with the keyboard and display components Current maintenance philosophy suggests that the display PCB assembly be replaced as a unit rather then replacing the display PCB keyboard connector element etc individually Maintenance proce dures have been included to allow for the disassembly of the display PCB assembly in the event that the shroud assembly is not available in a timely manne...

Страница 263: ...ators are out re place display PCB 4 If problem persists remove replaced display PCB 6 Go to probable cause b 5 Install original display PCB assembly c Faulty main PCB 1 Replace main PCB b Faulty display PCB ribbon cable 1 Replace display PCB rib bon cable 2 If problem persists go to probable cause c 3 No keyboard control of instrument a Keyboard locked 1 Press clear dot minus enter and set the lo...

Страница 264: ...nd lower edges This procedure requires precautions against ESD Electro Static Discharge Use a grounded wrist strap part no 9300 0969 large or 9300 0970 small connected to a suitable ground Failure to heed this caution may result in damage to the instrument 5 Free the keyboard connector J1 from connector receptacle P1 on the main PCB by releasing the locking tabs one on either side of the connector...

Страница 265: ...PCB assembly forward away from the front of the instrument 9 Remove the display PCB assembly from the instrument NOTE The display PCB assembly may be replaced as a unit or the individual pieces which make it up may be ordered If the entire display PCB assembly is to be replaced go to step 15 10 Remove the four screws securing the display PCB to the keyboard bezel 11 Remove the display PCB from the...

Страница 266: ...and secure using four screws 20 Install the electronics carrier top cover 21 Restore all gas supplies 22 Restore power to the instrument 23 Observe the alphanu meric display as the in strument performs an internal self diagnostic integrity check to en sure that the instrument shows the expected normal displays OVEN STATUS RUN NOT READY FINAL TIME RATE INITIAL TIME OVEN STATUS RUN NOT READY FINAL T...

Страница 267: ...not given in this section For replacement part numbers refer to the Section 9 of the IPB Electronics TABLE OF CONTENTS MAIN PCB SVC 9 1 Replace Main PCB SVC 9 2 Artisan Scientific Quality Instrumentation Guaranteed 888 88 SOURCE www artisan scientific com ...

Страница 268: ...NG ANY FLOW COMPONENTS 1 Set the main power line switch to the off position 2 Disconnect the power cable from its receptacle 3 Allow time for the oven and heated zones to cool 4 When the heated zones are cool turn off all gas supplies 5 Remove the electronics carrier top cover 6 Remove the right side panel by removing four screws two each along its top and bottom edges OFF ON RED O VISIBLE ELECTRO...

Страница 269: ...ge Use a grounded wrist strap part no 9300 0969 large or 9300 0970 small connected to a suitable ground Failure to heed this caution may result in damage to the instrument When storing or in between handling of PCBs Printed Circuit Boards always place them in static control envelopes or enclosures Artisan Scientific Quality Instrumentation Guaranteed 888 88 SOURCE www artisan scientific com ...

Страница 270: ...moval and installation of detector PCBs Refer to section 10 of this manual for information on removal and installation of Communications interface PCBs Refer to section 3 of this manual for information on removal and installation of the EPC MPC interface PCB PRESSURE CONTROL PCB TYPICAL DETECTOR PCB TYPICAL COMMUNICATIONS PCB TYPICAL Artisan Scientific Quality Instrumentation Guaranteed 888 88 SOU...

Страница 271: ...ach end of the plug these must be released to free the plug for removal Also note that J10 plug is released by squeezing its ribbed sides while pulling P1 P2 P3 P4 P5 P6 P7 P8 P9 J14 P11 P10 P12 P13 10 Remove the high voltage cover covering the triac components HIGH VOLTAGE COVER 11 Disconnect connector from receptacle J9 by squeezing its ribbed sides while pulling it straight out Artisan Scientif...

