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Information about the Manual

Table of contents

Information about the Manual .............................................................................................................. 6

1.1

Explanation of signs and symbols ..................................................................................................... 6

1.2

Disclaimer .......................................................................................................................................... 6

1.3

Copyright ............................................................................................................................................ 6

Safety ...................................................................................................................................................... 7

2.1

Explanation of the safety instructions ................................................................................................ 8

2.2

General safety instructions ................................................................................................................ 9

2.3

Repairs ............................................................................................................................................. 10

2.4

Intended use .................................................................................................................................... 10

2.5

Improper use .................................................................................................................................... 10

2.6

Safety symbols on the machine ....................................................................................................... 11

2.7

Emergency stop ............................................................................................................................... 12

2.8

Residual risks................................................................................................................................... 12

Description ........................................................................................................................................... 18

3.1

Front ................................................................................................................................................. 18

3.2

Back of the analyzer ........................................................................................................................ 19

Installation ............................................................................................................................................ 21

4.1

Setting up ......................................................................................................................................... 22

4.2

Filling the reagent tubes .................................................................................................................. 23

4.3

Establishing the gas supply ............................................................................................................. 23

4.4

Connecting the machine to the PC .................................................................................................. 24

4.5

Establishing the power supply ......................................................................................................... 24

Commissioning .................................................................................................................................... 25

Operation of the analyzer ................................................................................................................... 26

Technical data ...................................................................................................................................... 29

7.1

Technical data for the analyzer ........................................................................................................ 29

7.2

Type plate on the analyzer .............................................................................................................. 30

7.3

Standards for inorganic materials .................................................................................................... 31

Troubleshooting on the analyzer ....................................................................................................... 32

8.1

Troubleshooting on the analyzer. .................................................................................................... 32

Cleaning ............................................................................................................................................... 32

Maintenance ......................................................................................................................................... 33

10.1

Maintenance the analyzer ................................................................................................................ 33

10.1.1

Overview of maintenance work for the analyzer ...................................................................... 33

10.1.2

Removing the reagent tubes .................................................................................................... 34

10.1.3

Filling reagent tubes ................................................................................................................ 37

10.1.3.1

Filling the reagent tube on the SO

filter .......................................................................... 38

10.1.3.2

Filling the reagent tube on the inlet gas purification ........................................................ 39

10.1.3.3

Filling the reagent tube on the moisture filter .................................................................. 40

10.1.4

Inserting reagent tubes ............................................................................................................ 41

10.1.5

Replacing the dust filter cartridge on the analyzer .................................................................. 43

10.1.6

Filling the reagent tube on the catalyst furnace ....................................................................... 44

10.1.7

Cleaning the dust box .............................................................................................................. 47

10.1.7.1

Quick cleaning of the dust box ......................................................................................... 48

10.1.7.2

Thorough cleaning of the dust box .................................................................................. 49

10.1.8

Maintenance in the furnace area ............................................................................................. 50

10.1.8.1

Replacing the furnace cleaning brush and thermal shield ............................................... 50

10.1.8.2

Replacing the combustion tube ....................................................................................... 54

10.1.8.3

Removing the crucible tray .............................................................................................. 56

10.1.9

Replacing the O-rings .............................................................................................................. 57

Содержание ELEMENTRAC CS-i

Страница 1: ... Eltra GmbH 42781 Haan Retsch Allee 1 5 Germany 10 12 2020 Version 0005 Operating Manual ELEMENTRAC CS i Translation ...

Страница 2: ...Information about the Manual 2 Urheberrecht Copyright by Eltra GmbH Retsch Allee 1 5 42781 Haan Germany ...

Страница 3: ...Information about the Manual 3 ...

Страница 4: ...s for inorganic materials 31 8 Troubleshooting on the analyzer 32 8 1 Troubleshooting on the analyzer 32 9 Cleaning 32 10 Maintenance 33 10 1 Maintenance the analyzer 33 10 1 1 Overview of maintenance work for the analyzer 33 10 1 2 Removing the reagent tubes 34 10 1 3 Filling reagent tubes 37 10 1 3 1 Filling the reagent tube on the SO3 filter 38 10 1 3 2 Filling the reagent tube on the inlet gas...

