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Instruction Manual

Tokyo Rikakikai Co., Ltd.

FREEZE DRYER

Model FDU-1110(220V)
Model FDU-2110(220V)

R02

This manual contains important matters to maintain the functions and to use this product safely.

Keep this manual with care near the product for quick reference.

Important

Be sure to read “Safety Precautions”
carefully before use.

Содержание FDU-1110

Страница 1: ...FDU 1110 220V Model FDU 2110 220V R02 This manual contains important matters to maintain the functions and to use this product safely Keep this manual with care near the product for quick reference Important Be sure to read Safety Precautions carefully before use ...

Страница 2: ...potential hazardous situation in which mishandling will result in death or serious injury of the user CAUTION Indicates a potential hazardous situation in which mishandling will result in minor or moderate injury of the user or damage to the property Though we have given enough considerations to almost possible hazards during the product use it is still very difficult to anticipate all of the poss...

Страница 3: ...labels 2 Caution Label on the Product The caution label that is important especially is attached to the main body of the product This label is located as in the figure shown below Follow the instruction on the label with care during the product usage INJURY Do not touch the cooling fins with bare hands CAUTION ...

Страница 4: ...me of Each Part 3 Names and Functions of Operation Parts 3 1 Control Panel 3 2 Safety Function 4 Installation 4 1 Installation Environment 4 2 Installation Conditions 4 3 Installation Procedures 4 4 Connection of Utility 1 2 2 3 4 8 9 12 14 14 15 16 Trap Barrier Air Inlet Barrier Vacuum Joint Pipe Trap Cover Vacuum Hose NOTE Check attached parts inside the cold trap and main body Introduction Cont...

Страница 5: ...on of specimen such as organic solution and others which contain flammable material Use extreme caution about vaporization of flammable material such as organic solvent and others If any solvent not trapped enters into the vacuum pump it can be ignited and burnt Cooling Fins 1 Pre freeze the container for specimen Never start the vacuum pump before inner walls of Cold Trap has been cooled enough I...

Страница 6: ... 930 H Approx 140 kg 5 5A 2 4 kVA Cooling System Vessel cooling system 100 V AC Max 3 A Displacement of Vacuum Pump 100 120 L min 50 60 Hz or more option Other Functions Control of vacuum pump display for availability of freeze dry Indication accuracy at 0 4 to 4 0 Pa 2 0 Pa at 4 1 to 10 0 Pa 3 0 Pa at 10 1 to 15 0 Pa 4 0 Pa at 15 1 to 40 0 Pa 7 0 Pa 45 C 4 liters each time 600 W R404A Approx 100 ...

Страница 7: ...en which contain water of 375 cc pre frozen are mounted on the trap And amount of sublimation is calculated backward based on remaining amount of water in flasks along with time passage Input voltage AC220 V 50 Hz Room temperature 20 C Progress of sublimation depends on conditions in use such as room temperature capacity and shape of specimen container round bottom flask or bottle characteristic a...

Страница 8: ... 119820 119830 Port for Round bottom Flask Round bottom flask made of stainless material 9 ports for mounting specimen container are provided for Model PMH 1000 Inside of manifold is washable Models Code Nos PMH 1000 197440 To use this device incorporating into the product remove the base legs 4 BSC 2L BSC 3L Base Leg Base Leg DRC 2L Base Leg DRC 3L Base Leg PMH 4 PMH 8 PMH 24 PMH 1000 PMH 12 DRC ...

Страница 9: ...L 13 x 90 6 mL 13 x 100 7 mL 15 x 85 8 mL 15 x 105 10 mL 15 x 150 15 mL 16 5 x 105 12 mL 16 5 x 165 20 mL 18 x 165 24 mL 18 x 180 27 mL 21 x 200 42 mL 144010 144020 144030 144040 144050 144060 144070 144080 144100 144110 144120 144090 100 100 100 100 100 100 100 100 100 100 50 100 50 50 50 50 1 120210 Ampul Eggplant Type 1 mL Pencil type with round bottom 1 mL Flat Bottom 2 mL 120220 120221 120230...

