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Seres OL SOL-96.110.071, Operator'S Manual

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Seres OL SOL-96.110.071 Operator'S Manual Download Page 43

SOL-96.110.071 / 180122

TOPAZ Aluminum

Maintenance

41

 

6.6.2

Zero Calibration

Note: 

• On multi-channel instruments, only calibrate sample stream 1.

Procedure

The procedure is similar to the manual measurement procedure 

described in 

Manual Measurement, p. 40

. Use deionized water in

-

stead of standard.

Results

screen

At the end of the zero calibration, a window displays the previous 

(actual) and the new (calculated) offset. Confirm by pressing the   

button.

6.6.3

Standard Calibration

Note: 

• On multi-channel instruments, only calibrate sample stream 1.

Procedure

The procedure is similar to the manual measurement procedure 

described in 

Manual Measurement, p. 40

.

Begin calibration by entering the reference value of the standard 

used. Pay attention to the correct concentration unit (ppb by default). 

Then follow the instructions on the screen.

Results

screen

At the end of the standard calibration, a window displays the previ

-

ous (actual) and the new (calculated) calibration coefficient and the 

concentration measurement readings before and after calibration. 

Confirm by pressing the   button.

CALIBRATION ZERO RESULTS

Actual offset
Offset Calculated

-0.1

0.2

CALIBRATION RESULTS

Actual coefficient
Coef. Calculated
Measure before calib
Measure after calib

1.040

1.047

20.15

20.00

Summary of Contents for SOL-96.110.071

Page 1: ...TOPAZ Aluminum Operator s Manual TOPAZ Aluminum SOL 96 110 071 180122...

Page 2: ...ed staff of technical specialists around the world For any technical question contact your nearest Seres OL representa tive or the manufacturer Seres OL SAS ZA de la Sipi re 219 Avenue de Provence FR...

Page 3: ...s on I O Board 14 3 4 2 Cable thicknesses 18 3 4 3 AC power 19 3 4 4 Jbus via RS485 20 3 4 5 Jbus via TCP IP Option 21 4 Startup 22 4 1 Installing the Reagent Bottles 22 4 2 Starting Sample Flow 23 4...

Page 4: ...inum 2 6 6 3 Standard Calibration 41 6 7 Longer Stop of Operation 42 7 Configuration of the Analyzer 43 8 Troubleshooting 47 8 1 What To Do If 47 8 2 List of Errors and Alarms 51 8 3 Saving Diagnostic...

Page 5: ...ty instructions are given throughout this manual at the respective locations where observation is most important Strictly follow all safety instructions in this publication Target audience Operator Qu...

Page 6: ...the prevention instructions carefully WARNING Severe injuries or damage to the equipment can occur if such warnings are ignored Follow the prevention instructions carefully CAUTION Damage to the equi...

Page 7: ...071 180122 TOPAZ Aluminum Safety Instructions 5 Warning signs The warning signs in this manual have the following meaning Electrical shock hazard Corrosive Harmful to health Flammable Hot surface Gene...

Page 8: ...ordance with the local regula tions of the respective country WARNING Electrical shock hazard If proper operation is no longer possible the instrument must be disconnected from all power lines and mea...

Page 9: ...er and check it for visible damage If the analyzer shows any visible damage do not connect it to power and contact customer service immediately 1 4 International Symbols Used The symbols found on the...

Page 10: ...channels common measuring range Signal outputs Two signal outputs per measuring channel Current loop 4 20 mA Relays Five potential free contacts per measuring channel with the following functions two...

Page 11: ...nces and dust Process connections Sample inlet Sample outlet Sample outlet waste 1 4 BSP F soft tubing D INT 9 single channel soft tubing D INT 19 multi channel soft tubing D INT 12 Sample requirement...

Page 12: ...180122 TOPAZ Aluminum Product Description 10 Wall cabinet Material Screws Weight Protection degree Stainless steel SS316L 4x M6 6x M6 with reagent shelf 35 kg IP55 Reagent shelf made of SS316L availab...

Page 13: ...scription 11 2 2 Instrument Overview A B C D E F G H I J K Power switch Touchscreen Cable glands Peristaltic pumps Photometer Air cleaning inlet Pressure reducing device Calibration vessel Sample inle...

Page 14: ...ca tions p 9 3 2 Mounting the Wall Cabinet Mounting requirements Mount the instrument in vertical position The display should be at eye level to simplify operation and maintenance For dimensions see d...

Page 15: ...the instrument from a power outlet which has a protec tive earth connection Overview of electrical connections 1 In multi channel instruments there is an I O board for each measuring channel The I O b...

Page 16: ...d to control internal components of the analyzer Do not connect anything else to these contacts Analog signal output OUT_ANA2 is reserved for customized versions of the analyzer that provide a second...