Страница 272: ...eft or right as needed to align it with locater posts and holes for mounting screws 16 Secure the board in place with the seven mounting screws Make sure the longest screw is installed in the hole marked MAIN GND at the top of the board 17 Install all connectors detector PCBs communications interface PCB if present EPC MPC in terface PCB if present and signal cables 18 Restore all gas supplies to ...

Страница 273: ...ITIAL TIME OVEN STATUS RUN NOT READY FINAL TIME RATE INITIAL TIME OVEN STATUS RUN NOT READY FINAL TIME RATE INITIAL TIME ACTUAL SETPOINT ACTUAL ACTUAL ACTUAL SETPOINT SETPOINT SETPOINT Test of display elements all alphanumeric and LED ele ments are lit 5890A memory test in progress 5890A Self testing in progress LEDs off except possibly NOT READY Message indicating normal termination of diagnostic...

Страница 274: ...or first time installation of any of the options dis cussed The add on sheets which accompany the various options exist for just this purpose and should be referenced when performing a first time installation TABLE OF CONTENTS COMMUNICATION INTERFACE COMPONENTS SVC 10 1 Replace Communications Interface PCB SVC 10 2 Replace Rear Panel Connector PCB and or Cable for DICE PCB SVC 10 5 INET CONFIGURAT...

Страница 275: ...e panel by removing four screws two each along its upper and lower edges This procedure requires precautions against ESD Electro Static Discharge Use a grounded wrist strap part no 9300 0969 large or 9300 0970 small connected to a suitable ground Failure to heed this caution may result in damage to the instrument NOTE Depending upon the type of communications PCB installed there may be one or more...

Страница 276: ...he RS 232 C port of the connected device Remove the 12 pin connector from the com munications PCB The cable is installed through the opening where the INET cables are usual ly connected 10 If an analog input communications PCB in installed remove the cable connected to at the top of the PCB 11 Remove the communications PCB by grasping it in the center area along its right edge and pulling it from ...

Страница 277: ...NOT READY FINAL TIME RATE INITIAL TIME OVEN STATUS RUN NOT READY FINAL TIME RATE INITIAL TIME OVEN STATUS RUN NOT READY FI NAL TIME RATE INITIAL TIME OVEN STATUS RUN NOT READY FINAL TIME RATE INITIAL TIME ACTUAL SETPOINT ACTUAL ACTUAL ACTUAL SETPOINT SETPOINT SETPOINT Test of display elements all alphanumeric and LED elements are lit 5890 Series II memory test in progress 5890A Self testing in pro...

Страница 278: ...ifting upwards until its catch releases then pulling it towards the rear of the instrument 6 If the rear panel connector PCB ribbon cable is to be replaced remove the right side panel by removing four screws two each along its upper and lower edges 7 Remove the four screws securing the rear pan el to the instrument 8 If the rear panel connector PCB is to be re placed remove the three screws securi...

Страница 279: ... 13 If the ribbon cable is to be replaced slide the old ribbon cable out of the opening in the elec tronics carrier 14 If the ribbon cable is being replaced slide the new ribbon cable into the opening in the elec tronics carrier 15 If the ribbon cable is being replaced install the new ribbon cable into the connector receptacle on the communications PCB When the con nector is properly seated the lo...

Страница 280: ...INAL TIME RATE INITIAL TIME OVEN STATUS RUN NOT READY FINAL TIME RATE INITIAL TIME OVEN STATUS RUN NOT READY FI NAL TIME RATE INITIAL TIME OVEN STATUS RUN NOT READY FINAL TIME RATE INITIAL TIME ACTUAL SETPOINT ACTUAL ACTUAL ACTUAL SETPOINT SETPOINT SETPOINT Test of display elements all alphanumeric and LED elements are lit 5890 Series II memory test in progress 5890A Self testing in progress LEDs ...

Страница 281: ...O B A L A D D R 1 i 3 1 i 1 3 1 A D D R L O C A L 3174 Figure 13 4 CONFIGURE NETWORK Displays Figure 13 4 shows displays resulting from the key sequence CLEAR 3 ENTER Switching Between Global and Local With regard to the INET function at the HP 5890A there are two operating modes global or local In global mode default mode HP 5890A START and STOP keys when pressed affect other devices on the INET ...

