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Navigator 600 Phosphate

Multi-stream

Appendix G – Analyzing a Grab Sample

IM/NAV6P/MS–EN Rev. F

Appendix G –
Analyzing a Grab Sample

To analyze a grab sample:

1. Disable all streams apart from one:

a. at the 'Main Configuration' menu, select 'Measurement'

and scroll down to 'Enable Streams'.

b. press 'Enter' and untick each stream, leaving 1 ticked.

c. press the 'Menu' key and exit by 'Saving Current

Configuration' to internal memory.

2. Setup a grab sample:

a. unscrew the Secondary bottle lid and remove the level

sensor.

b. rinse the level sensor with high purity water.

c. place the level sensor into a grab sample container.

3. Energize the Secondary Calibration Valve:

a. at the 'Calibration & Maintenance' parameter, select

'Manual Test Settings' and press 'OK' (this takes the
unit Offline).

b. go to 'Test Valves' and set 'Sec. Cal Value On' by

pressing Enter.

c. exit this section by selecting 'TEST' mode (not

'NORMAL').

4. Measure the sample:

a. leave the sample flowing for at least 20 minutes – the

reading stabilizes between 15 and 20 minutes,
depending upon the difference in silica levels from the
analyzer sample and the grab sample.

5. Finish:

a. remove the level sensor form the grab sample, rinse

thoroughly with high purity water, place back in the
secondary calibration solution.

b. leave running for a 5 minutes to allow the sample line

to flush through.

6. Enable all the streams to be sample as before – follow

step 1,ensuring all required streams are ticked.

7. De-energize the Secondary Calibration Valve:

a. return to the 'Calibration & Maintenance' parameter

'Manual Test Settings' option, select 'Exit' and press
'Enter'.

b. exit this section by selecting 'NORMAL' (not 'TEST') –

the analyzer now reverts to normal operation following
a recovery period.

Содержание Navigator 600 Phosphate

Страница 1: ...N PROFIBUS Supplement Navigator 600 Series Analyzers Silica and Phosphate IM NAV6PBS Addendum RoHS Directive 2011 65 EU RoHS II ADD MEASUREMENT 001 EN Cost effective automated monitoring of phosphate...

Страница 2: ...uration Level Common Configuration Measurement Logging Communications Logging Level Not enabled from Audit Log Alarm Log This level cannot be accessed from Configuration Logging Alarm Relays Current O...

Страница 3: ...ay Contact Protection and Interference Suppression 20 4 7 Preparing the Analytical Section 21 4 7 1 Connecting Sample Inlet and Drain Line s 21 4 7 2 Connecting the Contaminated Drain Tube 21 5 Config...

Страница 4: ...peration 64 A 3 2 Safety Labels 64 Appendix B Diagnostics and Alarms 65 B 1 Analyzer Diagnostic Information 65 B 2 Audit Log and Alarm Event Log 70 B 2 1 Audit Log Icons 70 B 2 2 Alarm Event Log Icons...

Страница 5: ...y To ensure that our products are safe and without risk to health the following points must be noted The relevant sections of these instructions must be read carefully before proceeding Warning labels...

Страница 6: ...icates that the marked item can be hot and should not be touched without care This symbol indicates the presence of devices sensitive to electrostatic discharge and indicates that care must be taken t...

Страница 7: ...l damage or pollution caused by any of its products is minimized as far as possible The European Waste Electrical and Electronic Equipment WEEE Directive 2002 96 EC that came into force on August 13 2...

Страница 8: ...ng the instrument please contact the company that sold it to you If this is not possible or if the results of this approach are not satisfactory please contact the manufacturer s Customer Service 1 12...

Страница 9: ...wn in Fig 2 1 The hinged lower door provides environmental protection for the liquid handling section to ensure stabilized measurement conditions To maintain optimum measurement accuracy the analyzer...

Страница 10: ...microprocessor to measure only streams with sample present If all streams are out of sample the analyzer instigates a Shutdown procedure see Section 3 5 page 11 Once a sample stream returns the analy...

