Buchi Rotavapor R-187EL, Инструкция по эксплуатации

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BÜCHI Rotavapor R-187EL
5.4 Solvent table
5 Operating the Rotavapor
Solvent Formula Molary weight Energy of Boiling point in °C Tightness Vacuum in mbar
in g/mol evaporation in J/g at 1013 mbar in g/cm 3 for boiling at 40 ºC
Acetic acid C
2
H
4
O
2
60.0 6 9 5 11 8 1.049 4 4
Aceton C
3
H
6
O 58.1 5 5 3 5 6 0.790 5 5 6
N-Amylalcohol, n-Pentanol C
5
H
12
O 88.1 5 9 5 3 7 0.814 1 1
Benzene C
6
H
6
78.1 5 4 8 8 0 0.877 2 3 6
n-Butanol, tert. Butanol C
4
H
10
O 74.1 6 2 0 11 8 0.810 2 5
2-Methyl-2-Propanol C
4
H
10
O 74.1 5 9 0 8 2 0.789 1 3 0
Carbontetrachloride, tetra Chloromethane CCI
4
153.8 2 2 6 7 7 1.594 2 7 1
Chlorobenzene C
6
H
5
CI 112.6 3 7 7 132 1.106 3 6
Chloroform CHCI
3
119.4 2 6 4 6 2 1.483 4 7 4
Cyclohexane C
6
H
12
84.0 3 8 9 8 1 0.779 2 3 5
Diethyl ether C
4
H
10
O 74.0 3 8 9 3 5 0.714 850*
1, 2,-Dichloroethane C
2
H
4
CI
2
99.0 3 3 5 8 4 1.235 2 1 0
1,2,-Dichloroethylene (cis) C
2
H
2
CI
2
97.0 3 2 2 6 0 1.284 4 7 9
1,2,-Dichloroethylene (trans) C
2
H
2
CI
2
97.0 3 1 4 4 8 1.257 7 5 1
Di isopropyl ether C
6
H
14
O 102.0 3 1 8 6 8 0.724 3 7 5
Dioxane C
4
H
8
O
2
88.1 4 0 6 101 1.034 1 0 7
DMF (Dimethylformamide) C
3
H
7
NO 73.1 153 0.949 1 1
Ethanol C
2
H
6
O 46.0 8 7 9 7 9 0.789 1 7 5
Ethyl acetat C
4
H
8
O
2
88.1 3 9 4 7 7 0.900 2 4 0
Heptane C
7
H
16
100.2 3 7 3 9 8 0.684 1 2 0
Hexane C
6
H
14
86.2 3 6 8 6 9 0.660 3 3 5
Isopropyl alcohol C
3
H
8
O 60.1 6 9 9 8 2 0.786 1 3 7
Isoamyl alcohol, 3-Methyl-1-Butanol C
5
H
12
O 88.1 5 9 5 129 0.809 1 4
Methyl ethyl ketone C
4
H
8
O 72.1 4 7 3 8 0 0.805 2 4 3
Methanol CH
4
O 32.0 1 2 2 7 6 5 0.791 3 3 7
Methylenechloride, Dichloromethane CH
2
CI
2
84.9 3 7 3 4 0 1.327 850*
Pentane C
5
H
12
72.1 3 8 1 3 6 0.626 850*
n-Propyl alcohol C
3
H
8
O 60.1 7 8 7 9 7 0.804 6 7
Pentachlorethane C
2
HCI
5
202.3 2 0 1 162 1.680 1 3
1,1, 2,2,-Tetrachloroethane C
2
H
2
CI
4
167.9 2 4 7 146 1.595 3 5
1,1,1,-Trichloroethane C
2
H
3
CI
3
133.4 2 5 1 7 4 1.339 3 0 0
Tetrachloroethylene C
2
CI
4
165.8 2 3 4 1 2 1 1.623 5 3
THF (Tetrahydrofurane) C
4
H
8
O 72.1 6 7 0.889 3 5 7
Toluene C
7
H
8
92.2 4 2 7 111 0.867 7 7
Trichloroethylene C
2
HCI
3
131.3 2 6 4 8 7 1.464 1 8 3
Water H
2
O 18.0 2 2 6 1 100 1.000 7 2
Xylene (Isomers mixture) C
8
H
10
106.2 3 8 9 2 5
(o) 144 0.880
(m) 139 0.864
(p) 138 0.861
Table 2: Solvents * only possible when cooling water is 20°C