Страница 10: ...ecifications Code Nos Parts Names Cock D Vacuum Cock Body D Liner A Vacuum Cock D Adapter for Flask 10 11 12 13 14 15 209570 233480 143950 233490 120470 144500 Nos QTY 1 1 10 1 1 1 T 29 S T 24 S T 29 S T 29 S T 29 S T 29 S T 29 S T 29 S Cock D Freeze dry Bottle Flask etc 11 12 13 10 14 16 17 18 8 15 24 15 19 21 20 23 22 ...

Страница 11: ... 119980 119990 120000 120010 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Filter Holder 120100 Filter Cap for Adapter for Freeze dry Bottle For 45 40 80 mL For 70 120 150 300 mL For 105 600 900 1200m Adapter for Freeze dry Bottle 120450 120460 120110 120020 120030 120040 A type Adapter for Test Tube 16 120500 1 Multiple Serial Connection Adapter 120490 1 3 2 1 1 1 100 sheets 1 box Flask for Specimen 17 18 19 20 1 ...

Страница 12: ...old Trap Caster Component specified for FDU 1110 FDU 2110 respectively Inspection Door for Vacuum Pump Fuse Holder Recorder Output Vacuum Recorder Output Temp in Trap Plug Socket Recorder Output Vacuum Recorder Output Temp in Trap Drain Cap Drain Hose Fixing Parts Contact Tokyo Rikakikai for connecting cord provided with no charge for the recorder on FDU as necessary Fixing Parts Vibration Proof I...

Страница 13: ...ady Lamp Refrigerator Lamp Alarm Lamp Alarm Lamp for Refrigerator Timer Mode Lamps Timer Mode Select Switch Set Key Switch Set Key Lamp Timer Switch Def Auto Refrigerator Run Stop Auto Manual Select Switch Auto Operation Lamp Refrigerator Switch Refrigerator Switch Lamp Vacuum Pump Switch Lamp Vacuum Pump Switch Vac Pump Defroster Switch Defroster Switch Lamp Trap Monitor Lamp AC100V only Timer La...

Страница 14: ...y Defroster Switch Lamp This lamp is lighted when the Defroster Switch is turned ON The lamp goes off when defrosting is completed Trap Temp Display Displays temperatures measured on Trap Cooling Unit Vacuum Display Displays Pa value of the vacuum measured on the equipment Timer Display Displays a time period of measurement by switching the operation mode Freeze Drying Ready Lamp This lamp is ligh...

Страница 15: ... seconds or more respectively to stop the equipment 2 Press the Defroster Switch for 3 seconds or more for executing ON OFF operation 3 Press the Timer Reset Switch for 5 seconds or more for executing reset operation Trap Monitor Lamp AC100V only This lamp blinks when the optional trap monitor sensors amount of dehumidified liquid inside the cold trap Refer to Trap Monitor in Sec 2 4 Option 11 21 ...

Страница 16: ...e for the overload relay depends on conditions in use so that it differs 3 to 40 minutes Ambient temperature is too high Refrigerator filter is clogged Too many specimens are mounted at once Refrigerator starts operates under overload Fan for the refrigerator does not operate Low power supply voltage Fuse for Plug Socket The fuse rated 3 15 A is blown and the power to the product is interrupted Se...

Страница 17: ...pite preset period for operation recovery time in power failure Alarm Alarm of malfunction in guidewire of vacuum sensor Alarm lamp is lighted and PrEr is indicated on the vacuum gauge display Then the buzzer is sounded for 10 seconds Control is continued in manual operation In Auto operation the mode is switched into Manual operation and control is continued Circuit of vacuum Sensor has malfuncti...

Страница 18: ...erator under hot temperature and high pressure may result in equipment failure WARNING Keep enough space around the product CAUTION Be careful in carrying the heavy product CAUTION If the product is installed in inappropriate environment It may result in equipment damage in an early stage or insufficient exercise of its functions and performance Be careful of installation environment CAUTION Insta...

Страница 19: ...Part Product is lowered Product is lifted Level Adjuster Level Adjusters If the product is carried on uneven ground the caster may be damaged by excessive impact Lock Unlock Stopper Caster 3 When the product is placed in an appropriate location lock the caster stopper 4 If the installation location has uneven level secure the product using level adjusters Be sure to stabilize the product to a leve...