Страница 5: ...er 63 11 1 1 Front of the machine 63 11 1 2 Front interior view 64 11 1 2 1 Catalyst furnace 66 11 1 2 2 Complete dust filter housing with heating element 67 11 1 2 3 Complete dust filter 68 11 1 3 Furnace 69 11 1 4 Furnace cleaning mechanism 72 11 1 5 Back of the machine 73 11 1 6 Left hand side of the machine 74 11 1 6 1 Left side Dev Gate 75 11 1 6 2 Valve block compressed air control system 76...

Страница 6: ...dditional information 1 First instruction 2 Next instruction Result Numbered paragraphs contain a series of instructions An instruction can end with a result Tab 1 Signs and symbols used 1 2 Disclaimer Die vorliegende Bedi enungsanleitung w urde wi th größter Sorgfalt erstellt Technische Änder ung en sind vorbehalten Für Personenschäden die aus der Nichtbefolgung der Sicherheits and W arnhinw eise...

Страница 7: ... means of a verbal introduction by a competent person and or with the help of this Manual Incorrect operation may lead to personal injuries The operating company itself is responsible for its safety and that of its staff The operating company itself must ensure that no unauthorised personnel have access to the machine Target group This covers everybody who operates cleans or works on the machine T...

Страница 8: ... injuries may ensue if the Warning signs are not complied with There is an increased risk of a serious accident or potentially fatal injury The signal word WARNING is also used in the running text or instructions CAUTION C1 0000 Risk of injuries Source of the danger Possible consequences of failure to heed the risk Instructions and advice on how to avoid the risk Moderate or minor injuries may ens...

Страница 9: ...ne Improper modifications to the machine can lead to injuries Do not make any unauthorised changes to the machine Only use spare parts and accessories that have been approved by Eltra GmbH NOTICE N2 0012 Changes to the machine Improper modification As a result of improper modification the conformity with European directives as specified by Eltra GmbH will no longer be valid All warranty claims wil...

Страница 10: ... Retsch Allee 1 5 42781 Haan Germany 49 2104 2333 444 service eltra com www eltra com 2 4 Intended use The ELEMENTRAC CS i has been developed for the analysis of carbon and sulphur in various materials The induction furnace permits the analysis of typically inorganic materials such as metals alloys ceramics and cement 2 5 Improper use Use is prohibited in the private domain and for purposes other ...

Страница 11: ...analyzer Fig 1 Safety symbols on the analyzer Position Component Description 1 The warning signs at the top on the back and on the right hand side warn that the covers may only be opened by qualified personnel 2 3 The warning signs on the furnace opening warn of a risk of burns and crushing on fingers or hands 4 5 The warning sign on the dust filter housing warns of burns 2 1 4 5 3 ...

Страница 12: ...ntenance work on the analyzer WARNING W2 0015 Risk to life caused by an electric shock Connection to a socket without protective conductor Connecting the machine to sockets without protective conductor can lead to life threatening injuries caused by an electric shock Only operate the machine on sockets with a protective conductor PE WARNING W3 0002 Risk to life caused by an electric shock Damaged ...

Страница 13: ...rasp the sample insertion tool by the plastic handle when inserting it into the furnace WARNING W5 0017 Risk of injury Dangerous chemicals Dangerous chemicals can cause fatal poisoning or serious chemical burns to the skin when working on the machine Comply with the safety data sheet for the substances used Wear personal protective equipment Never eat or drink near chemicals WARNING W6 0022 Chemic...

Страница 14: ...nd cause serious poisoning Connect the exhaust air outlet on the machine to a suitable ventilation system Wear your personal protective equipment Comply with the safety data sheet for the substances used Carry out a risk analysis on the potential hazards of your samples and implement protective measures WARNING W9 0000 Risk of life threatening injuries Falling loads The analyzer may only be transp...

Страница 15: ... are placed securely on the surface CAUTION C6 0000 Risk of cuts Glass splinters Sample vials and reagent tubes are made of glass and can break Glass splinters can cause cuts Inspect reagent tubes and sample vials for damage prior to use Wear protective gloves and goggles when handling reagent tubes and sample vials Replace damaged reagent tubes and sample vials Do not touch glass splinters with u...

Страница 16: ...le light and invisible infrared light Wear suitable goggles when working on the furnace To protect your eyes slide the glass guard in front of the furnace entrance Never look directly into the furnace CAUTION C10 0093a Risk of burns Hot sample carriers The sample carrier may be very hot after the analysis and can cause fires and therefore injuries if in contact with flammable surfaces Always use s...