Страница 11: ...in the sample and require periodic replacement Zero Calibration Solenoid Valve Cleaning Solution Solenoid Valve Constant head Units Multi stream versions To Drain Sample s Cleaning Solution Light Gre...

Страница 12: ...oes not change the upscale time is used The analyzer dead time the time between the stream valve energizing and the corresponding response on the analyzer display is approximately 12 minutes This dead...

Страница 13: ...stream is out of sample the duration between reading updates is the upscale sampling time If all streams are out of sample the analyzer shuts down automatically to prevent air being drawn into the an...

Страница 14: ...ion bottle and cap 1 x DataManager software CD Cable Gland Kit comprising 10 x two wire cable glands for relays or Profibus 1 x one wire cable gland for power 11 x nuts for above glands 11 x O rings f...

Страница 15: ...ccess and where short sample lines can be used Avoid rooms containing corrosive gases or vapors for example chlorination equipment or chlorine gas cylinders Select a location away from strong electric...

Страница 16: ...he front of the analyzer and install a protective cover not supplied over the reagent bottles Caution Do not place reagent bottles on the floor Dimensions in m ft Fig 4 2 Reagent Bottles Mounted Behin...

Страница 17: ...g 4 5 Mounting Dimensions 314 12 36 271 10 67 182 7 16 638 25 12 280 11 02 184 7 25 150 5 90 289 11 34 122 4 80 770 30 31 Reagent bottles mounted on optional bracket see Sections 4 4 1 4 4 2 and 4 4 3...

Страница 18: ...ig 4 5 page 15 The shelf can be attached through the back plate or either of the side plates Referring to Fig 4 7 1 Mark the wall using the dimensions shown or with the shelf supported carefully again...

Страница 19: ...ta CR2025 3V lithium cell must be carried out by an approved technician only The analyzer conforms to Installation Category II of IEC 61010 All connections to secondary circuits must have insulation t...

Страница 20: ...ce Relay Calibration Failed Relay Alarm 2 Relay Alarm 4 Relay Alarm 6 Relay NO C NC NO C NC NO C NC NO C NC NO C NC Out of Service Relay Calibration in Progress Relay Alarm 1 Relay Alarm 3 Relay Alarm...

Страница 21: ...ected to the correct terminals see Fig 4 8 page 18 8 Reconnect the terminal block plugs to the appropriate sockets on the application board 9 Tighten gland nut H for each connection made 10 If require...

Страница 22: ...s on or off the relay contacts can become eroded due to arcing Arcing also produces RFI that can cause analyzer malfunctions and incorrect readings To minimize the effects of RFI arc suppression compo...

Страница 23: ...kinks and is as short as possible Keep the tube s cut end in free space to eliminate the risk of air locks If an alternative contaminated drain tube is used refer to Fig 4 13 and route contaminated dr...

Страница 24: ...Navigation and Editing Depending on the type of field to be edited the software provides a variety of methods for entering values 5 2 1 Text Editing If the field to be edited requires text a keyboard...

Страница 25: ...required checkbox and press To finish highlight OK and press or press to exit without making any changes Slider Bars To select a value use the and keys to move the slider To finish press or press to e...

Страница 26: ...on Open a new configuration with the default settings see Note 1 Cancel and return to Operator level See Note 2 Note 1 If New Configuration or Open Configuration is selected and the modified configura...

Страница 27: ...of the operator views Up to 20 characters can be used The instrument analyzer tag is also displayed on the analyzer on configuration and audit log files Fields Description Screen saver wait time The...

Страница 28: ...e second Sunday in March and decremented automatically by 1 hour at 2 00 am on the first Sunday in November Auto Europe The start and end of the daylight saving period in Central Europe is calculated...

Страница 29: ...users to have password protected access to any of the Configuration Calibration Maintenance or Logging menus Each user can be assigned a unique 20 digit alphanumeric case sensitive password A minimum...

Страница 30: ...enter this password to gain access to the Calibration Maintenance and Logging menus The following tabs are displayed only if Security System is set to Advanced Reconfigure preset Passwords are set ini...

Страница 31: ...er s access levels and passwords If selected additional fields appear User X Name Where X is the user number 2 to 12 up to 20 characters can be used User X Access Where X is the user number 2 to 12 A...