Страница 20: ...power source do not use split socket or power strip 16 Connection should be made confirming voltage phase capacity type of outlet WARNING Connect earthing conductor correctly WARNING Do not use split socket or power strip WARNING Product Model FDU 1110 Power necessary for connection Ampacity 10 A Voltages FDU 2110 AC220 V Single phase 7 A Power Cord Recommended Plugs Lock type In case power plug i...

Страница 21: ...mp outside the FDU main body and use it The vacuum tube can be used by drawing it from the outlet of the hose container in the back of the main body Refer to the figures on the below In such case for the vacuum pump use a different power source from the main body s then cannot drive automatically 5 1 Preparation for Operation Rear Face of the Main Body To installed the vacuum pump outside the main...

Страница 22: ... about proper handlings of the vacuum pump refer to the user s manual of the pump Drain Hose Socket outlet for Vacuum Pump Power Plug of Vacuum Pump 6 Follow the procedure in 4 to mount the stopper plate of the front part of the pump and tighten the wing bolts to fix the pump 7 Follow the procedures in reverse order 3 to 2 Insert the pump plate into the stoppers Put the stopper on the plate and ti...

Страница 23: ...ert the barrier into air inlet Air inlet barrier executes icing uniformly on the internal walls of the trap Cold Trap Trap Barrier Trap Cover Air Inlet Barrier Fixing rubber for Trap Cover Trap Cover Trap Joint Packing Trap Barrier Air Inlet Barrier Trap Packing Rubber Joint for Air Inlet Cold Trap To the center Air Inlet Packing Mount the trap cover positioning with the three pieces of fixing rub...

Страница 24: ...ith activation of the vacuum pump Capacity of the socket is 3 A If any load current more than 3 A is applied safety device fuse will be activated As for replacement of fuse refer to Sec 7 3 Fuse Replacement 3 A FUSE Vacuum Trap Temp Socket Outlet Fuse Box Fuse Recorder Output Trap Temp Vacuum Output voltages for recorder are as follows Output Signals For Trap Temp 1 C 1 mV Ex 40mV for 40 Red White...

Страница 25: ...erator Alarm Ref Alarm Disp Set Reset Run Stop Timer hour min Trap Temp Display Timer Display Freeze Drying Ready Lamp Refrigerator Lamp Alarm Lamp Alarm Lamp for Refrigerator Timer Mode Lamps Timer Mode Select Switch Set Key Switch Set Key Lamp Timer Switch Def Auto Refrigerator Run Stop Auto Manual Select Switch Auto Operation Lamp Refrigerator Switch Refrigerator Switch Lamp Vacuum Pump Switch ...

Страница 26: ... control Enter an appropriate time period between 0 to 1 hour and 30 minutes Numerous values are indicated in the range of 0 00 to 1 30 If preset time period is too long ice and water in the cold trap may be melted and sucked into the vacuum pump during this period This may result in equipment failure hour hour min TRAP TEMP 5 0 0 Timer Mode1 Mode2 TRAP TEMP P F F o T rap temp Vacuum Timer Mode1 M...

Страница 27: ...ntainers CAUTION 23 3 Usages of Timer Press Timer Mode Select Switch serially to switchover Timer Mode 1 or 2 Mode 1 Operation time of vacuum pump is measured and indicated automatically This mode is useful to calculate an appropriate period for oil replacement for the pump Mode 2 Timer switch is turned on off by stopwatch function This mode is useful to measure a period of sublimation To turn off...

Страница 28: ...s are kept it is possible to attach the containers serially FDU 1110 Freeze Drying Ready Lamp goes off where trap temperature exceeds 30 C and vacuum value exceeds 25 Pa The lamp is not lighted until trap temperature and vacuum value reach 30 C and 25 Pa again FDU 2110 Freeze Drying Ready lamp goes off where trap temperature exceeds 50 C and vacuum value exceeds 15 Pa The lamp is not lighted until...

Страница 29: ...other equipment failure replace the filter referring to Sec 7 1 3 Leak Filter Replacement Turn the cock rightward to regain normal pressure And detach the container VENT VAC VAC Hold the specimen container with hands not to drop it after releasing vacuum CAUTION Ice formed on the inner walls of trap begins to melt Hot Gas Trap Barrier Cooling Part After the defrosting operation make sure that the ...

