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© Retsch GmbH, 42781 Haan, Retsch-Allee 1-5, Germany 21.05.2015 0001

Manual

Ball Mill XRD-Mill McCrone

Translation

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Summary of Contents for XRD-Mill McCrone

Page 1: ... Retsch GmbH 42781 Haan Retsch Allee 1 5 Germany 21 05 2015 0001 Manual Ball Mill XRD Mill McCrone Translation ...

Page 2: ...2 Copyright Copyright by Retsch GmbH Haan Retsch Allee 1 5 D 42781 Haan Federal Republic of Germany ...

Page 3: ...3 ...

Page 4: ...place of installation 15 4 5 Installation of the machine 15 4 6 Type plate description 15 4 7 Electrical connection 16 4 8 Installation of the machine 16 4 8 1 Screw connection with mounting brackets 17 4 8 2 Screw connection of the device from underneath 17 4 8 3 Attaching with Powerstrips 18 4 8 4 Drill template 18 5 Operating the machine 19 5 1 Views of the Instrument 19 5 2 Overview table of t...

Page 5: ...5 8 1 Cleaning 29 8 2 Replacing the machine fuses 31 8 3 Returning for service and maintenance 32 9 Disposal 33 10 Index 35 Appendix following page ...

Page 6: ...ice This operating manual does not contain any repair instructions If faults arise or repairs are necessary please contact your supplier or get in touch with Retsch GmbH directly Application technology information relating to samples to be processed is not included but can be read on the Internet on the respective device s page at www retsch com Pos 1 1 3 0010 ELTR A 0005 R ETSCH 0005 R ETSCH Bedi...

Page 7: ...arnings and corresponding content WARNING Type of danger personal injury Source of danger Possible consequences if the dangers are not observed Instructions on how the dangers are to be avoided We also use the following signal word box in the text or in the instructions on action to be taken WARNING Moderate or mild injury may result from failing to heed these safety warnings We give you the follo...

Page 8: ...y of knowing the contents of this operating manual Target group All persons concerned with the machine in any form This machine is a modern high performance product from Retsch GmbH and complies with the state of the art Operational safety is given if the machine is handled for the intended purpose and attention is given to this technical documentation You as the owner managing operator of the mac...

Page 9: ... 0 mod_1228722954535_9 docx 4079 1 This operating manual does not contain any repair instructions For your own safety repairs may only be carried out by Retsch GmbH or an authorized representative or by Retsch service engineers In that case please inform The Retsch representative in your country Your supplier Retsch GmbH directly Your Service Address Pos 1 3 1 0010 ELTR A 0005 R ETSCH 0010 R ETSCH...

Page 10: ...ator owner that s he has received sufficient instructions about the operation and maintenance of the system The user has received the operating manual has read and taken note of its contents and consequently has all the information required for safe operation and is sufficiently familiar with the device As the owner managing operator you should for your own protection have your employees confirm t...

Page 11: ... substances can be ground easily fast and without loss Use of the machine for the intended purpose CAUTION Risk of explosion or fire Changing sample properties Consider that the properties and therefore also the hazardousness of your sample can change during the grinding process Do not use any substances in this device which carry the risk of explosion or fire CAUTION Risk of explosion or fire On ...

Page 12: ... R ETSCH Bedienungsanlei tungen Kapitelsamml ung en 0005 milling XRD Mill McCrone Modulordner 0010 Technische Daten XRD Mill McCrone 1030 M odul M otordr ehzahl XRD Mill McCrone 9 mod_1427186072151_9 docx 76443 1 The speed can be adjusted within the following 1050 Four speed levels can be set Pos 2 19 0025 Überschriften 1 1 Ü berschriften 1 1 Ü berschriften BDA 11 Emmisionen 0 mod_1226487095021_9 ...

Page 13: ...ight up to approx Weight XRD Pos 2 27 0025 Überschriften 1 1 Ü berschriften 1 1 Ü berschriften BDA 11 Erfor derliche Standfläche 0 mod_1226492678414_9 docx 3364 2 1 3 9 Required floor space Pos 2 28 0005 RETSCH 0005 R ETSCH Bedienungsanlei tungen Kapitelsamml ung en 0005 milling XRD Mill McCrone Modulordner 0010 Technische Daten XRD Mill McCrone 1060 M odul Standfl äche XRD Mill McCrone 9 mod_1427...

Page 14: ... 3398 2 1 4 2 Transport Pos 3 1 7 0030 Warnhinweise H0017 HIN WEIS Transport 0 mod_1228918883019_9 docx 4802 1 NOTICE Transport Mechanical or electronic components may be damaged The machine may not be knocked shaken or thrown during transport Pos 3 1 8 0030 Warnhinweise H0014 HIN WEIS Rekl amationen 0 mod_1228918881767_9 docx 4760 1 NOTICE H0014 Complaints The forwarding agent and Retsch GmbH mus...

