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9009
User’s Guide
20
Calibrator Characteristics
There is a temperature gradient vertically in the test well. The heater has been applied to the block in
such a way as to compensate for nominal heat losses out of the top of the calibrator. However, actual
heat losses will vary with design of the thermometer probes inserted into the calibrator. For best
results, insert probe to full depth of well.
Stabilization and Accuracy
The stabilization time of the Product depends on the conditions and temperatures involved. Typically
,
the test well will be stable to 0.1
°
C within 5 minutes of reaching the set-point temperature. Ultimate
stability is achieved 10 minutes to 20 minutes after the Product reaches the set temperature.
If you insert another cold probe into a well
,
this requires another period of stabilizing, depending on the
magnitude of the disturbance and the required accuracy. For example, if you insert a .25
-
in diameter
room temperature probe at 300
°
C
,
it takes 5 minutes to be within 0.1
°
C of its settled point and takes
10
minutes to achieve maximum stability.
To speed up the calibration process, know how soon to make the measurement. Make typical
measurements at the desired temperatures with the test probes under test to establish these times.
Calibration
Note
Consider this procedure a general guideline. Each laboratory must write their own procedure
based on their equipment and their quality program. Each procedure should be accompanied
by an uncertainty analysis also based on the equipment and environment of the laboratory
.
You may want to calibrate the Product to improve the temperature set-point accuracy. To adjust
calibration
,
adjust the controller probe calibration constants R0, ALPHA, DELTA, and BETA (cold side)
so that the temperature of the Product as measured with a standard thermometer agrees more closely
with the set-point. The thermometer used must be able to measure the well temperature with higher
accuracy than the desired accuracy of the Product. Use a good thermometer and this calibration
procedure to calibrate the Product to an accuracy of better than 0.5
°
C up to 100
°
C.
Calibration Points
When you calibrate the Product, adjust R0, ALPHA, DELTA, and BETA (cold side) to minimize the set-
point error at each of three different Product temperatures. Any three reasonably separated
temperatures can be used for the calibration. Improved results can be obtained for shorter ranges
when you use temperatures that are just within the most useful operating range of the Product. The
farther apart the calibration temperatures, the larger will be the calibrated temperature range, but the
calibration error will also be greater over the range. Choosing a range of 50
°
C to 90
°
C may allow the
calibrator to have a better accuracy of maybe
±
0.2
°
C over that range
,
but outside that range the
accuracy may be only
±
1.5
°
C.