Thermo Electron 3-Star Conductivity User Manual Download Page 109

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Chapter XII

Declaration of Conformity

Manufacturer:

Thermo Electron

Address:

166 Cummings Center
Beverly, Ma 01915
USA

The above named Manufacturer hereby declares that the product(s) described below
conforms to the Standards and Directives listed below:

5-Star pH/ISE/Cond/DO benchtop

5-Star pH/Cond/DO portable

4-Star pH/ Cond benchtop

4-Star pH/ Cond portable

4-Star pH/ DO benchtop

4-Star pH/ DO portable

4-Star pH/ ISE benchtop

4-Star pH/ ISE portable

3-Star Cond benchtop

3-Star Cond portable

3-Star DO benchtop

3-Star DO portable

3-Star pH Benchtop

3-Star pH portable

Directive / Standard:

89/336/EEC Electromagnetic Compatibility (EMC) Directive

EN 61326:1997 + A1:1998 + A2:2001, Electrical equipment for measurement,
control and laboratory use: EMC-requirements for measurement device
per Annex D.

XII-1

Orion Star Series Meter

Thermo Electron Corporation

Summary of Contents for 3-Star Conductivity

Page 1: ...Orion Star Series Meter User s Guide Analyze Detect Measure Control ...

Page 2: ...pHuture Triode Quatrode QuiKcheK rf link ROSS ROSS Resolution SAOB SMART AVERAGING Smart CheK SMART STABILITY Stacked Stat Face The Enhanced Lab ThermaSense Triode TRIUMpH Unbreakable pH Universal Access are trademarks of Thermo Guaranteed Success and The Technical Edge are service marks of Thermo PerpHecT meters are protected by U S patent 6 168 707 PerpHecT ROSS are protected by U S patent 6 168...

Page 3: ...er adapter II 1 Connecting the electrodes II 2 Turning on the Instrument II 3 Replacing the batteries II 4 Chapter III Operational Overview III 1 Display deﬁnitions III 1 Keypad functions III 3 Set up Menus navigation III 4 Calibration III 8 Measurement III 9 Chapter IV pH IV 1 Set up IV 1 Calibration IV 3 Measurement IV 5 Chapter V ISE V 1 Set up V 1 Calibration V 4 Measurement V 7 Chapter VI mV ...

Page 4: ...s IX 1 Automatic shutoff IX 1 Display backlight IX 1 AUTO READ IX 1 Stirrer control IX 2 Methods and passwords IX 2 Calibration alarm IX 3 Datalog setup IX 7 General instrument setup IX 9 GLP instrument setup IX 12 Time and Date setup IX 15 RS 232 instrument setup IX 19 Multiparameter printout IX 21 Log View IX 22 Error Codes and Debugging IX 23 Chapter X Speciﬁcations X 1 Chapter XI Terms and Con...

Page 5: ...remote control 21 CFR software package manual and other advanced capabilities Our website also has an updated list of application notes developed specifically for the Star series meter line Orion Star Series Quick Start Guide Star series Quick Start guide is designed to get user s up and running in a few minutes with basic calibration and measurement information You can contact the Thermo Water An...

Page 6: ...he benchtop meters carry a IP54 dustproof and splash proof rating and can easily be cleaned using a damp cloth water with a mild detergent The portable meters are constructed for use outdoors with a IP67 waterproof rating they can float and be submersed for a short period of time without any negative effect on their operation Any use outside of these instructions could invalidate your warranty cau...

Page 7: ...he top line and the current units are pH will start a pH calibration Each time is pressed in the calibration it will accept the current point value and move to the next cal pt until the max of cal pts are performed then it will return to measurement mode Print Log a measurement in continuous or timed measurement mode Prints Logs Freezes screen when the reading becomes stable Exits SETUP and return...

Page 8: ...r232 Log log delete on downloading or log roll over LOg General Instrument Setup gEn GLP Turns ON OFF Methods Password Protection gLP To select the General Instrument setup option line Middle Line Returns to measurement mode Stirrer jack stirrer or DO Auto stir probe Reference pH or ISE Cond ATC 8 pin DO 9 pin Ground BNC Power RS232 Rear View of Meter Electrode Connections ...

Page 9: ...ation Setup and Measurement pH ISE Conductivity Calibration Screen for 1 5 Points Accepts Autobuffer recognition as a 1 pt calibration starts the 2nd cal pt if pressed again To edit the value for a manual buffer entry Accepts Autobuffer recognition and returns to measurement mode DO Calibration AIr Water Saturated Air H2O Air Saturated Water mAn Winkler Manual SEt0 Zero Auto Read pH ISE ORP units ...

Page 10: ...s Returns to measurement mode pH Setup Menu Screen Selects pH setup rES Resolution bUF Auto Buffer Set USA or EUrO Selects the pH Resolution entry line Bottom Line Returns to measurement mode ISE Setup Menu Screen Selects ISE setup rES Resolution UnIt ISE Measurement units rAng ISE Measurement range nLIn Non linear Blank Correction Selects ISE Resolution entry line Bottom Line Returns to measureme...

Page 11: ...t Saturation Resolution SAt rES Concentration Resolution mg L bAr Barometric pressure compensation type Auto Manual PrES Manual Barometric Pressure Entry Only shown if manual pressure compensation is selected SAL Salinity correction factor type Auto Manual SALF Manual salinity correction factor Only shown if manual salinity correction factor CALt DO calibration type Air Water Manual SEtO Selects P...