Page 17: ...pins 1 and 4 unconnected Analog signal outputs 4 20 mA Name Available on Description IN_DIG1 all measuring channels Activates or deactivates the measuring channel Open contact Measuring channel will b...

Page 18: ...e Analyzer p 43 Name Available on Description OUT_DIG2 all measuring channels Sample flow alarm OUT_DIG3 all measuring channels Threshold 1 OUT_DIG4 all measuring channels Threshold 2 OUT_DIG5 all mea...

Page 19: ...onfigured as normally open or normally closed by setting the corresponding jumpers on the I O board The default setting is normally open jumper in the right position A Location of jumpers on I O board...

Page 20: ...luminum Installation 18 3 4 2 Cable thicknesses In order to comply with IP55 use the following cable thicknesses Note Seal cable glands that are not in use A B Outer diameter of cable 7 5 13 mm Outer...

Page 21: ...0122 TOPAZ Aluminum Installation 19 3 4 3 AC power Ferrite Wrap the mains cable two times around the supplied ferrite A B C Protective earth PE terminal 3 Neutral conductor terminal 2 Phase conductor...

Page 22: ...SOL 96 110 071 180122 TOPAZ Aluminum Installation 20 3 4 4 Jbus via RS485 Terminals Terminal 1 data B terminal 2 data A A RS485 interface A...

Page 23: ...lyzer The connection is made via the Ethernet port located on the right side of the analyzer exterior Mount the supplied connector onto the Ethernet cable and connect it to the port Addressing modes T...

Page 24: ...f all reagent tubes are cut at an angle This will prevent the tube ends from lying flat on the bottom of the bot tles 2 Check that there are two holes in the lid of each reagent bottle one hole to fee...

Page 25: ...122 TOPAZ Aluminum Startup 23 4 2 Starting Sample Flow Open the sample tap C so that a part of the sample overflows into the pressure reduction device A A B C Pressure reduction device Inner tube Samp...

Page 26: ...ically readjusted and the panel PC starts 2 Stop the measuring cycle by pressing the button and entering the password 0712 3 Open the TOOLS tab and press the Electrical test button Check transparent r...

Page 27: ...6 6 2 8 Let the pump run until the fluid has reached the photometer and there is no more air in the tube This takes approximately 2 5 minutes The pump stops automatically 9 Repeat steps 7 8 with pumps...

Page 28: ...R tab 11 Set SV Emptying to ON and SV Filling to OFF and wait until the instrument is empty 12 Then set SV Emptying and Stirrer to OFF as well ON ON ON ON OFF OFF OFF OFF Stirrer SV Emptying Heating S...

Page 29: ...ter and wait until the reagent arrives in the photometer This takes approximately 2 5 minutes The pump stops automatically 17 Go back to the ACTUATOR tab 18 Set Stirrer to ON 19 Check that the stirrer...

Page 30: ...ecessary 2 Calibrate the analyzer if required For detailed descriptions see Manual Measurement and Calibration p 39 4 6 Programming Program the following parameters if applicable Concentration values...

Page 31: ...d access levels User access Allows viewing data in the main window Access with extended permissions Allows stopping the measurement changing settings and performing maintenance tasks The password for...

Page 32: ...last manual measurement C Measured value D Trend E Measuring cycle information Stream that is being measured Number and description of step in measurement cycle Total number of steps to be completed...

Page 33: ...esult is satisfactory no calibration is needed If necessary calibrate the instrument Every 3 months Replace all peristaltic pump tubes After replacement of peristaltic pump tubes perform a manual meas...

Page 34: ...ubes one after the other not simultaneously Proceed as follows 1 Remove all reagent tubes from their bottles and place them in a beaker filled with deionized water 2 Open the PUMPS tab 3 Press the ON...

Page 35: ...ACTUATOR tab and set SV Filling to ON 7 Wait until the photometer has been filled with fresh water Then set SV Filling to OFF ON ON ON ON OFF OFF OFF OFF Stirrer SV Emptying Heating SV Filling ACTUATO...

Page 36: ...ntamination or dilution errors Reagent consumption At the standard measurement interval the following amounts of reagents are consumed Replacing reagents 1 Prepare the reagents according to the separa...

Page 37: ...Hexamethylenetetramine PTFE 1 6 3 2 21 Phenantrolin PTFE 1 6 3 2 22 Phenantrolin PTFE 1 6 3 2 31 Pyrocatechol violet PTFE 1 6 3 2 black 32 Pyrocatechol violet PTFE 1 6 3 2 black 91 HCl 2N Al 400 g l...

Page 38: ...SVB NC Silicone 5 8 Calibration vessel B SVB NO Silicone 5 8 SVB C Sample inlet right of photometer D Silicone 5 8 Water fault sensor U1 Silicone 2 5 Photometer sample outlet left SVA NC Tygon 5 8 SV...