Страница 17: ... The machine is pressurised during operation The removal of the reagent tube during operation results in an explosive escape of chemicals or sample material and can cause injuries Never remove reagent tubes during operation CAUTION C13 0094 Risk of burns Hot catalyst furnace The furnace temperature of the catalyst furnace can be up to 800 C during operation and cause burns Wear heat resistant prot...

Страница 18: ... 1 Front The following figure shows the front of the machine Fig 2 Front of the ELEMENTRAC CS i Position Component Description 1 Analyzer Analyzer with induction furnace 2 Crucible holder Holder for ceramic crucibles with sample material and furnace opening 3 Main switch on the analyzer Switches the analyzer on and off 4 Analyzer door Behind the machine door are the paper filter dust box carrier g...

Страница 19: ...essed air inlet Compressed air connector 6 Gas outlet For discharging the analysis gas 7 Carrier gas connector Connector with pressure reducer for the carrier gas oxygen 8 Inlet for analysis gas from the HTFr Return of the analysis gas from the HTFr for analysis 9 Connector for carrier gas supply to the HTFr Carrier gas supply for the HTFr 10 Connector for vacuum cleaner Connector for a vacuum cle...

Страница 20: ...rload or short circuit 13 Power connection for the vacuum cleaner Switched power socket to connect a vacuum cleaner The vacuum cleaner can be switched on automatically on opening the furnace after every analysis 14 Power connection for equipment with low output Socket for connecting equipment with low output such as a PC and monitor ...

Страница 21: ...c shock Check the mains lead and plug for damage before operating the machine Never operate the machine with a damaged mains lead or plug WARNING W12 0000 Risk of life threatening injuries Falling loads The analyzer may only be transported or lifted using suitable lifting gear such as a forklift or crane Loads can fall down causing life threatening injuries Only lift and transport the analyzer wit...

Страница 22: ...achine see Technical data The power plugs must be easily accessible at all times The surface of the machine bench must be non slip and fire resistant Set the machine up as follows 1 Set the machine up on the prepared workstation 2 Ensure that the power plugs on the analyzer are freely accessible at all times 3 Make sure to set up both machines in a way that does not block the fans 4 Set up the PC ...

Страница 23: ...l and grease free compressed air Set a pressure of at least 2 4 bar Use only oil and grease free compressed air Check the set pressure of the carrier gas Establish the gas supply for the machine as follows 1 Ensure that the gas supply for the carrier gas is switched off 2 Connect the carrier gas inlet on the analyzer see Pos 7 in Back of the analyzer to the operating company s carrier gas supply U...

Страница 24: ...ck Connection to a socket without protective conductor Connecting the machine to sockets without protective conductor can lead to life threatening injuries caused by an electric shock Only operate the machine on sockets with a protective conductor PE The power supply is provided using the supplied power plug The operating company s mains connections must meet the power requirements of the machine ...

Страница 25: ...Setting up The reagent tubes have been filled see Filling the reagent tube The machine has been connected to the PC see Connecting the machine to the PC The gas supply has been established see Establishing the gas supply The power supply has been established see Establishing the power supply Commission the machine as follows 1 Switch on the PC and start the ELEMENTS software a current version of t...

Страница 26: ...RNING W16 0000 Risk of poisoning Toxic combustion gases Samples are exposed to high temperatures during the analysis Harmful gaseous fission products can be released or formed from reaction processes here These gases can escape from the gas outlet and cause serious poisoning Connect the exhaust air outlet on the machine to a suitable ventilation system Wear your personal protective equipment Compl...

Страница 27: ...AUTION C18 0096 Risk of eye injury Very bright combustion tube The combustion tube shines very brightly when it is hot and can cause eye injuries if you look directly into the furnace due to visible light and invisible infrared light Wear suitable goggles when working on the furnace To protect your eyes slide the glass guard in front of the furnace entrance Never look directly into the furnace CAU...

Страница 28: ...e Analyses and results window Create a new analysis and select a suitable application see Elements Software Application 3 Prepare a crucible with sample material Only use crucibles Part number 90148 or 90149 from Eltra GmbH 4 Use the automatic transfer of the sample weight from the balance to the PC or enter the sample weight manually Give a name for the sample in the ID box 5 If you wish to analy...