Page 12: ...f Bottom Line Returns to measurement mode Date Time Setup Menu Screen Selects the Date Time setup HOUr Enter the Hour in 24 hr format mIn Enter minutes 0 59 tyPE US or European Style Month Day Year or Day Month Year yEAr Enter the Year dAtE Enter the Month dAy Enter the day Selects Hour entry line Bottom Line Returns to measurement mode RS232 Setup Menu Screen Selects RS232 setup bAUd Baud Rate 12...

Page 13: ...r Adapter for benchtop meters only Carefully remove the components of white power adapter box The universal power supply has three plugs to be use for 110V 220V and 240V wall plugs Select the plug that is appropriate for your power source and slide it into the grooves on the adapter A click will be heard when the plug is properly in place in the adapter The external electrical power supplies are r...

Page 14: ...s on the meter Review the attached diagram Depending on the functions on the meter you purchased some of these connectors may not be on your meter Benchtop Meter Electrode Connections Portable Meter Electrode Connections Stirrer jack stirrer or DO Auto stir probe Reference pH or ISE Cond ATC 8 pin DO 9 pin Ground BNC Power RS232 RS232 BNC Cond ATC 8 pin DO 9 pin ...

Page 15: ...the BNC connector Non glass ISFET pHuture MMS sensors for pH ORP and temperature use the waterproof 9 pin MiniDIN connector The pH ORP conductivity and temperature Pentrode 6175MD uses both the waterproof 9 pin MiniDIN and waterproof 8 pin MiniDIN connectors Turning On the Instrument With the batteries installed in the portable meters or either the batteries installed or line power attached to the...

Page 16: ...thin 20 hours Note The instrument uses four AA Alkaline Batteries Do not use lithium or rechargeable batteries Improper installation of non alkaline batteries could create a hazard To access the Benchtop Meter Battery Door Note Stored data calibrations and methods will remain in nonvolatile memory so data is saved while batteries are changed 1 Turn the meter off 2 Place it upside down gently on a ...

Page 17: ...e One of the batteries has the positive top inserted at the spring end of the battery compartment This is the correct orientation 6 Replace the cover 7 Turn the meter power on 8 If the batteries took more than a minute to replace you may want to update the time date by pressing the setup key to reset the time and date 9 Dispose of the used alkaline batteries in accordance with local regulations ...

Page 18: ...nd will not come out With these loose lift the bottom back of the meter to expose the batteries Install the batteries in the orientation shown in the graphics of the battery compartment Note The instrument uses four AA Alkaline Batteries Do not use lithium or rechargeable batteries Improper installation of non alkaline batteries could create a hazard Note After a battery change the real time clock...

Page 19: ...ill float for short periods of time After being submersed the meters should be cleaned with a mild detergent solution for the protection of future users Approved Operating Conditions The Star Series Meters are designed to operate according to their specifications under the following conditions Portable and Bench top Meters Environmental Conditions Ambient Operating Temperature 5 to 45 C Relative H...

Page 20: ...Thermo Electron Corporation II 8 Orion Star Series Meter ...

Page 21: ...etric Pressure a On the left of the screen are arrows that indicate the currently selected line b The right of the screen shows the measurement units for the selected measurement modes The units will flash until the reading is stable c nLF icon indicates that non linear temp comp is active for conductivity d The graph indicates Calibration mode or calibration setup Auto Read pH ISE ORP units Condu...

Page 22: ...s lit g The numbers on the top indicate which pH Auto buffers were used in the last calibration h The Caution symbol indicates an error condition or when shown with the probe that a sensor quality issue exists i The AR icon indicates the meter is in AUTO READ mode j The printer icon indicates the meter is printing exporting or logging data 3 4 Star Meter Display Auto Read pH ISE ORP units Conducti...

Page 23: ...ill turn the meter on b If the meter is on a quick press of the power key will toggle the backlight on off c If the meter is on holding down the power key will turn off the meter 2 The LINE SELECTION key switches the arrow on the left of the screen between the 3 display lines to select the line to edit Power Back Light Measure Save Print View Log Line Select Digits Setup Calibrate Scroll Up Scroll...

Page 24: ...d Screens 6 The CALIBRATE key starts a Calibration for the currently selected line and measurement mode g So if the Arrow is pointed to line 1 Top Line and the current units on that line is pH then pressing the CALIBRATE key will start a pH Calibration h Each time the CALIBRATE key is pressed in the calibration it will accept the current point calibration value and move to the next calibration poi...

Page 25: ...ode when in setup m Will accept the Calibration point and return to measurement mode when in Calibration Benchtop Meters The benchtop meters have an additional key On all Benchtop meters there is a 10th key for turning on off the STIRRER In AUTO READ mode the MEASURE key will also turn the stirrer on off automatically during the measurement This feature is not available on portable meters Stirrer ...

Page 26: ... key will enter the SETUP menu starting with the SETUP for the currently selected line and measurement mode So if the Arrow is pointed to line 1 Top Line and the current units on that line is ISE then pressing the SETUP key will enter the ISE setup screen How to Navigate the Setup Menus Press the UP DOWN arrow to scroll through the Setup Menu s until the Setup Menu you want Grayed Text in Center C...