Страница 282: ... has two states if GLOBAL flashes default mode when displayed the HP 5890A is in global mode but NOT configured into the INET system When the HP 5890A is properly configured into the INET system GLOBAL is displayed continuously This feature provides a convenient diagnostic to determine if system configuration has occurred at least as far as the HP 5890A is concerned INET HP IL Addresses Figure 13 ...

Страница 283: ...receptacle on the controller device the controller is always defined as 0 A 2 indicates the HP 5890A is the second device on the loop etc to a maximum value of 31 If cabling is altered or if one or more devices are powered off and then on again automatic loop configuration initiated by the controller updates the displayed value accordingly SETTING THE DEFAULT HP IL ADDRESS Remaining displays in Fi...

Страница 284: ...nel is considered inactive no data from this signal channel is transmitted to other devices on the loop OFF has the same meaning here as shown in the HP 5890A portion of the INET configuration table in the HP 3392A work file listing It is important to note that ON or OFF in this context are strictly INET definitions defined at the system controller They do not for example bear any relationship to ...

Страница 285: ...nd disconnect it at the next device on the INET loop 3 Connect this free cable to both IN and OUT INSTRUMENT NETWORK receptacles on the HP 5890A 4 Enter the following key sequence CLEAR 7 ENTER Upon pressing ENTER the test is performed the HP 5890A both sends and verifies a diagnostic message to itself through the connected cable Each press of ENTER repeats the test Each test requires about one se...

Страница 286: ...ronic Troubleshooting for more information The LOOPBACK TEST may be used to check for continuity in an INET cable an open cable causes test failure Verify that the cable is at fault rather than the HP 5890A by testing a second cable If an intermittent cable problem is suspected the test may be re peated as necessary while flexing the cable particularly at its plugs An ohmmeter should also be used ...

Страница 287: ...IPB portion of this document Oven Assembly This document is not meant to provide instruction for first time installation of the different power supply options discussed Add on sheets exist for just this purpose and should be referenced when per forming a first time installation TABLE OF CONTENTS REPLACING POWER SUPPLY COMPONENTS SVC 11 1 Remove Replace Power Supply PCB SVC 11 2 Remove Replace Powe...

Страница 288: ...grounded wrist strap part no 9300 0969 large or 9300 0970 small connected to a suitable ground Failure to heed this caution may result in damage to the instrument 6 Use a 7 mm nut driver to remove the screw securing the upper portion of the dual duct as sembly to the outer oven shell 7 Use a Pozidriv screwdriver to loosen but not remove the screw securing the lower portion of the dual duct assembl...

Страница 289: ...ower supply PCB mounting bracket NOTE The AC power supply PCB and its associated mounting bracket are removed and replaced as a unit 13 Lift the PCB bracket at its right edge while sliding it to the right to remove it from the instrument R3 P1 WHT J28 F1 20A R2 P3 P4 J26 J27 F2 6A R1 Oven 120 Vac Single Phase AC Board Blk P2 MOUNTING HOLES MOUNTING SLOT 14 Install the replacement AC power supply P...

Страница 290: ...e alphanu meric display as the in strument performs an internal self diagnostic integrity check to en sure that the instrument shows the expected normal displays OVEN STATUS RUN NOT READY FINAL TIME RATE INITIAL TIME OVEN STATUS RUN NOT READY FINAL TIME RATE INITIAL TIME OVEN STATUS RUN NOT READY FI NAL TIME RATE INITIAL TIME OVEN STATUS RUN NOT READY FINAL TIME RATE INITIAL TIME ACTUAL SETPOINT A...

Страница 291: ...rument 6 Remove the electronics carrier top cover by grasping it at the rear and lifting until its catch releases the pulling it toward the rear of the instrument 7 Remove the right side panel by removing four screws two each along its top and bottom edges This procedure requires precautions against ESD Electro Static Discharge Use a grounded wrist strap part no 9300 0969 large or 9300 0970 small ...