Страница 30: ...equipment failure in vacuum pump etc or leakage current Do not fill the water up to 5 liters or more in Cold Trap CAUTION Scrape the ice out After the defrosting operation never fail to clean up the inside walls of the trap and drain pipe Not doing so may leave a small amount of ice at the trap bottom or inside the pipe Be sure to pour the hot water for a few times to clean up and discharge the re...

Страница 31: ...er begins to melt Therefore adjust the tilt of the container in advance of the process so that the rubber dewdrop tray can receive dripping dewdrops appropriately If granular frost formation is found inside the cold trap during freeze drying process vacuum leakage might have been occurred Check the joint between the specimen container and adaptor 5 Freeze drying process After attaching the specime...

Страница 32: ...side the trap simultaneously Before stopping the vacuum pump be sure to detach all of the specimen containers If normal pressure is not regained in the trap or this process is too slow leak filter may be clogged In such case since it may result in reverse flow of oil or other equipment failure replace the filter referring to Sec 7 1 3 Leak Filter Replacement 8 Defrost Operation Press Defrost switc...

Страница 33: ...esult in equipment failure in vacuum pump etc or leakage current Do not fill the water up to 4 liters or more in Cold Trap CAUTION Scrape the ice out After the defrosting operation never fail to clean up the inside walls of the trap and drain pipe Not doing so may leave a small amount of ice at the trap bottom or inside the pipe Be sure to pour the hot water for a few times to clean up and remove ...

Страница 34: ... insufficient Gas is leaking After the activation of timer make sure that the refrigerator operates normally Refrigerator protection timer is activated for approx 5 minutes Keep enough space behind the equipment Refer to 4 2 Installation Conditions Ambient temperature exceeds 35 C Heating overload to the refrigerator is too heavy Adjust the heating overload to the appropriate rated load Vacuum pum...

Страница 35: ...ed Refrigerator is started operated under overload If several causes are considered conditions of operation differs Alarm for malfunction in guidewire of temp sensor Guidewire of temp sensor has malfunction Alarm Lit 0000 Trap Temp display PrEr Trap Temp display Lit Alarm Vacuum pump does not emit light exhaust noise when 30 seconds passed since it had been started Pressure is not lowered Connecti...

Страница 36: ... Alarm SYMPTOMS CAUSES SOLUTIONS oFF Current trap temp and OFF are indicated in turn Measured temp CPAr Vacuum gauge display Lit Alarm Backup Battery failed or runs out Backup Battery Error Alarm Contact your sales dealer or nearest service center of Tokyo Rikakikai Press Set key to release alarm message By doing this normal indication recovers However backup function for recovery select for power...

Страница 37: ...dewdrop These parts can be removed and fixed easily utilizing their inherent elasticity 2 Replacement of air inlet connecting rubber trap connecting packing 1 Remove these parts from the equipment 2 Untighten 3 pieces of screws fixing the air inlet Prepare screwdriver by yourself 3 Remove the top cover for inspection and untighten the wing nuts 4 pieces Connecting trap rubber and inlet can be remo...

Страница 38: ...e overcurrent is flown This failure may result in fire If the replaced fuse blows again stop the operation immediately And inspect the optional devices Parts Name Code No Fuse 3 15 A 147670 Fuse Holder Body Fuse Holder Body Fuse 3 15 A Power On Off Main Body Left face CAUTION 7 4 Control of Vacuum Pump Oil Oil conditions largely depend on ultimate pressure and the lifespan of the pump Therefore to...

Страница 39: ...tilation Cover 2 Remove the spring for the filter mount 3 Take out the filter and brush the dust Then wash the filter using water or a neutral detergent 4 Dry the filter completely And reattach the filter in place Never touch the cooling fins with bare hands during maintenance Sharp edges of the fins may hurt user s hands Do not touch the cooling fins with bare hands Do not dissemble the equipment...

Страница 40: ...ccordance with applicable disposal rules Disposal of Product 8 Main components and their disposal methods Packing materials should be disposed of separately with each material Members Specifications FDU 2110 Weights Outer Dimensions mm Main Body Approx 140 kg 36 FDU 1110 700W x 550D x 930H Approx 100 kg 700W x 550D x 930H ...

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