Страница 32: ...onfiguration 30 IM NAV6P MS EN Rev F 5 3 6 Messages Fields Description Messages Up to 24 messages can be defined to indicate a particular event or action has occurred These are displayed on the chart...

Страница 33: ...to 50 C 98 to 122 F in 0 1 C 0 18 F increments The analyzer is optimized to run at a reaction temperature of 45 C 113 F Any changes to the reaction temperature may affect analyzer performance Any chan...

Страница 34: ...o 15 ppm Range High sets the high range value 0 to 15 ppm Fields Description Reagent Bottle Capacity The Reagent Bottle Capacity can be set between 0 1 and 10 0 liters This should be changed only if t...

Страница 35: ...ration Hysteresis Alarm Off Trip Point Alarm On Alarm Latched Alarm Off Alarm acknowledged by operator Earliest point that the alarm can be acknowledged Earliest point that the alarm can be acknowledg...

Страница 36: ...selected stream source Alarm Tag The Alarm identification tag up to 20 characters Trip The value at which the alarm is to activate 0 to 15 ppm Hysteresis When an alarm trip value is exceeded the alarm...

Страница 37: ...ntly 0 to 15 ppm If the difference between the zero and span is too small the output is very noisy Output Type The electrical high and low limits 0 to 22 mA For example if the output range is set to 0...

Страница 38: ...l memory and the SD card if fitted Fields Description Chart view enable The orientation and direction of the chart display Options are Horizontal Horizontal Vertical Chart annotation Enables chart ann...

Страница 39: ...enables At least one of these options must be selected for data to be archived automatically to an SD Card A dialog box is displayed showing the log files that are to be recorded Text format file con...

Страница 40: ...rated by a period Subnet mask The subnet mask is used to indicate which part of the IP address is for the network ID and which is for the host ID Set each section that is part of the network ID to 255...

Страница 41: ...sent includes a link to the analyzer s embedded web server enabling the analyzer s data and status to be viewed remotely using an internet browser on a PC Fields Description SMTP Server IP Address The...

Страница 42: ...l Test Settings button b Select Test Pumps and increase the sample pump speed to 5 rpm using the key pad c Exit the Test Pumps page and enter the Test Valves page d Select Cleaning ON to energize the...

Страница 43: ...ion being used 4 Start a Baseline Calibration The Baseline Calibration window is displayed Note Before starting the initial Baseline calibration it is important to check the reagent lines are fully pu...

Страница 44: ...y a a secondary calibration solution of a known concentration Fig 7 1 Calibration Maintenance Overview Fig 7 2 Calibration Progress Invalid Password Valid Password No Password Required Password Requir...

Страница 45: ...s so reproducible that this response can be compared to a theoretical response built into the analyzer The theoretical response has an ideal calibration factor of 1 0 If the response is not perfect co...

Страница 46: ...wetted reducing the effects of bubble formation due to sample and reagent degassing Cleaning can be initiated either manually or automatically at pre programmed intervals with an adjustable duration T...

Страница 47: ...are separated by 6 hours to ensure the best calibration accuracy this also applies to manually triggered functions Clean Frequency the frequency the analyzer is cleaned up to 4 weeks Next Clean if Cl...

Страница 48: ...culated and the Zero Offset is reset to 0 0 ppm A recovery period follows A baseline calibration must be performed when the reagents have been replaced or an annual service has been performed A progre...

Страница 49: ...the Material Safety Data Sheets prior to handling containers reservoirs and delivery systems that contain chemical reagents and standards Take care if cleaning any spillages and observe all relevant s...

Страница 50: ...e reagent bottles This is done either automatically by entering the solution replacement page or manually through the Manual Test Settings menu Fields Description Replace All Reagent Solutions Prompts...

Страница 51: ...p the new tubing into place Ensure the correct tubing is used for each pump and the seals are in place Wet the mating surfaces with demineralized water and squeeze between the two points shown below t...

Страница 52: ...e solution is flowing If there is air leaking into the filter housing tighten the filter cap onto the filter holder 8 2 2 Reagent Tube Filter Replacement Each reagent tube has an integral filter fitte...

