Agilent Technologies varian 320-MS LC/MS Скачать руководство пользователя страница 11

9300025700: Rev. A 

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Pre-installation Instructions 

 

Qualified Computer Equipment 

If the Varian MS Workstation software is to be installed on a computer not purchased 
from Varian, the customer is responsible to ensure that the computer is adequately 
equipped and compatible with the operation of the data system and its communication 
interfaces. Please check the current list of requirements, available at the following web 
site. 

Varian does not guarantee the function of the Varian MS Workstation software on 
computer hardware or operating systems that do not meet the specified requirements. 

NOTE: Contact your Sales Representative for a list of qualified equipment or for more 
information. 

Gas Requirements  

Nitrogen 

A nitrogen gas supply that can provide up to a maximum of 12 L/min of gas regulated at 80 psi 
is sufficient for ESI or APCI operation for one LC/MS. If there is more than one LC/MS, use a 
nitrogen supply that can deliver a maximum of 18 L/min. The nitrogen must be at least 99% 
pure with less than 0.1 ppm hydrocarbons and less than 1% oxygen. It must be clean and dry 
with a 

40 °C

 

dew point. Use a nitrogen generator, or a liquid nitrogen boil-off to supply the 

nitrogen gas. All nitrogen generators require regular maintenance. The customer is responsible 
for setting up the preventive maintenance procedures and schedules (contact the nitrogen 
generator manufacturer). The Varian Warranty does not cover any MS problems caused by 
poor gas quality. It is the responsibility of the customer to conform to all regulations regarding 
the installation and operation of the gas system. The nitrogen supply uses ¼ in. connectors

;

 

Check the checklist box: Nitrogen gas (at least 99% pure), regulator, and gas 

lines are installed.

 

Air 

A compressed air gas supply, capable of providing up to 3 L/min of gas regulated to 80 psi with 
a two-stage regulator, is required as a nebulizing gas for negative ESI. The customer is 
responsible to conform to all regulations for the installation and operation of the gas system. 
The air must be clean and dry, with less than 0.1 ppm total hydrocarbons, including methane, 
and have a 

40 °C dew point. The air supply uses ¼ in. connectors. 

;

 

Check the checklist box: Air (less than 0.1 ppm hydrocarbons), regulator, and 

gas lines are installed.

 

CID Gas (triple quadrupole only) 

Argon is required as collision gas for MS/MS work with triple quadrupole instruments. The 
argon supply uses 1/8 in. connectors. Use a two-stage 0-100 psi pressure regulator with a 
stainless steel diaphragm. The purity of the argon must be greater than 99.0%.  

;

 

Check the checklist box: Argon (greater than 99.0% pure), regulator, and gas 

lines are installed. Argon required only for triple quadrupole instruments.

 

 

Содержание varian 320-MS LC/MS

Страница 1: ...114 kg 250 lb 320 MS with HTS PAL at least 103 kg 231 lb Bench does not vibrate Exhaust system is suitable Temperature maintained between 16 and 30 C 61 86 F Relative humidity maintained between 20 a...

Страница 2: ...s can be analyzed After meeting all of these requirements contact the Customer Service office in your region to schedule the installation The LC MS operates reliably under carefully controlled environ...

Страница 3: ...needed Allow additional room for maneuvering the shipping containers around corners and through doors Check the checklist box Entrance to the installation site is at least 92 cm 36 in wide CAUTION The...

Страница 4: ...ut the modules in Figure 1 Table 1 Bench Width with the 460 LC Bench Width 212 LC 460 LC MS CPU Monitor and Keyboard Total cm 26 30 53 5 18 7 51 178 cm in 10 5 12 21 7 5 20 71 in Table 2 Bench Load wi...

Страница 5: ...5 11 5 231 lb The system requires a clean flat bench The bench must be strong enough to support the weight of the modules The area under the bench must be large enough for the foreline pump If the be...

Страница 6: ...have sufficient room to connect the MS to the foreline pump If the distance between the bench and the wall is less than 10 2 4 in then the bench must be at least 94 cm 37 in deep To accommodate the v...

Страница 7: ...least 20 L min to a separate vent line Ensure that the exhaust system does not pull a vacuum on the API chamber Consult local regulations for the proper method of exhausting the fumes Check the checkl...

Страница 8: ...er particulate matter Particulate matter may block airflow vents causing the electronics to overheat Check the checklist box Installation site is free of excessive particulate matter Power Requirement...

Страница 9: ...instruments and equipment Never plug the mass spectrometer and the chromatograph into the same power source or the power source may overload Never use the free outlet on any of the power sources for e...

Страница 10: ...ags or transients The voltage must meet EN IEC 61000 4 5 and EN IEC 61000 4 11 standards for voltage stability A measured ground to neutral potential of greater than 3V ac or V dc indicates grounding...

Страница 11: ...erators require regular maintenance The customer is responsible for setting up the preventive maintenance procedures and schedules contact the nitrogen generator manufacturer The Varian Warranty does...

Страница 12: ...ean and new volumetric flask for optional APCI Table 14 Solvents for ESI or APCI Quantity each Solvent 2 4 liter bottle HPLC grade or better water new and unopened 2 4 liter bottle HPLC grade or bette...

Страница 13: ...ansit and instrument damage may have occurred One indicator is on the exterior Read and follow the instructions on the label If the tube on the ShockWatch indicator is red the carton was dropped in tr...

Страница 14: ...e and the conditions of delivery accepted The process requires at least three days Spare Parts Please refer to the Quadrupole Hardware Manual which has list of spare parts for routine operation Preven...

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