Страница 29: ...ion class I Overvoltage category II Degree of contamination 2 Type of environment Indoors Max altitude 2000 m Ambient temperature 5 to 35 C Ambient humidity 80 at 31 C non condensing Type of protection IP20 Carrier gas Type Oxygen Purity Min 99 5 Pressure 2 to 4 bar 30 to 60 psi Connection Polyamide hose 6 4 mm Adapter with G female thread included with delivery Compressed air Type Oil free Pressu...

Страница 30: ...ate on the analyzer Fig 4 Type plate on the analyzer Position Component 1 Manufacturer s address 2 Part number 3 Mains frequency 4 Read the Manual 5 CE mark 6 Type of protection 7 Disposal label 8 Current 9 Voltage 10 Year of manufacture 11 Serial number 12 Machine designation 2 5 7 1 8 10 4 6 3 12 11 9 ...

Страница 31: ...balt alloys CS i CS d ASTM E 1587 2010 C S Refined nickel CS i CS d ASTM E1915 13 C S Metalliferous ores and related materials i e tailings waste rock CS i CS d UOP703 09 C Catalysers CS i CS d ASTM E 1941 2010 C Refractory metals CS i CS d EN ISO 15349 2 C Steel CS i CS d ISO 13902 S Steel and iron CS i CS d ISO 4689 3 S Iron ores CS i CS d ISO 7524 C Nickel CS i CS d EN 27526 S Nickel CS i CS d ...

Страница 32: ...lectric shock if the machine has not been disconnected from the power supply Only clean the machine with water when it has been disconnected from the power supply NOTICE N5 0077 Damage to the housing Use of organic solvents Organic solvents can damage the coating Organic solvents must not be used to clean the housing The outside of the ELEMENTRAC CS d must be cleaned regularly Proceed as follows t...

Страница 33: ...at the specified maintenance intervals or upon reaching the number of possible analyses Component No of analyses Maintenance interval Service instructions See chapter Cellulose 2000 Every 3 months Replace when 50 of the filter is black Filling the reagent tube on the SO3 filter Inlet gas purification 1000 Every 3 months Replace early if clumping is apparent Filling the reagent tube on the inlet ga...

Страница 34: ...e between the furnace and metal filter 10 1 2 Removing the reagent tubes CAUTION C21 0076 Risk of burns Hot machine parts Some parts of the machine can get very hot and cause burns when touched without wearing protective gloves Wear heat resistant protective gloves when working with hot machine parts Never touch hot parts of the machine without suitable protective gloves CAUTION C22 0000 Risk of c...

Страница 35: ...ive goggles when working with chemicals Comply with the safety data sheets for the chemicals used The reagent tubes of the analyzer must not be removed during operation The following diagram shows the filters on the front of the analyzer with the machine door open Fig 5 Front of the analyzer with the door open Position Component 1 Moisture filter 2 Inlet gas purification 3 SO3 filter 3 2 1 ...

Страница 36: ...e pressure The following diagram shows an example of removing a reagent tube on the front of the analyzer Fig 6 Removing the reagent tube on the front of the analyzer 3 Slide the reagent tube upwards 4 Swivel the reagent tube slightly to the side or to the front 5 Pull the reagent tube out from below If the reagent tube cannot be moved easily turn it slightly while puling it out The reagent tube o...

Страница 37: ...ION C26 0090 Risk of eye injury Chemicals When changing the chemicals minute particles of chemicals may be suspended in the air and cause burns to eyes Always wear protective goggles when working with chemicals Comply with the safety data sheets for the chemicals used WARNING W18 0000 Risk of poisoning Toxic combustion gases Samples are exposed to high temperatures during the analysis Harmful gase...

Страница 38: ... 1 Turn the main switch on the analyzer to Position 1 2 Remove the reagent tube see Removing the reagent tubes on filters 3 Remove the used filling from the reagent tube 4 Dispose of the reagent tube filling in accordance with local regulations and provisions 5 Ensure that the reagent tube is undamaged If it is damaged or too contaminated use a new reagent tube Part No 88400 0422 6 Fill the reagen...

Страница 39: ...the reagent tube is undamaged If it is damaged or too contaminated use a new reagent tube Part No 88400 0006 6 Fill the reagent tube with 1 5 to 2 cm of glass wool Part No 90331 7 Fill approx 10 cm of magnesium perchlorate Part No 90200 onto the glass wool 8 Fill 0 5 to 1 cm of glass wool Part No 90331 onto the magnesium perchlorate 9 Fill approx 10 cm of sodium hydroxide Part No 90210 onto the gl...