Page 27: ...mp Coefﬁcient COEF 0 0 10 0 2 1 Enable Methods Set OFF On TDS Factor tdSF 0 00 10 0 0 49 Enable Set Password PASS 0000 9999 AutoCal Cell Constant CELL 0 001 199 0 0 475 Time Date dAtE Options Reference Temp trEF 15 20 25 Hour Setting HOUr 00 23 12 Cell Type Ranging tyPE PLnr Std 1 2 3 4 5 6 7 Minute Setting tInE 00 59 Dissolved Oxygen DO Options Date Format tyPE mdy dmy Sat Resolution rES 1 0 1 Ye...

Page 28: ...eral Navigation for Selecting Calibration to be Performed 1 In measurement mode press the RIGHT ARROW key until the arrow on the left of the screen is pointed toward the measurement line associated with the measurement your calibrating pH ORP ISE Top Line Conductivity Middle Line DO Bottom Line 2 Press the UP or DOWN scroll key until the appropriate measurement icon is lit for the measurement you ...

Page 29: ...e UP or DOWN arrow keys to change the measurement mode of the selected line This can also be used to turn off this measurement line Press the RIGHT arrow key to move the arrow selecting the line to the next line Mode Selections Top Line pH mV Rel mV ISE Off Middle Line µS cm or mS cm for conductivity mg L for TDS ppt for Salinity MegOhms cm for resistivity Off Bottom Line Sat for DO percent satura...

Page 30: ... making measurements and updating the screen To print Log the measurement in this mode press the MEASURE key In Timed mode the instrument is constantly making measurements and updating the display but it prints logs the data at the selected time interval In AUTO READ mode the instrument starts a measurement whenever the MEASURE key is pressed Once the reading becomes stable it auatomatically print...

Page 31: ...o change the digit to be scrolled Press the RIGHT Arrow key to move to enter setup Press the MEASURE key to exit to measurement mode Press the UP DOWN arrow to scroll through the Setup Menu until rEAd is displayed on the Top line Press the RIGHT ARROW key to select the rEAd setup option line Middle Line Press the MEASURE key to return to measurement mode Measurement Setup Option Menu Screen Press ...

Page 32: ...nu Screen This screen will only appear when timed readings have been selected for the measurement type Enter the Minutes Seconds between timed readings by Pressing the UP DOWN arrow keys to change the value of the flashing digit Press the DECIMAL DIGIT key to change the digit to be scrolled 00 05 to 99 59 Press the RIGHT ARROW key to accept the selection and select the Measurement Setup Menu line ...

Page 33: ...n will appear when setup is pressed Press the UP DOWN arrows to select the Method to be used or edited Press the SETUP or RIGHT arrow key to edit the selected method b If a password has been setup then the password entry screen will appear and a password will need to be entered to enter setup and edit the method Press the UP DOWN arrow keys to change the value of the flashing digit Press the DECIM...

Page 34: ...e Press the MEASURE key to return to measurement mode pH Resolution Selection Menu Screen Press the UP DOWN arrow to select the pH resolution options as listed below 0 001 0 01 or 0 1 Press the RIGHT ARROW key to accept the selection and select the pH Setup Menu line Top Line Press the MEASURE key to return to measurement mode pH Auto Buffer Set Selection Menu Screen Press the UP DOWN arrow to sel...

Page 35: ...t at least a two point calibration should be performed before the first samples of the day are analyzed and a single point calibration should be performed every two hours Fresh buffers should be used each time you calibrate Care should be taken when rinsing the electrode with deionized water and GENTLY BLOTTING all remaining water drops with a lint free tissue prior to moving the electrode to the ...

Page 36: ...easurement mode 2 Press the CALIBRATE key to accept Autobuffer recognition as the 1st calibration point start the 2nd calibration point when prompted for the next buffer 3 Use the UP DOWN arrow keys and the DIGIT DECIMAL keys to edit the value for a manual buffer entry Then follow step 1 or 2 4 Continue measuring for each calibration point rinsing the electrode between each buffer until the desire...

Page 37: ...ng the stirrer from the sample b If you are in AUTO READ mode then press the MEASURE key to start the measurement Once the ready is stable the meter will automatically Log Print the results and freeze the display If the stirrer is enabled then the stirrer will turn on when the MEASURE key is pressed and turn off once the reading has stabilized With the AutoStir BOD Probe pressing the button on the...

Page 38: ...Thermo Electron Corporation IV 6 Orion Star Series Meter ...

Page 39: ...uring ISE Calibration HIgH Yes ISE Auto Blank Correction ISE nLIn AUtO AUtO OFF Enables or Disables Calibration Auto Blank AUtO Yes ISE Resolutions This selects the number of significant digits displayed in measurement mode In addition the resolution selection is used by SMART STABILITY SMART AVERAGING algorithms to optimize the accuracy precision and response of the ISE measurement ISE Units This...

Page 40: ... the user can choose the turn the Auto blank correction OFF How to Change the ISE Setup Options To access the ISE Setup Menu From the Measurement Screen press the SETUP key a If methods have been turned on then the Method selection screen will appear when setup is pressed Press the UP DOWN arrows to select the Method to be used or edited Press the SETUP or RIGHT arrow key to edit the selected meth...

Page 41: ...ion Selection Menu Screen Press the UP DOWN arrow to select the ISE resolution Sig Digits Options as listed below 1 2 or 3 Press the RIGHT ARROW key to accept the selection and select the ISE Setup Menu line Top Line Press the MEASURE key to return to measurement mode ISE Measurement Units Selection Menu Screen Press the UP DOWN arrow to select the ISE measurement units as listed below m Molar mgL...

