Agilent Technologies varian 320-MS LC/MS Скачать руководство пользователя страница 12

9300025700: Rev. A 

12

 

of 14

  

Pre-installation Instructions 

 

Materials and Solvents 

The Varian Representative will prepare solutions to tune and evaluate the LC/MS. Please 
supply the materials on Table 13 and the solvents on Table 14

.

 

Table 13 Materials 

Quantity (each) 

Item 

50 mL clean and new volumetric flasks 

1 L clean and new bottles for mobile phase reservoirs 

1 L or larger bottle for LC/MS waste 

10 mL clean and new volumetric flask 

100 mL clean and new volumetric flask 

Pipette 100 to 1000 µL and tips 

Pipette 20 to 200 µL and tips 

50 mL clean and new volumetric flask (for optional APCI) 

500 mL clean and new volumetric flask (for optional APCI) 

 

Table 14 Solvents for ESI or APCI  

Quantity (each) 

Solvent 

2  

4-liter bottle HPLC grade or better water, new and unopened  

2  

4-liter bottle HPLC grade or better, acetonitrile, new and unopened 

Additional tubing is required to complete installation. Most of this tubing is included in the 
accessory kits of the LC modules. Additional tubing (PEEK™ or stainless steel) may be 
required for installation of special valves or modules. For most analytical HPLC systems, use 
1/16 in. tubing with an ID of 0.005 in. Use 0.005 in. ID or smaller tubing downstream of the 
sample injector and autosampler to prevent peak broadening. Keep tubing as short as possible 
to prevent peak broadening and to minimize run time. 

;

 

Check the checklist box: Materials and solvents of specified grade are on site.

 

Содержание varian 320-MS LC/MS

Страница 1: ...114 kg 250 lb 320 MS with HTS PAL at least 103 kg 231 lb Bench does not vibrate Exhaust system is suitable Temperature maintained between 16 and 30 C 61 86 F Relative humidity maintained between 20 a...

Страница 2: ...s can be analyzed After meeting all of these requirements contact the Customer Service office in your region to schedule the installation The LC MS operates reliably under carefully controlled environ...

Страница 3: ...needed Allow additional room for maneuvering the shipping containers around corners and through doors Check the checklist box Entrance to the installation site is at least 92 cm 36 in wide CAUTION The...

Страница 4: ...ut the modules in Figure 1 Table 1 Bench Width with the 460 LC Bench Width 212 LC 460 LC MS CPU Monitor and Keyboard Total cm 26 30 53 5 18 7 51 178 cm in 10 5 12 21 7 5 20 71 in Table 2 Bench Load wi...

Страница 5: ...5 11 5 231 lb The system requires a clean flat bench The bench must be strong enough to support the weight of the modules The area under the bench must be large enough for the foreline pump If the be...

Страница 6: ...have sufficient room to connect the MS to the foreline pump If the distance between the bench and the wall is less than 10 2 4 in then the bench must be at least 94 cm 37 in deep To accommodate the v...

Страница 7: ...least 20 L min to a separate vent line Ensure that the exhaust system does not pull a vacuum on the API chamber Consult local regulations for the proper method of exhausting the fumes Check the checkl...

Страница 8: ...er particulate matter Particulate matter may block airflow vents causing the electronics to overheat Check the checklist box Installation site is free of excessive particulate matter Power Requirement...

Страница 9: ...instruments and equipment Never plug the mass spectrometer and the chromatograph into the same power source or the power source may overload Never use the free outlet on any of the power sources for e...

Страница 10: ...ags or transients The voltage must meet EN IEC 61000 4 5 and EN IEC 61000 4 11 standards for voltage stability A measured ground to neutral potential of greater than 3V ac or V dc indicates grounding...

Страница 11: ...erators require regular maintenance The customer is responsible for setting up the preventive maintenance procedures and schedules contact the nitrogen generator manufacturer The Varian Warranty does...

Страница 12: ...ean and new volumetric flask for optional APCI Table 14 Solvents for ESI or APCI Quantity each Solvent 2 4 liter bottle HPLC grade or better water new and unopened 2 4 liter bottle HPLC grade or bette...

Страница 13: ...ansit and instrument damage may have occurred One indicator is on the exterior Read and follow the instructions on the label If the tube on the ShockWatch indicator is red the carton was dropped in tr...

Страница 14: ...e and the conditions of delivery accepted The process requires at least three days Spare Parts Please refer to the Quadrupole Hardware Manual which has list of spare parts for routine operation Preven...

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