Страница 40: ...ube Part No 88400 0005 8 Release the threaded rod from the paper filter holder and remove the paper filter If the paper filter holder is damaged use a new paper filter holder Part No 11120 9 Where necessary replace the O ring on the paper filter holder Part No 70230 10 Place a new paper filter Part No 11185 into the paper filter holder and fold the edge of the paper over 11 Carefully guide the pap...

Страница 41: ...lling reagent tubes 4 Clean the connections for the reagent tube on the analyzer 5 Lightly grease the inner ends of the reagent tube and the O rings with high vacuum silicon grease Part No 92610 The following diagram shows an example of inserting a reagent tube on the front of the analyzer Fig 7 Inserting a reagent tube on the front of the analyzer 6 Hold the filled reagent tube 3 at a slight angl...

Страница 42: ... impression of approx 2 mm on the reagent tube and that there is no leak on the O ring caused by the glass wool 11 Confirm the message on the ELEMENTS software so that the pressure can be built up again The reagent tube on the front of the analyzer has been inserted ...

Страница 43: ...ch on the analyzer to Position 1 2 Press the Change reagents button in the ELEMENTS software to release the pressure 3 Press the dust filter cartridge 2 upwards against the top support 1 4 Swivel the bottom end of the dust filter cartridge 2 forwards and pull the dust filter cartridge 2 out from below 5 Press the new dust filter cartridge 2 upwards at an angle into the top support 1 The diameter o...

Страница 44: ...ear heat resistant protective gloves when working with the catalyst furnace Only replace the catalyst furnace filling after a sufficiently long cooling period This diagram shows the front of the analyzer with open catalyst furnace and details of the reagent tube Fig 9 Open catalyst furnace with details of the reagent tube The catalyst furnace is only functional once it has reached its operating te...

Страница 45: ...ent tube 9 Carefully pull the reagent tube 5 out of the guide 4 10 Where this is not the first filling remove the used filling from the reagent tube 11 Dispose of the reagent tube filling in accordance with local regulations and provisions 12 Ensure that the reagent tube is undamaged If it is damaged or too contaminated use a new reagent tube Part No 88400 0452 13 Turn the reagent tube over for fi...

Страница 46: ...0 Carefully slide the hose 1 onto the reagent tube 5 The hose must be pushed at least 5 mm over the reagent tube connector 21 Secure the hose 1 using the clamp 2 The reagent tube on the catalyst furnace has been filled ...

Страница 47: ...nfrared measuring cells of the analyzer It is necessary to clean the dust box to prevent the absorption of reaction gases and associated lower results Fig 10 Removing the dust box Position Component 1 Dust box 2 O ring 3 Lock For cleaning the metal filter holder with the dust box must first be removed 1 Release the plug in connector on the metal filter heater 2 Turn the lock 3 90 to the left to re...

Страница 48: ...aling mechanism should be clean and remain absolutely free of grease Proceed as follows to quickly clean the dust box 1 Ensure that the filter housing with the dust filter has been removed see Cleaning the dust box 2 Using a suitable paper towel remove the grease at the top end of the filter cartridge _ Clean the filter from the top end of the filter housing 2 3 To do this turn the supplied brush ...

Страница 49: ...lter with the dust box has been removed see Cleaning the dust box Position of the O rings Fig 12 Assembled metal filter Position Component 1 Outer O ring 2 Inner O ring 2 Slide the metal filter 5 out of the filter housing 4 with a suitable blunt tool 3 Fig 13 Thoroughly cleaning the dust box Position Component 3 Suitable tool e g screwdriver 4 Filter housing 5 Metal filter 3 Check the outer O ring...

Страница 50: ...contacts can cause life threatening injuries or death Turn the main switch to Position 0 and pull out the power plug prior to maintenance work on the analyzer Turn the main switch to Position 1 prior to maintenance work on the HTFr machine and allow the machine to cool down sufficiently Only set the main switch to Position 0 and pull out the power plug once you have allowed sufficient time for the...

Страница 51: ...ed and the knurled nuts can be easily unscrewed 2 Turn the main switch on the analyzer to Position 0 and pull out the power plug 3 Wait until the furnace of the analyzer has cooled down sufficiently The following diagram shows the mounting bolts for the top furnace lining at the top and at the front of the machine Fig 14 Removing the top furnace lining 4 Unscrew the Allen screws 1 3 and 4 at the t...