Page 42: ...IGHT ARROW key to accept the selection and select the ISE Setup Menu line Top Line Press the MEASURE key to return to measurement mode ISE Calibration for 1 5 Points 1 Prepare the electrode and standards for use according to the instructions received with the electrode 2 The standards should be prepared in the same ISE units as required by the sample results It is preferable to use serial dilution...

Page 43: ...issue to remove water drops before moving the electrode to the next beaker Continue from the next lowest concentration up to the highest point to reduce the potential effects of carryover Note For greater low level measurement accuracy a new low level ISE calibration option is available An additional rinse of the electrode with the next standard or sample solution is recommended for any low level ...

Page 44: ...rn to the measurement mode If you are doing a manual calibration go above to step 4 to edit the value of your manual standard entry Note Before returning to measurement mode the slope will be displayed For a 2 or more point calibration it will automatically proceed to measurement mode after 3 seconds On a 1 point calibration it will allow you to edit the slope then press the MEASURE key to proceed...

Page 45: ...rner of the display ISE Measurement After calibrating the electrode the meter is ready to start making measurements Make sure that the instrument is in measurement mode the probe icon is lit and that the ISE icon is lit If the probe icon is not lit press the MEASURE key to return to measurement mode If the ISE icon is not lit press the RIGHT ARROW key until the arrow on the left of the display is ...

Page 46: ...er will start making measurements as soon as it goes into measurement mode at the frequency set in setup It will automatically Log Print each measurement If you are using the benchtop meter the stirrer control is enabled then pressing the STIRRER button will start the stirrer Pressing the stirrer button again will turn off the stirrer 3 Remove the electrode from the sample and rinse with deionized...

Page 47: ... icon lights 4 Press CALIBRATE key 5 When the electrode is stable the RmV icon will stop flashing and the temperature corrected value for the Standard Hydrogen Electrode value for Orion ORP standard 967901 or 967961 will be displayed 6 Press CALIBRATE or MEASURE key to accept the standard value and return to measurement mode If performing a manual calibration use the UP DOWN arrow keys and the DIG...

Page 48: ...e the instrument will start measuring immediately If you are using the benchtop meter the stirrer control is enabled then pressing the STIRRER button will start the stirrer The mV icon will flash until the ready is stable Once the ready is stable you can Log Print the measurement by pressing the MEASURE key If the sitirrer is on press the stirrer button to turn off the stirrer before removing the ...

Page 49: ... the top line Then press the UP arrow key until the Rel mV icon lights You are now ready to start measuring 1 Rinse the electrode in deionized water 2 Place the electrode in your sample a If you are in continuous measurement mode the instrument will start measuring immediately If you are using the benchtop meter the stirrer control is enabled then pressing the STIRRER button will start the stirrer...

Page 50: ... you are using the benchtop meter the stirrer control is enabled then pressing the STIRRER button will start the stirrer Pressing the stirrer button again will turn off the stirrer 3 Remove the electrode from the sample and rinse with deionized water then place it in your next sample and repeat step 2 4 Once your finished measuring samples rinse the electrode with deionized water and blot dry Then...

Page 51: ... TDS factor 0 49 Yes Conductivity Auto Calibration Default Cell Constant Setting Cond CELL 0 475 0 001 199 0 Cell Constant used for Cond Auto Standard 0 475 Yes Conductivity Temperature Reference Selection Cond trEF 25 15 20 25 Conductivity Reference Temperature 25 Yes Conductivity Cell Type Manual Ranging Selection Cond tyPE PLnr PLnr Std 1 2 3 4 5 6 7 Standard Planer Cond Cell Or sets Manual ran...

Page 52: ... of Conductivity per ûC Solution C Ultrapure Water 4 55 Salt NaCl Solutions 2 12 5 NaOH 1 72 Dilute Ammonia 1 88 10 HCl 1 32 5 Sulfuric Acid 0 96 98 Sulfuric Acid 2 84 Sugar Syrup 5 64 ConductivityTDS Factor Total Dissolved Solids TDS refers to the dissolved inorganics in a solution These dissolved inorganics will carry a current and will be reflected as a conductivity reading Since a relationship...

Page 53: ...conductivity standards 1413 μS cm 100 μS cm and 12 9 mS cm ConductivityTemperature Reference By definition temperature compensated conductivity of a solution is the conductivity which that solution exhibits at the reference temperature The temperature is chosen to be either 25 C 20 C or 15 C A measurement made at the reference temperature needs no compensation The closer the sample is to the refer...

Page 54: ... MEASURE key to return to measurement mode Temperature Compensation Selection Menu Screen Press the UP DOWN arrow to select the Conductivity Temperture compensation selection as listed below OFF No temperature compensation LIn Linear temperature compensation nLF Natural Water Non Linear Temperature Compensation Press the RIGHT ARROW key to accept the selection and select the Conductivity Setup Men...

Page 55: ...nge the value of the flashing digit Press the DECIMAL DIGIT key to change the digit to be scrolled and the place of the decimal poit 0 001 to 199 0 Press the RIGHT ARROW key to accept the selection and select the Conductivity Setup Menu line Top Line Press the MEASURE key to return to measurement mode Temperature Compensation Selection Menu Screen Press the UP DOWN arrow to select the Conductivity...