Страница 292: ...Disconnect connectors J26 and J27 from their respective receptacles on the AC power sup ply PCB Remove each one by squeezing its ribbed sides while si multaneously pulling it out of the receptacle 10 Remove the screw and lock washer securing the ground strap to the transformer bracket SCREW INSULATOR BUSHING CONNECTOR J26 CONNECTOR J27 GROUND STRAP CONNECTOR P10 Artisan Scientific Quality Instrume...

Страница 293: ... strain the wiring from connector P10 and the power switch AC POWER SUPPLY BASE EXTENSION CABLE FOR UPGRADED SERIES I TRANSFORMER BRACKET TRANSFORMER SCREW INSULATOR BUSHING POWER SUPPLY ASSEMBLY SHOWN REMOVED FROM INSTRUMENT FOR CLARITY 15 Free the wiring from connector P10 and the power switch from their associated paths in the electronics carrier 16 Remove the transformer and transformer bracke...

Страница 294: ...onics carrier top cover 28 Slide the rear cover on to the instrument 29 Secure the rear cover to the instrument by in stalling and tightening four screws 30 Restore all gas sup plies 31 Restore power to the instrument 32 Observe the alphanu meric display as the in strument performs an internal self diagnostic integrity check to en sure that the instrument shows expected normal displays 1A 1 1B 2 2...

Страница 295: ...emove the right side panel by removing four screws two each along its top and bottom edges This procedure requires precautions against ESD Electro Static Discharge Use a grounded wrist strap part no 9300 0969 large or 9300 0970 small connected to a suitable ground Failure to heed this caution may result in damage to the instrument 6 At the right side of the instrument below the main PCB remove the...

Страница 296: ...nt shows expected normal displays 1A 1 1B 2 2A 2B GREY BLACK BLACK YELLOW WHITE OVEN STATUS RUN NOT READY FINAL TIME RATE INITIAL TIME OVEN STATUS RUN NOT READY FINAL TIME RATE INITIAL TIME OVEN STATUS RUN NOT READY FINAL TIME RATE INITIAL TIME OVEN STATUS RUN NOT READY FINAL TIME RATE INITIAL TIME ACTUAL SETPOINT ACTUAL ACTUAL ACTUAL SETPOINT SETPOINT SETPOINT Test of display elements all alphanu...

Страница 297: ...ounded wrist strap part no 9300 0969 large or 9300 0970 small connected to a suitable ground Failure to heed this caution may result in damage to the instrument 6 Use a 7 mm nut driver to remove the screw securing the upper portion of the dual duct as sembly to the outer oven shell 7 Use a Pozidriv screwdriver to loosen but not remove the screw securing the lower portion of the dual duct assembly ...

Страница 298: ...air of pliers 17 With the strain relief compressed insert the power cable through the opening in the power sup ply base and seat the strain relief in the opening 18 Install the power cable ground lead on the stud on the AC power supply base and secure with a locking nut 19 Connect power cord lead push on type connectors J1 WHITE lead and J2 BLACK lead to their appropriate connectors on the AC powe...

Страница 299: ...TUS RUN NOT READY FINAL TIME RATE INITIAL TIME ACTUAL SETPOINT ACTUAL ACTUAL ACTUAL SETPOINT SETPOINT SETPOINT Test of display elements all alphanumeric and LED elements are lit 5890 Series II memory test in progress 5890A Self testing in progress LEDs off except possibly NOT READY Message indicating normal termination of diagnostic tests after power restoration User setpoints remain in force LEDs...