Страница 52: ...ng system mounting plate 6 Remove the knurled nuts 6 and 13 7 Unscrew the wing nuts 8 and 12 8 Unscrew the gas connectors 5 and 9 also see detailed image and remove the gas hoses The following image shows the removed furnace cleaning system Fig 16 Removed furnace cleaning system 12 13 6 10 7 8 5 9 11 15 14 17 18 16 ...

Страница 53: ...ield where necessary Part No 14072 The thermal shield must be replaced if it is too contaminated or damaged Check whether the purge drilled hole is clean and unblocked 13 Insert the furnace cleaning system again from the top 14 Check that the top end plate of the furnace 11 is resting on the O ring 15 Evenly tighten the wing nuts 8 and 12 on the top end plate of the furnace 16 Tighten the knurled ...

Страница 54: ...r as follows 1 Turn the main switch on the analyzer to Position 0 and pull out the power plug 2 Wait until the analyzer has cooled down sufficiently 3 Remove the furnace cleaning system see Replacing the furnace cleaning brush and thermal shield The following diagram shows the bottom end plate of the furnace on the analyzer Fig 17 Bottom end plate of the furnace on the analyzer 4 Unscrew the wing ...

Страница 55: ...ing from the top 8 Hold the combustion tube tight from above and if necessary insert a new O ring from below 9 Secure the bottom end plate of the furnace again Ensure that the combustion tube is resting cleanly in the guide of the bottom end plate of the furnace 10 Tighten the wing nuts 1 and 2 11 Insert the furnace cleaning system see Replacing the furnace cleaning brush and thermal shield 12 Plu...

Страница 56: ... tray 1 out of the furnace bell 3 If it is difficult to release this perform steps 4 to 8 otherwise continue with step 9 4 If the sample stand is difficult to lift unscrew the guide 2 from the bell 3 using a 24 mm wrench 5 Twist the guide out completely 6 Using a tool remove the tray from the guide 7 Clean the thread on the furnace bell 3 and on the nut 2 Use a vacuum cleaner to clean the thread 8...

Страница 57: ... break Glass splinters can cause cuts Inspect reagent tubes and sample vials for damage prior to use Wear protective gloves and goggles when handling reagent tubes and sample vials Replace damaged reagent tubes and sample vials Do not touch glass splinters with unprotected hands 10 1 9 1 Replacing the O ring at the top of the combustion tube Replace the top O ring on the combustion tube of the ana...

Страница 58: ...8 Insert the furnace cleaning system again see Replacing the furnace cleaning brush and thermal shield 9 Plug in the power plug and turn the main switch on the analyzer to Position 1 The O ring at the top of the combustion tube on the analyzer has been replaced 10 1 9 2 Replacing the O rings at the bottom and in the bottom furnace locking device Replace the O rings at the bottom of the combustion ...

Страница 59: ...ace lock 1 down and off The O ring on the underneath of the furnace is now accessible Fig 22 O ring on the bottom furnace lock 6 Remove the O ring 4 7 Apply a thin layer high vacuum silicon grease Part No 92610 to the inside of the new O ring Part No 70380 8 Insert the new O ring on the underneath of the furnace on the combustion tube 2 3 1 4 ...

Страница 60: ...ng the furnace cleaning brush and thermal shield 14 Plug in the power plug and turn the main switch on the analyzer to Position 1 The O rings at the bottom of the combustion tube and in the bottom furnace lock of the analyzer have been replaced 10 1 9 3 Replacing the O rings on the furnace seal The O rings must be replaced when they no longer provide an adequate seal due to damage or age Replace t...

Страница 61: ...ing surfaces on the rods and the inside of the furnace lock to remove grease and dust 11 Insert the new O rings 12 Slide the top furnace lock 6 back on 13 Insert the retaining rings 4 and 9 14 Slide on the support 5 from above 15 Insert the washers 2 and 11 and the springs 3 and 10 16 Screw on the nuts 1 and 12 17 Insert the furnace cleaning system again see Replacing the furnace cleaning brush an...

Страница 62: ...rew the hose nuts on the filter connector and on the bottom furnace locking device 1 3 Pull the hose 2 off 4 In der ELEMENTS software start the vacuum Analyzer status window under User service or use an external vacuum cleaner to remove falling particles while cleaning 5 Clean the hose with a pipe cleaner Part No 70002 or with a micro brush Part No 88400 0501 6 Replace the hose Part No 51100 2040 ...