Page 56: ...If methods have been turned on then the Method selection screen will appear when setup is pressed Press the UP DOWN arrows to select the Method to be used or edited Press the SETUP or RIGHT arrow key to edit the selected method b If a password has been setup then the password entry screen will appear and a password will need to be entered to enter setup and edit the method Press the UP DOWN arrow ...

Page 57: ...e arrow pointed at the conductivity line press the Calibrate key 6 The screen will display the cell constant on the Top line and the conductivity on the middle line To perform a manual calibration use the UP DOWN arrow keys to change the value of the flashing digit on the cell constant Press the DECIMAL DIGIT key to change the digit to be scrolled Edit the cell constant until the conductivity meas...

Page 58: ...last calibration point press the MEASURE key instead pf the CALIBRATE key to accept the value and return to the measurement mode 10 Repeat steps 5 and 6 for each standard 11 After the standard value for the last standard has been entered the cell constant will be displayed automatically CELL appears in the lower field while the actual CELL constant appears in the main field Then the meter automati...

Page 59: ...Ar AUtO AUtO mAn Selects Internal Barometer or Manual Pressure AUtO Yes Dissolved Oxygen Manual Barometric Pressure Setting DO PrES 760 0 450 0 850 2 Manual Pressure Compensation Value 760 0 Yes Dissolved Oxygen Salinity Correction Selection DO SAL AUtO AUtO mAn Selects Method of Salinity Correction Meters w Cond Only AUtO Yes Dissolved Oxygen Manual Salinity Correction Factor DO SALF 0 0 2 45 Man...

Page 60: ...e probe is exposed to higher pressures then the meter DO Manual Pressure Setting This screen will only appear if Manual Barometric Pressure compensation has been selected This is where you enter the pressure to use for pressure compensating the DO measurement The pressure in entered in mm of Hg Mercury See the following table to convert from other units of pressure hPa mBar mm Hg torr Inches Hg lb...

Page 61: ...32 22 54 40 18 12 33 23 56 42 19 13 34 24 Salinity depending on the conductivity at 20 C ppt Parts per Thousand Salinity This table was calculated from the International Oceanographic Tables International Oceanographic Tables Vol 1 National Institute of Oceanography of Great Britian Womley Godaming Surrey England and Unesco Paris 1971 DO CalibrationType This allows you to select the type of DO cal...

Page 62: ...to change the digit to be scrolled Press the RIGHT Arrow key to move to enter setup Press the MEASURE key to exit to measurement mode Press the UP DOWN arrow to scroll through the Setup Menu s until DO is displayed on the Top line Press the LINE SELECT key to select the DO setup option line Middle Line Press the MEASURE key to return to measurement mode DO Setup Option Menu Screen Press the UP DOW...

Page 63: ...elect the DO resolution options as listed below 0 1 or 0 01 Press the LINE SELECT key to accept the selection and select the DO Setup Menu line Top Line Press the MEASURE key to return to measurement mode Pressure Compensation Selection Menu Screen Press the UP DOWN arrow to select the DO resolution options as listed below AOtO Automatic Press Comp using the Internal Barometer mAn Manual Press Com...

Page 64: ...nt mode Manual Salinity Correction Setting Menu Screen Press the UP DOWN arrow keys to change the value of the flashing digit Press the DECIMAL DIGIT key to change the digit to be scrolled 0 2 to 45 Press the RIGHT ARROW key to accept the selection and select the DO Setup Menu line Top Line Press the MEASURE key to return to measurement mode Calibration Type Selection Menu Screen Press the UP DOWN...

Page 65: ...bove but not into the sponge This water saturated air has 100 humidity and is a standard for calibration For BOD measurements this calibration can be performed in a BOD bottle An air saturated water calibrated probe can be used for measurement of dissolved oxygen in water For low oxygen levels a second zero calibration point is often required although some probes generate zero current at zero oxyg...

Page 66: ... mg L a zero calibration should be performed Probe Polarization The dissolved oxygen probe are continuously polarized when they are connected to the meter But when first connected to the meter or has been unplugged from the meter for more then an hour it needs to be given 30 to 60 minutes to polarize the probe Interrupted connections of less then an hour will take 5 25 minutes for the readings to ...

Page 67: ...ibration Note The probe and calibration standard water saturated air or air saturated water should be allowed to reach equilibrium before the system is calibrated If a polarographic probe is used it is also important to allow sufficient time at least 30 to 50 minutes for the system to polarize Air Calibration AutoCal using water saturated air as the calibration standard The default calibration mod...

Page 68: ... for three seconds The meter will return to measure mode A standard 300 mL BOD bottle may also be use for AIR calibration Fill the bottom of the bottle with 50 mL of distilled water Be sure to use the BOD funnel accessory Orion Cat Nos 080044 or 080160 depending on the probe in use Place the probe into the funnel so that it is just above the stirring paddle Ensure that there are no drops of water ...

Page 69: ...re immersed Ensure that there are no air bubbles accumulating on the membrane 3 To initiate the Water calibration press the CALIBRATE key The cal indicator will light up and the current slope SLP will be displayed briefly with the calibration type 4 While the electrode signal is stabilizing the meter will flash a dissolved oxygen reading based upon the current calibration data in the main field On...

Page 70: ...ter will flash a dissolved oxygen reading based upon the current calibration data in the main field Once the input has stabilized the concentration value which corresponds to saturation at the current temperature pressure and salinity will be displayed 4 The concentration value should then be adjusted using the UP DOWN arrow DECIMAL DIGIT keys to the value that was obtained via the Winkler titrati...