Страница 300: ... A 3 220VAC SPLIT PHASE BOARD APPX A 4 MAIN PCB CONNECTORS APPX A 5 P1 KEYBOARD CONNECTOR APPX A 5 P2 DETECTOR A PCB CONNECTOR APPX A 6 P3 DETECTOR B PCB CONNECTOR APPX A 7 P4 ANALOG SIGNAL 1 OUTPUT CONNECTOR APPX A 7 P5 ANALOG SIGNAL 2 OUTPUT CONNECTOR APPX A 8 P6 REMOTE START CONNECTOR APPX A 8 P7 TEMPERATURE SENSOR CONNECTOR APPX A 8 P8 OVEN FLAP MOTOR CONNECTOR APPX A 9 J9 CRYOGENIC VALVE AND ...

Страница 301: ...CONNECTORS APPX A 18 INET PCB APPX A 19 BUFFERED INET PCB APPX A 20 DICE PCB APPX A 21 DICE CONNECTOR PCB APPX A 22 ELECTRONIC FLOW SENSOR MODULE APPX A 24 VALVE PCB CONNECTORS APPX A 25 Artisan Scientific Quality Instrumentation Guaranteed 888 88 SOURCE www artisan scientific com ...

Страница 302: ... J27 2 NC J27 3 MAIN POWER SWITCH NEUTRAL J28 1 OVEN FAN MOTOR NEUTRAL J28 2 OVEN FAN MOTOR NEUTRAL J28 3 OVEN FAN MOTOR PHASE 1 J28 4 OVEN FAN MOTOR PHASE 1 220VAC SINGLE PHASE BOARD P1 LINE CORD NEUTRAL P2 LINE CORD PHASE 1 P3 OVEN HEATER NEUTRAL oven triac controlled P4 OVEN HEATER PHASE 1 P5 OVEN TRIAC ANODE 1 P6 OVEN TRIAC ANODE 2 P7 OVEN TRIAC GATE P26 1 GND P26 2 OVEN CONTROL to pulse trans...

Страница 303: ...en triac controlled P4 OVEN HEATER PHASE 1 P5 OVEN TRIAC ANODE 1 P6 OVEN TRIAC ANODE 2 P7 OVEN TRIAC GATE P26 1 GND P26 2 OVEN CONTROL to pulse transformer and oven triac gate P26 3 K1 OVEN CONTACTOR CONTROL J27 1 MAIN POWER SWITCH PHASE 1 J27 2 NC J27 3 MAIN POWER SWITCH PHASE 2 J28 1 OVEN FAN MOTOR PHASE 2 J28 2 OVEN FAN MOTOR PHASE 2 J28 3 OVEN FAN MOTOR PHASE 1 J28 4 OVEN FAN MOTOR PHASE 1 Art...

Страница 304: ...P1 7 BA4 P1 8 GND P1 9 38 4KHz P1 10 38 4KHz P1 11 POP P1 12 15V P1 13 5V P1 14 5V P1 15 24V P1 16 EXT_IN1 P1 17 EXT_OUT9 P1 18 EXT_OUT10 P1 19 BD0 P1 20 BD1 P1 21 BD2 P1 22 BD3 P1 23 BD4 P1 24 BD5 P1 25 BD6 P1 26 BD7 Artisan Scientific Quality Instrumentation Guaranteed 888 88 SOURCE www artisan scientific com ...

Страница 305: ... 7 1Q P2 8 A1 OF U16 2 P2 9 STARTA P2 10 A2 OF U16 2 P2 11 gnd P2 12 gnd P2 13 gnd P2 14 gnd P2 15 GND P2 16 GND P2 17 153 6KHz P2 18 307 4KHz P2 19 24V P2 20 2Q P2 21 24V P2 22 4 9152MHz P2 23 5V P2 24 5V Artisan Scientific Quality Instrumentation Guaranteed 888 88 SOURCE www artisan scientific com ...

Страница 306: ...D P3 16 GND P3 17 153 6KHz P3 18 307 2KHz P3 19 24V P3 20 4Q P3 21 24V P3 22 4 9152MHz P3 23 5V P3 24 5V P4 ANALOG SIGNAL 1 OUTPUT CONNECTOR P4 1 RECORDER COMMON gnd P4 2 gnd P4 3 RECORDER1 P4 4 INTEG1 P4 5 GND P4 6 AGROUND P4 7 AGROUND P4 8 GND P4 9 INTEG1 P4 10 RECORDER1 P4 11 GND P4 12 RECORDER COMMON gnd Artisan Scientific Quality Instrumentation Guaranteed 888 88 SOURCE www artisan scientific...

