Installation and Start-Up | 3-43
If the X-axis time interval on the
ColumnSetup.dyc
needs to be ad-
justed, right-click your mouse button on the graph, click
Display
and
change the time period in the
Minutes
text field.
4. The sample gas should now be flowing through the analyzer and peri-
odically, approximately every 120 seconds (default setting), should be
switching the two columns. The graph on the computer screen being
displayed should resemble one of the three graphs in Figure 3-24. Im-
mediately after a column switch, the real-time concentrations of H
2
S,
COS, and MeSH should drop.
After a short time delay (usually 10–20 seconds) the concentration of
H
2
S should start to increase. This is the onset of H
2
S elution from the
column. A few seconds later, COS should also begin to elute from the
column. The concentrations should then stabilize into a plateau.
Eventually, if the
Switching Interval
(Figure 3-23) is sufficiently long,
the MeSH will elute and also plateau. Typically, EtSH elution may
begin soon after (10–30 seconds) the MeSH stabilizes into a plateau.
Figure 3-22.
Column setup graph.
NOTE
Содержание 933S
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Страница 52: ...3 6 Model 933S UV Analyzer Figure 3 1 Analyzer backpan dimensions European...
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Страница 187: ...Maintenance and Troubleshooting 6 11 Figure 6 2 Optical Bench Assembly with Standard Range Measuring Cell...
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Страница 191: ...Maintenance and Troubleshooting 6 15 Figure 6 3 2 Low Range White Cell 81 2 cm P N 100 1780 1A...
Страница 197: ...Maintenance and Troubleshooting 6 21 Figure 6 4 Column Block assembly...
Страница 229: ...Maintenance and Troubleshooting 6 53 Figure 6 14 Optical Bench Chopper Assembly Maintenance diagram 100 2313 1A...
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Страница 279: ...Appendix A Drawings A 15 Optical Bench Board P N 100 1662...
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Страница 285: ...Appendix A Drawings A 21 Inlet and Vent Flame Arrestor Locations Environmental Purge Option 100 1783 1A...
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