Page 71: ... a magnetic stirrer stir gently 5 Allow the solution to eliminate all oxygen from the membrane module This should take at least 5 minutes 6 To initiate the Probe Zero calibration press the CALIBRATE key The cal indicator will light up and the current slope SLP will be displayed briefly with the calibration type 7 While the electrode signal is stabilizing the meter will flash a dissolved oxygen rea...

Page 72: ...Thermo Electron Corporation VIII 14 Orion Star Series Meter ...

Page 73: ...s of the power key will toggle the backlight on off On the portable meters and the benchtop meters when on battery power the backlight will automatically turn off after 2 minutes to conserve battery power When line power is attached to the benchtop meter the the backlight will remain on until turned off AUTO READ If you are in AUTO READ mode then press the MEASURE key to start the measurement Once...

Page 74: ...be pressing the MEASURE key will start the AUTO READ measurement and stirring Methods If methods have been turned on then this screen will appear when setup is pressed Press the UP DOWN arrows to select the Method to be used or edited Press the MEASURE button to implement the selected method and return to measurement mode Press the SETUP or RIGHT arrow key to edit the selected method Up to 10 meth...

Page 75: ...issolved Oxygen Calibration Alarm Setting dUE COnd 0 0000 9999 Time in Hours 0000 Cal Alarm Off 0000 Yes pH Calibration Alarm Setting This selects the time in hours after a calibration before the meter will remind you that the pH needs to be recalibrated It will provide this warning by lighting the Caution icon and flashing the Probe icon In addition the units icon for pH will flash about once eve...

Page 76: ...ed It will provide this warning by lighting the Caution icon and flashing the Probe icon In addition the Sat or mg L icon will flash about once every 5 seconds A setting of 0000 turns off the calibration alarm How to Change the Cal Alarm Setup Options To access the Cal Alarm Setup Menu From the Measurement Screen press the SETUP key a If methods have been turned on then the Method selection screen...

Page 77: ...o change the value of the flashing digit Press the DECIMAL DIGIT key to change the digit to be scrolled 0000 to 9999 where 0000 turns the calibration alarm off Press the RIGHT ARROW key to accept the selection and select the Cal Alarm Setup Menu line Top Line Press the MEASURE key to return to measurement mode ORP Calibration Alarm Setting Menu Screen Scroll in the number of hours between calibrat...

Page 78: ... calibrations Press the UP DOWN arrow keys to change the value of the flashing digit Press the DECIMAL DIGIT key to change the digit to be scrolled 0000 to 9999 where 0000 turns the calibration alarm off Press the RIGHT ARROW key to accept the selection and select the Cal Alarm Setup Menu line Top Line Press the MEASURE key to return to measurement mode Dissolved Oxygen Calibration Alarm Setting M...

Page 79: ...re filled To continue datalogging you must download the data to a printer or computer If No is selected when all 200 datalog points are filled it will start overwriting the datalog starting at point 1 How to Change the Datalog Setup Option To access the Datalog Setup Menu From the Measurement Screen press the SETUP key a If methods have been turned on then the Method selection screen will appear w...

Page 80: ...t mode Datalog Setup Option Menu Screen Press the RIGHT ARROW key to select the option editing line Bottom Line Press the MEASURE key to return to measurement mode Datalog Auto Delete Selection Menu Screen Press the UP DOWN arrow to select the Measurement Type options as listed below yES Automatic log delete after download nO Roll over log when full Press the RIGHT ARROW key to accept the selectio...

Page 81: ...d Setting This screen is only present on the Benchtop meters It is used to set the stirrer speed The speeds are 1 through 7 with speed 1 being the slowest qand speed 7 being the fastest We generally recommend a speed of 3 or 4 for most applications When a stirrer speed is selected In continuous or timed reading mode the stirrer is toggled on and off with the stirrer button In AUTO READ mode pressi...

Page 82: ... edited Press the SETUP or RIGHT arrow key to edit the selected method b If a password has been setup then the password entry screen will appear and a password will need to be entered to enter setup and edit the method Press the UP DOWN arrow keys to change the value of the flashing digit Press the DECIMAL DIGIT key to change the digit to be scrolled Press the RIGHT Arrow key to move to enter setu...

Page 83: ...MEASURE key to return to measurement mode Stirrer Speed Selection Setting Menu Screen Press the UP DOWN arrow to select the Stirrer options as listed below OFF Disables the stirrer 1 Slowest Speed 2 2nd Speed 3 3rd Speed 4 4th Speed 5 4th Speed 6 6th Speed 7 Fastest Speed Press the RIGHT ARROW key to accept the selection and select the General Setup Menu line Top Line Press the MEASURE key to retu...

Page 84: ...ods can be selected created or edits or just the current method The default current method is method 1 a If methods have been turned on then the Method selection screen will appear when setup is pressed Press the UP DOWN arrows to select the Method to be used or edited Press the SETUP or RIGHT arrow key to edit the selected method Password Setup This allows the user to Enable and setup a password ...

Page 85: ...the selected method b If a password has been setup then the password entry screen will appear and a password will need to be entered to enter setup and edit the method Press the UP DOWN arrow keys to change the value of the flashing digit Press the DECIMAL DIGIT key to change the digit to be scrolled Press the RIGHT Arrow key to move to enter setup Press the MEASURE key to exit to measurement mode...

