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7.3 Calibrate the sensor

7.3.1 About sensor calibration

The sensor characteristics slowly shift over time and cause the sensor to lose accuracy. The sensor
must be calibrated regularly to maintain accuracy. The calibration frequency varies with the
application and is best determined by experience.

7.3.2 Temperature calibration

It is recommended to calibrate the temperature sensor once a year. Calibrate the temperature sensor
before calibrating the measurement sensor.

1.

Put the sensor in a container of water that is at a known temperature. Under agitation, measure
the temperature of the water with an accurate thermometer or independent instrument.

2.

Push the 

menu

 key and select SENSOR SETUP>CALIBRATE.

3.

If the pass code is enabled in the security menu for the controller, enter the pass code.

4.

Select 1 PT TEMP CAL and push 

enter

.

5.

The raw temperature value is displayed. Push 

enter

.

6.

Enter the correct value if different from that displayed and push 

enter

.

7.

Push 

enter

 to confirm the calibration. The temperature offset is displayed.

7.3.3 Zero calibration

Because of the stability of the electrode, for most applications this calibration is not required but can
be used to define the unique zero point of the sensor.

1.

Remove the sensor from the process and rinse in distilled water.

2.

Push the 

menu

 key and select SENSOR SETUP>CALIBRATE.

3.

If the pass code is enabled in the security menu for the controller, enter the pass code.

4.

Select ZERO CAL and push 

enter

.

5.

Select the option for the output signal during calibration:

Option

Description

ACTIVE

The instrument sends the current measured output value during the calibration procedure.

HOLD

The sensor output value is held at the current measured value during the calibration procedure.

TRANSFER

A preset output value is sent during calibration. Refer to the controller user manual to change
the preset value.

6.

Place the clean sensor in a zero concentration solution, push 

enter

.

7.

Wait for up to one hour for the value to stabilize and push 

enter

.

8.

Review the calibration result:

• PASS—the sensor is calibrated and the offset is displayed.
• FAIL—the calibration is outside of accepted limits. Clean the sensor and retry with a fresh

reference solution. Refer to 

Troubleshooting

 on page 17 for more information.

9.

If the calibration passed, push 

enter

 to continue.

10.

If the option for operator ID is set to YES in the CAL OPTIONS menu, enter an operator ID. Refer
to 

Change calibration options

 on page 13.

11.

On the NEW SENSOR screen, select whether the sensor is new:

Option Description

YES

The sensor was not calibrated previously with this controller. The days of operation and previous
calibration curves for the sensor are reset.

NO

The sensor was calibrated previously with this controller.

English

   

11

Содержание Polymetron 9582sc

Страница 1: ...DOC023 53 93067 Hach 9582sc Dissolved Oxygen 02 2020 Edition 5 User Manual...

Страница 2: ......

Страница 3: ...iguration 10 7 2 Configure the sensor 10 7 3 Calibrate the sensor 11 7 3 1 About sensor calibration 11 7 3 2 Temperature calibration 11 7 3 3 Zero calibration 11 7 3 4 Calibration in air 12 7 3 5 Cali...

Страница 4: ...Table of Contents 2...

Страница 5: ...pressure Atmospheric pressure Relative humidity 0 90 Certifications EN 61326 1 2006 EN 61010 1 2010 Sensor module Specification Details Measuring range 0 2 ppm Sensitivity 0 5 ppb Repeatability 0 5 p...

Страница 6: ...if not avoided could result in death or serious injury C A U T I O N Indicates a potentially hazardous situation that may result in minor or moderate injury N O T I C E Indicates a situation which if...

Страница 7: ...t transfer liquid 3 3 Product components Make sure that all components have been received If any items are missing or damaged contact the manufacturer or a sales representative immediately Components...

Страница 8: ...il there is resistance Do not force the electrode 4 Install and tighten the holding nut by hand 5 Install the gasket and filling screw to prevent electrolyte leakage or external contamination from the...

Страница 9: ...connector not provided 3 Assembled sensor 7 M4 screws not provided 4 Gasket 8 1 4 NPT sample output connector not provided 4 4 Install the controller Refer to the controller documentation to see mount...

Страница 10: ...c components can be damaged by static electricity resulting in degraded performance or eventual failure Refer to the illustrated steps that follow and Table 1 Be sure to connect all sensor ground shie...

Страница 11: ...English 9...

Страница 12: ...on and push enter To enter numbers characters or punctuation push and hold the up or down arrow keys Push the right arrow key to advance to the next space Option Description EDIT NAME Changes the name...

Страница 13: ...tilled water 2 Push the menu key and select SENSOR SETUP CALIBRATE 3 If the pass code is enabled in the security menu for the controller enter the pass code 4 Select ZERO CAL and push enter 5 Select t...

Страница 14: ...rops of water Place the sensor vertically in the calibration cap with the membrane downwards Tighten the calibration cap and push enter 8 Wait for the value to stabilize and push enter 9 Review the ca...

Страница 15: ...libration options on page 13 10 On the NEW SENSOR screen select whether the sensor is new Option Description YES The sensor was not calibrated previously with this controller The days of operation and...

Страница 16: ...STANDBY Section 8 Maintenance W A R N I N G Multiple hazards Only qualified personnel must conduct the tasks described in this section of the document 8 1 Membrane replacement C A U T I O N Chemical e...

Страница 17: ...embrane 1 Unscrew the filling screw and remove along with the gasket 2 Unscrew the holding nut 3 Carefully remove the electrode from the sensor body 4 Empty any electrolyte left in the sensor body 5 U...

Страница 18: ...e and membrane visually check the silver anode If more than 2 3 of the surface is coated with silver bromide then an electrode rejuvenation is required To do this very softly polish the areas coated w...

Страница 19: ...nd install finger tight The gold surface is scratched or damaged Change the electrode Sludge or particles on the cathode Clean the cathode with a soft and absorbent tissue Rinse the membrane Cable or...

Страница 20: ...membrane filling screw and change the electrolyte and the membrane Electrolyte leaking Check the screw in parts membrane filling screw and change the electrolyte and the membrane Interferences mainly...

Страница 21: ...number for the sensor module SENSOR INFORMATION Shows the name and serial number that was entered by the user CAL DAYS Shows the number of days since the last calibration CAL HISTORY Shows a list of t...

Страница 22: ...he sensor CAL IN PROGRESS A calibration was started but not completed Return to calibration 9 3 2 Error list Errors may occur for various reasons An error icon consists of an exclamation point within...

Страница 23: ...uaranty of the described product properties 1 IDENTIFICATION OF THE SUBSTANCE Product code 09181 A 3600 Product name Electrolyte 2 COMPOSITION INFORMATION ON INGREDIENTS Water 90 CAS No 108 18 9 Potas...

Страница 24: ...cautions protective equipment and emergency procedures Use personal protective equipment Environmental precautions Do not flush into surface water or sanitary sewer system Methods and material for con...

Страница 25: ...f Specific effects in experiment on an animal No data is available on the product itself 12 ECOLOGICAL INFORMATION Toxicity No data is available on the product itself Do not flush into surface water o...

Страница 26: ...REGULATORY INFORMATION EU regulatory information The product does not need to be labelled in accordance with EC directives or respective national laws National regulatory information Water contaminati...

Страница 27: ......

Страница 28: ...669 2932 orders hach com www hach com HACH LANGE GMBH Willst tterstra e 11 D 40549 D sseldorf Germany Tel 49 0 2 11 52 88 320 Fax 49 0 2 11 52 88 210 info de hach com www de hach com HACH LANGE S rl 6...

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