Страница 307: ...rt of run P6 9 READY OUTPUT connects with 5 READY P6 10 START OUTPUT same as pins 7 8 above P6 11 GND P6 12 REMOTE READY INPUT Relay contacts are rated at 3 Watts 0 25 Amp 28VDC maximum resistive load only 1 2 msec bounce Relay contacts are rated at 10 Watts 0 5 Amp 200VDC maximum resistive load only 0 4 msec bounce P7 TEMPERATURE SENSOR CONNECTOR P7 1 OVEN SENSOR P7 2 GND P7 3 DETA SENSOR P7 4 GN...

Страница 308: ...X HEATED ZONE CONNECTOR J9 1 CRYO J9 2 CRYO RETURN TO ACGND J9 3 INJ B HEATER J9 4 INJB HEATER RETURN TO ACGND J9 5 INJA HEATER J9 6 INJB HEATER RETURN TO ACGND J9 7 DETB HEATER J9 8 DETB HEATER RETURN TO ACGND J9 9 DETA HEATER J9 10 DETA HEATER RETURN TO ACGND P10 AC POWER SUPPLY CONNECTOR P10 1 40VAC P10 2 ACGND CT P10 3 40VAC P10 4 OVEN PULSE TRANSFORMER P10 5 ACGND CT P10 6 3VAC P10 7 120VAC f...

Страница 309: ...1 12 ACGND P11 13 24V P11 14 24V P11 15 3VAC fused F1 P11 16 3VAC fused F1 P11 17 3VAC fused F1 P11 18 3VAC fused F1 P11 19 3VAC fused F1 P11 20 3VAC fused F1 P11 21 3VAC fused F2 P11 22 3VAC fused F2 P11 23 3VAC fused F2 P11 24 3VAC fused F2 P11 25 3VAC fused F2 P11 26 3VAC fused F2 Artisan Scientific Quality Instrumentation Guaranteed 888 88 SOURCE www artisan scientific com ...

Страница 310: ...12 12 EXT_OUT0 P12 13 EXT_OUT1 P12 14 EXT_OUT8 P12 15 5V P12 16 5V P12 17 9 8304MHz P12 18 GND P12 19 GND P12 20 GND P12 21 GND P12 22 GND P12 23 D240 P12 24 POP P12 25 15V P12 26 15V P12 27 10VREF P12 28 COMMON P12 29 DAC2 P12 30 ATTN2 goes thru R5 to RCDR2 of P5 Artisan Scientific Quality Instrumentation Guaranteed 888 88 SOURCE www artisan scientific com ...

Страница 311: ...240 Hz square wave P13 18 POP power on pulse P13 19 SGND for switching or analog circuits P13 20 SGND for switching or analog circuits P13 21 24V P13 22 24V P13 23 24V P13 24 24V J14 AUXILIARY CONNECTOR J14 1 AUX HEATER J14 2 AUX HEATER RETURN TO ACGND J14 3 VALVE2 J14 4 VALVE2 RETURN TO ACGND J14 5 VALVE1 J14 6 VALVE1 RETURN TO ACGND P15 WORKFILE EMULATION CONNECTOR P15 1 Workfile emulation to A2...

Страница 312: ...ND J1 9 38 4KHz J1 10 38 4KHz J1 11 JOJ J1 12 15V J1 13 5V J1 14 5V J1 15 24V J1 16 EXT_IN1 J1 17 EXT_OUT9 J1 18 EXT_OUT10 J1 19 BD0 J1 20 BD1 J1 21 BD2 J1 22 BD3 J1 23 BD4 J1 24 BD5 J1 25 BD6 J1 26 BD7 Artisan Scientific Quality Instrumentation Guaranteed 888 88 SOURCE www artisan scientific com ...