Page 39: ...ear appropriate protective equipment gloves glasses protective clothing 1 Flush the reagent tubes with deionized water as described in Stop of Operation for Maintenance p 32 2 Turn the power switch to...

Page 40: ...the tube around the rotor while turning it 6 Connect the other tube end to the left side fitting 7 Install the front cover on the pump 8 Insert the reagent tubes all the way to the bottom of the corre...

Page 41: ...ntact customer service for details Entering the maintenance menu 1 To stop the current measuring cycle press the button on the main screen and enter the password 0712 In the next dialog confirm with O...

Page 42: ...l A with the standard 3 Wait until the calibration vessel is empty and the message Add standard appears again 4 Repeat steps 2 and 3 until the measurement starts automatically 5 When the measurement i...

Page 43: ...stream 1 Procedure The procedure is similar to the manual measurement procedure described in Manual Measurement p 40 Begin calibration by entering the reference value of the standard used Pay attentio...

Page 44: ...as follows 1 Prime the reagent system with deionized water as described in Stop of Operation for Maintenance p 32 2 Clean the photometer thoroughly with diluted hydrochloric acid Note Do not use a bot...

Page 45: ...by Seres OL customer service pressure setting Setpoint of the water fault sensor Adjust this value only if instructed to do so by Seres OL customer service Gain setpoint Setpoint of the electronic ga...

Page 46: ...n mea surement cycles Note Since the analyzer is designed for continuous operation a maximum duration of 15 minutes is recommended for pauses 1 Press the Add button and select one of the following opt...

Page 47: ...3 and OUT_DIG4 are high or low thresholds The combinations high high low high and low low are possible The threshold values can be set in the parameter menu see 46 DATE TIME tab Set time and date A B...

Page 48: ...ld value is made in the THRESHOLD tab of the OPTIONS menu Threshold 2 Threshold value for relay OUT_DIG4 The definition as high or low threshold value is made in the THRESHOLD tab of the OPTIONS menu...

Page 49: ...r message Water default although there is sample flow Possible cause Corrective action No power on the socket Check mains power supply Power supply defective Check output voltage of the internal 24 vo...

Page 50: ...ptying solenoid valve SVA does not switch Check that the solenoid valve is plugged in correctly If necessary change the membrane Possible cause Corrective action Pump does not work properly Check that...

Page 51: ...passed or if the reagents have been stored incorrectly If necessary replace the reagents Check that the reagents are of Analysis Use quality ask supplier Tubes connected to the wrong reagent containe...

Page 52: ...s working correctly if present If no filter system is installed it might be necessary to install one Water does not drain Check that the drain is pressure free and not blocked Check condition of empty...

Page 53: ...If the error persists contact customer support 5 Error reading cycle zero configuration Reset analyzer configuration to factory defaults by pressing the Recover button in the tab 6 Error writing cycle...

Page 54: ...ve optical measure value in the DIAGNOSTIC tab With a functioning measuring card the value changes continuously If the value does not change restart the analyzer and check again If the error persists...

Page 55: ...e INPUT tab and test the digital inputs If the error persists contact customer support 20 Error reading on IO card Check if all I O boards work properly Navigate to TOOLS Electrical test Open the RELA...

Page 56: ...utton in the tab 25 Error reading on JBUS slave card Check request compliance with JBUS protocol 26 Error treatment on JBUS slave card Check request compliance with JBUS protocol 27 Error reading meas...

Page 57: ...replace the membrane Check sample tubes 33 Optical setting Default Info setting not received Observe the Live optical measure value in the DIAGNOSTIC tab With a functioning measuring card the value c...

Page 58: ...ncentration after linearization 0 or Calibra tion Coeff 0 Check if the calibration coefficient is equal to zero In this case make a new calibration Check if the final absorbance is equal to zero If th...

Page 59: ...ue out of range Check that the analyzer is well calibrated check standard solution concentration by a manual measure cycle 45 Division by zero Absorbance 999998 0 Check that the optical fibers are wel...

Page 60: ...255 analyzer cannot adjust the optical gain Check that the optical fibers are well connected to their holder on the door Check that the photometer is not dirty Check that the analyzer is supplied wit...

Page 61: ...USB stick into the USB port A on the back of the panel PC 3 Open the TOOLS tab and press the Log files copy button Enter the password 0712 if necessary 4 On the next screen press OK to start data tra...

Page 62: ...TOPAZ Aluminum Notes SOL 96 110 071 180122 60 9 Notes...

Page 63: ...SOL 96 110 071 180122 TOPAZ Aluminum Notes 61...

Page 64: ...i l G a s Seres OL SAS FR 13730 Saint Victoret www seres ol com info seres ol com Seres OL Products Analytical Instruments for Seres OL is represented worldwide by subsidiary companies and distributor...

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