Страница 63: ...parts 63 11 Spare parts 11 1 Spare parts for the analyzer 11 1 1 Front of the machine Fig 26 Diagram of the front when closed Position Designation Part No Quantity 1 Hinge with eccentric pin 88400 0288 2 1 1 ...

Страница 64: ...Spare parts 64 11 1 2 Front interior view Fig 27 Diagram of the front inside 12 1 2 3 4 5 6 7 8 9 11 10 ...

Страница 65: ... 51100 2017 1 4 Bottom filter holder 35361 1 5 Bottom reagent tube holder moisture trap 11045 1 6 O ring 9x3 70230 6 7 Dust filter cartridge 11170 1 8 Top filter holder 35363 1 9 Reagent tube 88400 0006 2 10 Complete catalyst furnace 20100 2003 1 11 Top reagent tube holder moisture trap 11042 1 12 Complete dust filter housing with heating element 51100 2035 1 ...

Страница 66: ...tom reagent tube holder catalyst furnace 20100 2004 1 2 Quartz tube 88400 0422 1 3 Top reagent tube holder catalyst furnace 20100 2005 1 4 Reagent tube 240x20 16 4 88400 0452 1 5 Hose clip clamp 66500 0084 1 6 O ring 9x3 70230 1 7 O ring 8x3 70200 1 8 O ring 8x1 5 for 20100 2003 catalyst furnace 70180 1 1 2 3 4 5 6 7 8 ...

Страница 67: ...g with heating element Fig 29 Complete dust filter housing 51100 2035 Position Designation Part No Quantity 1 Dust box mechanism 51100 2019 1 2 Complete dust filter housing with heating element 51100 2035 1 3 Filter connection holder 51100 2013 1 1 2 3 ...

Страница 68: ...1 1 2 3 Complete dust filter Fig 30 Dust filter 11107 Position Designation Part No Quantity Complete dust filter 11107 1 1 Metal filter 11105 1 2 O ring 34x3 70370 1 3 Filter lock 11093 1 4 O ring 20x5 70320 1 1 2 3 4 ...

Страница 69: ... 2 6 Bottom knurled nut 14161 2 7 Wing nut 76003 4 8 Glued 9 Bottom end plate of the furnace 14025 2001 1 10 Pneumatic cylinder 14009 2001 1 11 Cone 14180 1 12 Cone insert 14170 13 Crucible tray 14168 1 14 Crucible 90148 90149 1000 15 Combustion tube 14130 1 16 Combustion coil 13067 1 17 Mounting bar 14080 2 18 Retaining ring 08 647 0006 2 Fig 31 Furnace front view 1 1 2 3 4 5 7 8 9 7 10 11 12 13 ...

Страница 70: ...70380 2 2 O ring 3 4x1 9 70120 2 3 M4 spacer sleeve 75150 2 4 Brush holder 14051 1 5 Cleaning brush 14045 1 6 Heat protection ceramic 14072 1 7 Bottom knurled nut 14161 4 8 Disc 08 701 0076 4 9 O ring 35x5 70390 1 Fig 32 Furnace front view 2 1 2 3 4 9 5 1 6 7 8 7 ...

Страница 71: ...Spare parts 71 Fig 33 Furnace front view 3 Position Designation Part No Quantity 1 Furnace cover 51100 2045 1 2 M4x10 countersunk screw 08 643 0055 4 1 2 ...

Страница 72: ...y 1 Spring 75122 2 2 Mounting bar 14080 2 3 Complete top furnace locking device 14021 1 4 O ring 3 4x1 9 70120 2 5 Spacer sleeve 75150 2 6 Brush holder 14051 1 7 Combustion tube cleaning brush 14045 1 8 Complete ceramic thermal shield for the brush 14072 1 Complete furnace cleaning mechanism 51100 2004 1 1 2 3 4 5 6 7 8 ...

Страница 73: ...ion Designation Part No Quantity 1 2P 16 AC circuit breaker 66400 0385 1 2 SCHUKO socket 88400 0413 2 3 250V 16A mains filter 77140 1 4 Fan guard 120x120 88400 0155 1 5 24V fan 66400 0304 1 6 Gas valve 51100 2031 1 7 O2 pressure regulator 11492 1 1 2 6 7 3 4 5 ...