Page 86: ... DOWN arrow to select the Stirrer options as listed below OFF Disables Methods On Enables Methods Press the RIGHT ARROW key to accept the selection and select the GLP Setup Menu line Top Line Press the MEASURE key to return to measurement mode Password Setting Menu Screen Set the Password by Pressing the UP DOWN arrow keys to change the value of the flashing digit Press the DECIMAL DIGIT key to ch...

Page 87: ...y dmy Month Day Year or Day Month Year Selection mdy Yes Date Year Setting dAtE yEAr 2004 00 99 Sets the year for the current date from 2000 to2099 04 Yes Date Month Setting dAtE dAtE mm01 01 12 Month Setting 01 Jan Thru 12 Dec 01 Yes Date Day of the Month Setting dAtE dAy dd01 01 31 Day of the Month 01 Yes Time Hour Setting This is to set the Hour of the current time in 24 hour Military Time form...

Page 88: ... has been setup then the password entry screen will appear and a password will need to be entered to enter setup and edit the method Press the UP DOWN arrow keys to change the value of the flashing digit Press the DECIMAL DIGIT key to change the digit to be scrolled Press the RIGHT Arrow key to move to enter setup Press the MEASURE key to exit to measurement mode Press the UP DOWN arrow to scroll ...

Page 89: ...RE key to return to measurement mode Minute Setting Menu Screen Enter the Minutes of the current time by Pressing the UP DOWN arrow keys to change the value of the flashing digit Press the DECIMAL DIGIT key to change the digit to be scrolled 00 to 59 Press the RIGHT ARROW key to accept the selection and select the Time Date Setup Menu line Top Line Press the MEASURE key to return to measurement mo...

Page 90: ...nth of the current date by Pressing the UP DOWN arrow keys to change the value of the flashing digit Press the DECIMAL DIGIT key to change the digit to be scrolled 00 to 12 Press the RIGHT ARROW key to accept the selection and select the Time Date Setup Menu line Top Line Press the MEASURE key to return to measurement mode Day Setting Menu Screen Enter the Day of the current month by Pressing the ...

Page 91: ... comma delimited output for direct interfacing to LIM s systems Excel or data analysis software How to Change the General Instrument Setup Options To access the RS 232 Instrument Setup Menu From the Measurement Screen press the SETUP key a If methods have been turned on then the Method selection screen will appear when setup is pressed Press the UP DOWN arrows to select the Method to be used or ed...

Page 92: ...the RIGHT ARROW key to select the option editing line Bottom Line Press the MEASURE key to return to measurement mode Baud Rate Setting Menu Screen Enter serial ports baud rate by Pressing the UP DOWN arrow keys to change the selection Press the RIGHT ARROW key to accept the selection and select the RS 232 Setup Menu line Top Line Press the MEASURE key to return to measurement mode Output Format S...

Page 93: ...ff nothing other than the header will get printed PH 10 45 pH MV 183 3 mV Temperature Temperature 25 0 C Blank line Conductivity Conductivity 1413 uS cm Conductance Conductance 30 2 mS Temperature Temperature 25 0 C Temp Coefficient Temp Coefficient 10 0 C or OFF or NLF Temp Reference Temp Reference 25 0 C Cell Constant Cell Constant 1 00 cm Blank line Concentration Concentration 100 0 mg L Satura...

Page 94: ... top line the date of the log point on the middle line and the year of that log point on the bottom line a Use the Up Down arrow key to scroll to different time and dates or hit the Log View Button to view the log point b In viewing the log point use the Up Down scroll view key to different log points or press the Log View key to return to the Time Date selection screen c Press the MEAS key to esc...

Page 95: ...rror E1 Setup Event or Error E8 ISE Event or Error E2 SW Event or Error E9 ORP Event or Error E3 HW Event or Error EA Conductivity Event or Error E4 Memory Event or Error EB DO Event or Error E5 ISE Event or Error EC Measurement Event or Error E6 System Events Errors Error Code Description Press MEAS to Clear Cause Trouble Shooting E001 No Model Number Yes Memory Corrupted Call Customer Service E0...

Page 96: ...r Service E035 Password Wrong Yes User entered incorrect password Re enter the password If you have forgotten your pass word contact Customer Service E036 User Entered Wrong Value Yes User entered value is out of range Re enter value Check speciﬁca tions for range of correct values pH Events Errors Error Code Description Press MEAS to Clear Cause Trouble Shooting E105 Auto Buffer Failure Yes Auto ...

Page 97: ...uracy 0 2 mV or 0 5 whichever is greater 3 Star ISE ISE Concentration Range 0 0 to 19 900 0 Units M mg L ppb none Resolution 1 2 or 3 sig Digits Relative Accuracy 0 2 mV or 0 05 whichever is greater mV RmV 1999 9 3 Star DO DO Concentration 0 000 to 90 00 mg L Relative Accuracy 0 2 mg L Saturation 0 0 to 600 Salinity factor 0 to 45 ppt Barometric pressure 450 850 mm Hg X 1 Orion Star Series Meter T...

Page 98: ...001 to 199 9 Reference temperature 15 C 20 C or 25 C default autoranging 4 Star Meter Speciﬁcations Benchtop and Portable 4 Star pH ISE pH Range 2 000 to 19 999 Resolution 0 1 0 01 0 001 Relative accuracy 0 002 ISE Concentration Range 0 0 to 19 900 0 Units M mg L ppb none Resolution 1 2 or 3 sig Digits Relative Accuracy 0 2 mV or 0 05 whichever is greater mV RmV 1999 9 ORP mV RmV Eh Range 1999 9 R...