Страница 53: ...o secure 8 4 Manual Test Settings This function is used to aid troubleshooting see Appendix C page 71 The analyzer is taken offline when Manual Test Settings are used On exiting Manual Test Settings i...

Страница 54: ...hiving see Section 9 2 page 54 Switches the removable media online offline Opens the file viewer see Section 9 3 page 54 On line help Appendix D page 75 Note ABB s DataManager software can be used to...

Страница 55: ...ed on an SD card is lost it can be re archived see Section 9 2 page 54 Data is copied to an SD card when required An SD card is inserted into the analyzer and a prompt is displayed asking the user to...

Страница 56: ...ected all data in the internal memory is re archived to external media To re archive data 1 Insert an SD card with sufficient free space into the analyzer 2 Select Off line in the menu 3 Select Reset...

Страница 57: ...Filenames Data files can be configured to contain data gathered over a predefined period of time New File Interval see Section 5 7 3 page 37 The Analyzer Tag is set in the configuration see Section 5...

Страница 58: ...r 2011 filename 26Oct11AW6SIL DS D00 Summertime ends at 3 00am on 26th October 2011 and the clock changes automatically to 2 00am The existing file is closed and a new file is created filename 26Oct11...

Страница 59: ...lternately the messages can be user defined Annotations can also be added remotely via the web see Appendix E page 76 The annotation is added to the chart at the time it is entered For example An entr...

Страница 60: ...ed stream is displayed sequentially The displayed scale is color coded to match the stream For example 10 6 Trace Select Selects the traces to display 11 Alarm Acknowledge To acknowledge a particular...

Страница 61: ...ibration the date of the last calibration and the scheduled date for the next see Section 7 4 page 45 Zero Offset a baseline calibration sets this offset to zero The result of a subsequent zero calibr...

Страница 62: ...S EN Rev F 12 4 Valves and Pumps Status Displays the status of the wet section valves and pumps 12 5 Statistics Displays the highest lowest and mean values of the sample streams since the analyzer was...

Страница 63: ...s Number 2 reagents 2 standard solution 1 cleaning solution Volume 2 5 l max per reagent 500 ml per standard solution 500 ml cleaning solution Reagent Consumption Continuous operation mode 2 5 l max p...

Страница 64: ...ld alarm relay Six per unit fully user assignable and alarm relays Rating Wetted Materials PMMA acrylic PP polypropylene PTFE PP 20 glass filled PEEK NBR nitrile EPDM Santoprene PTFE 15 polysulphane N...

Страница 65: ...the appropriate stock solution with high purity water to make the secondary calibration solution The dilution should be carried out using polyethylene apparatus wherever possible The stock solutions a...

Страница 66: ...can be used see Appendix A 3 2 A 3 1 Regular Cleaning Solution for Automatic Cleaning Operation 1 Dissolve 50 g of analytical grade sodium hydroxide pellets NaOH in approximately 600 ml of high purity...

Страница 67: ...led Relay Inhibits Monitor in Service The analyzer is operating correctly ON 20 Character User defined Alarm Tag User defined alarm message Media Card Full The SD card used for recording is full and a...

Страница 68: ...her too high or too low 1 Check the Electronics value displayed on the Measurement Status page within Diagnostic Information see Section 12 3 page 59 2 Check that the ambient temperature is within quo...

Страница 69: ...ration is performed If the message is displayed after the second zero calibration 1 Check the Audit Log to see if a baseline calibration was carried out after the reagents were replaced If not carry o...

Страница 70: ...riod OFF ON Scheduled calibrations and cleans In Manual Test Setting The analyzer has been taken off line while manual test settings are checked adjusted 1 Complete the manual test settings routine 2...

Страница 71: ...ning solution bottle is empty 1 Replace the cleaning solution 2 At the Calibration Maintenance level select Solution Replacement and at the Replace Cleaning Solution parameter press the key to confirm...

Страница 72: ...se the and keys to scroll through log data Icon Event Power failed Power restored Configuration changed File created File deleted Archive media inserted Archive media removed Archive media off line Ar...