Страница 74: ...ion Part No Quantity 1 Complete compressed air control system 27000 2024 1 2 PCB pressure sensor 27000 5004 3 Valve block 51100 2030 1 4 Complete gas valve 51100 2029 4 5 CS i d gas valve 51100 2041 2 6 Complete control valve 51100 2032 1 7 Uni 2 x with housing 11001 3003 1 1 3 4 5 6 4 5 2 7 ...

Страница 75: ...Spare parts 75 11 1 6 1 Left side Dev Gate Fig 37 DevGate Position Designation Part No Quantity 1 Inlet pressure regulator 11492 1 2 PCB DevGate 88600 5000 1 2 1 ...

Страница 76: ...ol system Fig 38 Valve block compressed air control system 27000 2024 Designation Part No Quantity 1 5 2 way valve 66200 0140 1 2 5 3 way valve 66200 0139 1 3 Pressure regulator 60236 2 4 Pushbutton switch 66300 0158 1 5 2 2 way valve 66200 0141 1 1 2 3 4 5 ...

Страница 77: ...l Part No 1101 2005 is required to discharge the oscillating circuit ELTRA Service must be contacted before opening the right hand side of the machine to work on this side DANGER D5 0005 Risk to life caused by an electric shock Exposed power contacts high voltage An electric shock can cause serious injuries in the form of burns cardiac arrhythmia respiratory failure or cardiac arrest Set the mains...

Страница 78: ...posed power contacts high voltage An electric shock can cause serious injuries in the form of burns cardiac arrhythmia respiratory failure or cardiac arrest Set the mains switch on the analyzer to position 0 and unplug the mains plug from the socket A Fig 39 Top mounting plate 1 2 3 4 5 6 7 1 8 9 10 ...

Страница 79: ...3 1 3 Transformer 12045 1 4 Maxthermo Power Controller 88400 0394 1 5 Coupling relay 2 changeover 8A 24VDC 66400 0450 1 6 24VDC 4 NO mini contactor 66300 0428 1 7 Toroidal transformer catalyst furnace 66400 0061 1 8 Power supply unit 88400 0395 1 9 Fan furnace cooling 24V 66400 0304 1 10 Fuse holder 88400 0268 2 ...

Страница 80: ...ion furnace optional Fig 40 Complete gas purification furnace Part No Designation Quantity 21000 1001 Complete gas purification furnace 1 21120 Quartz tube 1 70380 O ring 35x5 2 88400 0122 Filling for the gas purification furnace CS 1 ...

Страница 81: ...vGate board and 27000 5001 PCB furnace power control 2 66300 0410 Safety fuse 3 15A for the top mounting plate 1 11 4 Consumables Part No Designation Quantity 90148 90149 Crucible 1000 Stk 90200 Anhydrone 454g 90210 Sodium hydroxide 500g 88400 0535 Pt Si 15g 90330 Quartz wool 50g 90332 Glass wool 50g ...

Страница 82: ...ally remove the consumed chemicals and dispose of them in accordance with local regulations 9 Check the reagent tube for damage In the event of damage such as cracks or recrystallisation dispose of the reagent tube in accordance with local regulations because proper use is no longer possible 10 Insert the empty reagent tube This ensures that the reagent tube is not damaged when not in use The mach...

Страница 83: ... August 2005 in the B2B area which applies to this product may be disposed of with the municipal or domestic waste The machines have a disposal label to indicate this Fig 41 Disposal label Since the disposal regulations may differ from country to country throughout the world and within the EU you should contact the supplier of the machine directly where necessary In Germany this labelling duty has...

Страница 84: ...ablishing the power supply 24 Filling the reagent tubes 23 Setting up 22 Instructions 8 Intended use 10 L Left hand side of the machine 74 M Machine designation 30 Mains frequency 30 Maintenance Overview for the analyzer 33 Maintenance Removing the reagent tubes 34 Maintenance Filling the reagent tube on the SO3 filter 38 Maintenance Filling the reagent tube on the inlet gas purification 39 Mainte...

Страница 85: ...ock on the analyzer 58 Replacing the O rings 57 Replacing the O rings Furnace seal on the analyzer 60 Residual risks 12 Return of the machine 83 Revision status 6 S Safety 7 Residual risks 12 Safety symbols on the machine 11 Safety officer 7 Safety symbols on the machine 11 Serial number 30 Service address 10 Signs and symbols 6 Spare parts 63 Spare parts for the furnace cleaning mechanism 72 Spar...

Страница 86: ...Copyright Copyright by Eltra GmbH Retsch Allee 1 5 42781 Haan Deutschland ...

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