Page 99: ...RP mV RmV Eh Range 1999 9 Resolution 0 1 Relative accuracy 0 2 mV or 0 5 whichever is greater 4 Star pH Conductivity pH Range 2 000 to 19 999 Resolution 0 1 0 01 0 001 Relative accuracy 0 002 Conductivity Range 0 3000 mS cm cell constant dependent Resistivity 0 0001 to 100 Megohms Salinity 0 01 to 80 0 ppt NaCl TDS 0 0 to 19 999 0 mg L Cell Constant 0 001 to 199 9 Reference temperature 15 C 20 C o...

Page 100: ...curacy 0 2 mV or 0 05 whichever is greater mV RmV 1999 9 DO Concentration 0 000 to 90 00 mg L Relative Accuracy 0 2 mg L Saturation 0 0 to 600 Salinity factor 0 to 45 ppt Barometric pressure 450 850 mm Hg Conductivity Range 0 3000 mS cm cell constant dependent Resistivity 0 0001 to 100 Megohms Salinity 0 01 to 80 0 ppt NaCl TDS 0 0 to 19 999 0 mg L Cell Constant 0 001 to 199 9 Reference temperatur...

Page 101: ...mits Environmental Operating Conditions Ambient Operating Temperature 5 to 45 C Relative Humidity 5 to 85 Non Condensing Storage Temperature 20 to 60 C Storage Humidity 5 to 85 Non Condensing Case Material ABS Shock and Vibration Vibration Shipping Handling Per ISTA 1A Shock Drop Test in Packaging Per ISTA 1A Enclosure IP67 Portable Meter IP54 Benchtop Meter ...

Page 102: ...Thermo Electron Corporation X 6 Orion Star Series Meter ...

Page 103: ...ting and signed by Seller and Buyer Seller s failure to object to terms contained in any subsequent communication from Buyer will not be a waiver or modification of the terms set forth herein All orders are subject to acceptance in writing by an authorized representative of Seller 2 Warranty Thermo Electron warranty for Orion products covers failures due to manufacturer s workmanship or material d...

Page 104: ...ver is earlier provided use is in accordance with the operating limitations and maintenance procedures in the instruction manual and when not having been subjected to accident alteration misuse abuse or breakage of electrodes Thirty six months from date of purchase by the user or forty two months from date of shipment fromThermo Electron All Orion Star Series pH ISE DO and Conductivity Meters Orio...

Page 105: ...d Line pH Electrodes Tris pH Electrodes KNIpHE electrode ORP Triode Orion 9180BN pHuture pH Probes Orion 616500 and pHuture MMS Quatrode and Triode Orion 616600 and 617900 Orion 97 08 DO Probe Series 100 Conventional Conductivity Cells temperature probes and compensators except those models noted Orion 93 and 97 ionplus Series sensing modules are warranted to give six months of operation if placed...

Page 106: ...ement please visit our website at www thermo com THE WARRANTIES DESCRIBED ABOVE ARE EXCLUSIVE AND IN LIEU OF ALL OTHER WARRANTIES WHETHER STATUTORY EXPRESS OR IMPLIED INCLUDING BUT NOT LIMITED TO ANY IMPLIED WARRANTY OF MERCHANTABILITY OR FITNESS FOR A PARTICULAR PURPOSE AND ALL WARRANTIES ARISING FROM THE COURSE OF DEALING OR USAGE OF TRADE THE BUYER S SOLE AND EXCLUSIVE REMEDY IS FOR REPAIR OR R...

Page 107: ...QUIPMENT LOSS OF REVENUE LOSS OF DATA LOSS OF PROFITS OR LOSS OF GOODWILL REGARDLESS OF WHETHER SELLER a HAS BEEN INFORMED OF THE POSSIBILITY OF SUCH DAMAGES OR b IS NEGLIGENT 4 Miscellaneous a The rights and obligations of the parties hereunder shall be governed by and construed in accordance with the laws of the Commonwealth of Massachusetts without reference to its choice of law provisions Each...

Page 108: ...Thermo Electron Corporation XI 6 Orion Star Series Meter ...

Page 109: ...nd benchtop 4 Star pH Cond portable 4 Star pH DO benchtop 4 Star pH DO portable 4 Star pH ISE benchtop 4 Star pH ISE portable 3 Star Cond benchtop 3 Star Cond portable 3 Star DO benchtop 3 Star DO portable 3 Star pH Benchtop 3 Star pH portable Directive Standard 89 336 EEC Electromagnetic Compatibility EMC Directive EN 61326 1997 A1 1998 A2 2001 Electrical equipment for measurement control and lab...

Page 110: ...use general requirements These products have been manufactured in compliance with the provisions of the relevant Thermo Electron manufacturing and test documents and processes Further these documents and processes are recognized as complying with ISO9001 2000 by QMI listed as File 001911 Place and date of issues Beverly MA February 22 2005 ______________________________ Robert Manning Manager of Q...

Page 111: ...oration Environmental Instruments Water Analysis Instruments 166 Cummings Center Beverly MA 01915 USA Tel 978 232 6000 Toll Free 800 225 1480 Dom Fax 978 232 6015 Int l Fax 978 232 6031 www thermo com water 248590 001 RevA ...

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