Страница 313: ...J2 8 A1 OF U16 2 J2 9 STARTA J2 10 A2 OF U16 2 J2 11 gnd J2 12 gnd J2 13 gnd J2 14 gnd J2 15 GND J2 16 GND J2 17 153 6KHz J2 18 307 4KHz J2 19 24V J2 20 2Q J2 21 24V J2 22 4 9152MHz J2 23 5V J2 24 5V Artisan Scientific Quality Instrumentation Guaranteed 888 88 SOURCE www artisan scientific com ...

Страница 314: ...rcuits J1 20 SGND for switching or analog circuits J1 21 24V J1 22 24V J1 23 24V J1 24 24V P1 1 ALARM RELAY common for 2 4 P1 2 ALARM RELAY connects with 1 3 on alarm P1 3 ALARM RELAY common for 2 4 P1 4 ALARM RELAY disconects from 1 3 on alarm P1 5 24VDC P1 6 CHANNEL A BPR ENABLE VALVE P1 7 24VDC P1 8 CHANNEL B BPR ENABLE VALVE P1 9 15VDC P1 10 ALARM BUZZER DRIVE P1 11 5VDC P1 12 GND P2 1 P_SENSA...

Страница 315: ...DC P3 7 SHEILD EPC PRESSURE TRANSDUCER MODULE P1 1 15VDC P1 2 5VDC P1 3 ACOM P1 4 P_SNS pressure sensing EPC PROPORTIONAL CONTROL VALVE pin 1 VLV DR proportional valve control pin 2 SHEILD pin 3 15VDC Artisan Scientific Quality Instrumentation Guaranteed 888 88 SOURCE www artisan scientific com ...

Страница 316: ...t J1 12 EXT_IN3 J1 13 5V J1 14 5V J1 15 DGND for digital circuits J1 16 DGND for digital circuits J1 17 D240 240 Hz square wave J1 18 POP power on pulse J1 19 SGND for switching or analog circuits J1 20 SGND for switching or analog circuits J1 21 24V J1 22 24V J1 23 24VDC J1 24 24VDC Artisan Scientific Quality Instrumentation Guaranteed 888 88 SOURCE www artisan scientific com ...

Страница 317: ...D J12 19 GND J12 20 GND J12 21 GND J12 22 GND J12 23 D240 240 Hz square wave J12 24 POP power on pulse J12 25 15V J12 26 15V J12 27 10VREF J12 28 COMMON J12 29 DAC2 J12 30 ATTN2 J13 1 GND J13 2 RXD RECEIVE DATA J13 3 TXD TRANSMIT DATA J13 4 GND J13 5 GND J13 6 GND J13 7 GND J13 8 GND J13 9 GND J13 10 TXD TRANSMIT DATA J13 11 RXD RECEIVE DATA J13 12 GND Artisan Scientific Quality Instrumentation Gu...

Страница 318: ... 14 EXT_OUT8 J12 15 5V J12 16 5V J12 17 9 8304MHz J12 18 GND J12 19 GND J12 20 GND J12 21 GND J12 22 GND J12 23 D240 240 Hz square wave J12 24 POP power on pulse J12 25 15V J12 26 15V J12 27 10VREF J12 28 COMMON J12 29 DAC2 J12 30 ATTN2 J13 1 OUT J13 2 OUT_REF J13 3 IN_REF J13 4 IN Artisan Scientific Quality Instrumentation Guaranteed 888 88 SOURCE www artisan scientific com ...

Страница 319: ...T1 J12 14 EXT_OUT8 J12 15 5V J12 16 5V J12 17 9 8304MHz J12 18 GND J12 19 GND J12 20 GND J12 21 GND J12 22 GND J12 23 D240 240 Hz square wave J12 24 POP power on pulse J12 25 15V J12 26 15V J12 27 10VREF J12 28 COMMON J12 29 DAC2 J12 30 ATTN2 P1 1 OUT P1 2 OUT_REF P1 3 IN_REF P1 4 IN Artisan Scientific Quality Instrumentation Guaranteed 888 88 SOURCE www artisan scientific com ...