Страница 73: ...ro and secondary calibration valves see Section C 3 4 page 74 Check mV values from the optical system see Section C 3 2 page 73 Failing calibration calibration parameters vary from one calibration to...

Страница 74: ...e sample filter assembly tighten if necessary b Check the solenoid valves and ensure the screws on the reverse side are tight 2 From the reagent line s a Check the pump tube connections b Check the re...

Страница 75: ...tion C 3 1 above If the problem persists perform a manual system clean see Section 7 4 page 45 Calibration failure or no response from optical system If there is no response or calibrations fail check...

Страница 76: ...tly To check flowrates 1 Remove the 2 reagent tubes from the reagent bottles 2 Increase the reagent pump speed to 10 rpm see Section 8 4 page 51 3 Check the air reagent interface is moving up each of...

Страница 77: ...e the and keys to select Help and press the key 2 Highlight a section icon If it changes to an icon there are help topics available press the key to open it If the section icon remains closed the sect...

Страница 78: ...oes not affect this view c Access Buttons provides access to the analyzer s data if the user has the appropriate access permission Stream Values see Appendix E 1 page 77 Reagent Solution Levels see Ap...

Страница 79: ...hosphate Multi stream Appendix E Web Server IM NAV6P MS EN Rev F 77 E 1 Stream Values E 2 Reagent Solution Levels E 3 Measurement Status E 4 Valve Pump Status E 5 Statistics E 6 System Information E 7...

Страница 80: ...see Section 5 8 1 page 38 2 Type either the message or an instruction only one field can be populated at any one time 3 Click the button to send the message or instruction to the analyzer E 9 Configur...

Страница 81: ...all icon large icon list or details by selecting the appropriate option from the Views menu 5 Files Folders can be copied to from the analyzer E 12 FTP Access via DataManager DataManager can be used w...

Страница 82: ...ds followed by an ABB splash screen 7 A Warning screen appears next This provides the option to upgrade the existing system software or exit without upgrading 8 To proceed press the key 9 The Commissi...

Страница 83: ...e unit Offline b go to Test Valves and set Sec Cal Value On by pressing Enter c exit this section by selecting TEST mode not NORMAL 4 Measure the sample a leave the sample flowing for at least 20 minu...

Страница 84: ...ers with upgraded pumps and instruments manufactured after October 2010 AW602100 Tubing kit excluding pump tubes AW600096 Pump tube blue green see AW601108 and AW602108 AW600097 Pump tube grey see AW6...

Страница 85: ...at switch level sensor red AW600726 Float switch level sensor grey Part No Description AW600727 Float switch level sensor yellow AW600025 Primary debubbler AW600034 Calibration clean sample select val...

Страница 86: ...stant head assy multi stream right hand side end module AW602112 Reaction coil manifold cover AW600730 Bottle empty cleaning solution secondary calibration zero calibration AW600731 Bottle empty reduc...

Страница 87: ...onnection PCB AW600051 AC power supply AW600056 DC power supply AW600065 Transmitter application board AW600067 Profibus board Part No Description AW600028 AC Transmitter excluding Profibus card AW600...

Страница 88: ...E Editing 22 Email 39 Ethernet 38 F Fail safe 34 File viewer 54 Filters 50 Flow schematic 8 Front panel controls 22 H Historical review 57 Hysteresis 34 I Illustrated spares list 82 Inactive user disa...

Страница 89: ...r wait time 25 SD Card 53 Security 27 Security type 28 Shutdown Automatic 11 Software Updating 80 Solution levels 59 Solutions 47 63 Spares Illustrated spares list 82 Statistics 60 Status Measurement...

Страница 90: ...Navigator 600 Phosphate Multi stream Index 88 IM NAV6P MS EN Rev F...

Страница 91: ...S DOS Excel and Internet Explorer are registered trademarks of Microsoft Corporation in the United States and or other countries PROFIBUS is a registered trademark of PROFIBUS and PROFINET Internation...

Страница 92: ...document and in the subject matter and illustrations contained therein Any reproduction disclosure to third parties or utilization of its contents in whole or in parts is forbidden without prior writ...

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