Страница 320: ... GND J12 20 GND J12 21 GND J12 22 GND J12 23 D240 240 Hz square wave J12 24 POP power on pulse J12 25 15V J12 26 15V J12 27 10VREF J12 28 COMMON J12 29 DAC2 J12 30 ATTN2 P1 1 OUT P1 2 OUT_REF P1 3 IN_REF P1 4 IN J1 1 DIGITAL GROUND J1 2 T R J1 3 REN J1 4 IFC J1 5 5 DCV J1 6 NDAC J1 7 NRFD J1 8 DAV J1 9 DIGITAL GROUND J1 10 EOI J1 11 ATN J1 12 SRQ Artisan Scientific Quality Instrumentation Guarante...

Страница 321: ...J1 3 REN J1 4 IFC J1 5 5 DCV J1 6 NDAC J1 7 NRFD J1 8 DAV J1 9 DIGITAL GROUND J1 10 EOI J1 11 ATN J1 12 SRQ J1 13 5 DCV J1 14 DIO0 J1 15 DIO1 J1 16 DIO2 J1 17 DIO3 J1 18 DIGITAL GROUND J1 19 DIO4 J1 20 DIO5 J1 21 DIO6 J1 22 DIO7 J1 23 5 DCV J1 24 RX RECEIVE J1 25 TX TRANSMIT J1 26 GROUND J2 1 DIO1 J2 2 DIO2 J2 3 DIO3 J2 4 DIO4 J2 5 EOI J2 6 DAV Artisan Scientific Quality Instrumentation Guaranteed...

Страница 322: ...M to digital J2 22 DCOM ground J2 23 DCOM J2 24 LOGIC J3 1 SHEILD J3 2 TX TRANSMIT J3 3 RX RECEIVE J3 4 NC J3 5 NC J3 6 NC J3 7 GND J3 8 NC J3 9 NC J3 10 NC J3 11 NC J3 12 NC J3 13 NC J3 14 NC J3 15 NC J3 16 NC J3 17 NC J3 18 NC J3 19 NC J3 20 NC J3 21 NC J3 22 NC J3 23 NC J3 24 NC J3 25 NC Artisan Scientific Quality Instrumentation Guaranteed 888 88 SOURCE www artisan scientific com ...

Страница 323: ...2 ACGND J1 13 24V J1 14 24V J1 15 3VAC fused F1 J1 16 3VAC fused F1 J1 17 3VAC fused F1 J1 18 3VAC fused F1 J1 19 3VAC fused F1 J1 20 3VAC fused F1 J1 21 3VAC fused F2 J1 22 3VAC fused F2 J1 23 3VAC fused F2 J1 24 3VAC fused F2 J1 25 3VAC fused F2 J1 26 3VAC fused F2 Artisan Scientific Quality Instrumentation Guaranteed 888 88 SOURCE www artisan scientific com ...

Страница 324: ...any Printed in USA 3 91 Manual Part No 05890 90320 This product is recyclable Printed on recycled paper Print 115 of this size Artisan Scientific Quality Instrumentation Guaranteed 888 88 SOURCE www artisan scientific com ...

Страница 325: ...NECTORS J1 1 24V J1 2 PURGE A J1 3 PURGE B J1 4 GROUND J1 5 120VAC J1 6 120VAC J1 7 120VAC J1 8 GROUND J1 9 VALVE A J1 10 VALVE B Artisan Scientific Quality Instrumentation Guaranteed 888 88 SOURCE www artisan scientific com ...

Страница 326: ...nt Service Center Repairs Experienced Engineers and Technicians on staff in our State of the art Full Service In House Service Center Facility InstraView Remote Inspection Remotely inspect equipment before purchasing with our Innovative InstraView website at http www instraview com We bUy used equipment We also offer credit for Buy Backs and Trade Ins Sell your excess underutilized and idle used e...

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