Page 15: ...464 2 1 4 5 Installation of the machine Pos 3 1 15 0005 RETSCH 0099 R ETSCH Standard Kapitel Modul e_StandardkapitelAufstellungshöhe Gener al 0 mod_1228918538349_9 docx 4724 1 Installation height maximum 2000 m above sea level Pos 3 1 16 1 0025 Überschriften 1 1 Ü berschriften 1 1 Ü berschriften BDA 11 Typenschil d Beschrei bung 3 mod_1280933953941_9 docx 22302 2 1 4 6 Type plate description Pos 3...

Page 16: ...tions underneath the mounting surface Pay attention to the length of screws Transport scope of delivery installation WARNING When connecting the power cable to the mains supply use an external fuse complies with the regulations applicable to the place of installation Please check the type plate for details on the necessary voltage and frequency for the device Make sure the levels agree with the ex...

Page 17: ...iency the mill must be fixed securely to a stable bench Align the supplied drill template to the bench Drill the four holes in the bench using the marked drilling positions Align the device between the drilled holes Slide the supplied mounting brackets VBL into the designated cut Where possible use the screws supplied VBS Screw the device tight Use the following parameters as a guide when selectin...

Page 18: ...strips Stick eight Powerstrips to the base plate of the device Use the marked positions BP on the drill template as a guide Peel the protective film off the Powerstrips After positioning it will no longer be possible to move the device Place the device in the desired target position Use the following parameters as a guide when selecting the installation site and installation materials Powerstrips ...

Page 19: ...schriften BD A 11 Ansichten des Ger ätes R etsch 0 mod_1228990581782_9 docx 4966 2 1 5 1 Views of the Instrument Pos 4 4 0005 R ETSCH 0005 RETSCH Bedienungsanl eitung en Kapi telsammlungen 0005 milling XRD Mill McCr one M odulor dner 0020 Bedienung XRD Mill McCrone 2000 M odul Ansichten des Ger ätes 9 mod_1427186271594_9 docx 76599 1 Fig 4 Front view of the device Fig 5 Close up of grinding chambe...

Page 20: ...Function A Soundproof hood Closes the grinding chamber B Control panel Device controller C Grinding jar clamping bracket Clamps grinding jar on the support D Grinding jar support Support for grinding jar E Main switch Disconnects the device from the mains F IEC socket Power supply for the power cable G Entry for fuse Access to the device fuse H Type plate Description of device parameters I Warning...

Page 21: ...DA 11 Ü bersichtstabelle der Bedienel emente und der Anzeige 0 mod_1228990697273_9 docx 4978 2 1 5 4 Overview Table of the Operating Elements and the Display Pos 4 11 0005 RETSCH 0005 R ETSCH Bedienungsanlei tungen Kapitelsamml ung en 0005 milling XRD Mill McCrone Modulordner 0020 Bedienung XRD Mill McCr one 2010 M odul Ü bersichtstabelle der Bedi enel emente und der Anzeige 9 mod_1427186277273_9 ...

Page 22: ...presence of abrasive composite considerably reduce t When grinding electronic scrap take the properties of the composite materials into account Inserting the grinding jar CAUTION Risk of personal injury Ejected sample material Take the appropriate steps required to rule out the risk of injuries according to the danger posed by your sample Only start grinding when using the soundproof hood Reductio...

Page 23: ... up to the bottom of the grinding jar NOTICE For each grinding operation place 6 grinding bodies MK each in all 8 chambers Then remove the applicator The sample volume during a single grinding process must not exceed 5 millilitres The ideal grinding efficiency is achieved with a sample volume of 2 millilitres This corresponds to a weight of 10g for a material with a density of 5g per millilitre or...

Page 24: ...Operating the machine 24 Fig 9 Removing the soundproof hood Fig 10 Grinding jar clamping bracket Pull the grinding jar clamping bracket KB forwards and rotate it upwards SH KB ...

Page 25: ... fits closely against the front edge of the grinding jar support Fig 12 Clamping the grinding jar When using the grinding jar lid with groove it is necessary to ensure that the clamping bracket clicks into place in the groove anti rotation protection Pull the clamping bracket KB forwards and rotate it by180 degrees downwards until it clicks into place ME KB ...

Page 26: ...n hole pouring lid DK Pour the contents of the grinding jar into a glass beaker or bowl Pos 4 18 0005 RETSCH 0005 R ETSCH Bedienungsanlei tungen Kapitelsamml ung en 0005 milling XRD Mill McCrone Modulordner 0020 Bedienung XRD Mill McCr one 2030 M odul Tr ockenver mahlung XRD Mill McCrone 9 mod_1427186437237_9 docx 76676 3 1 5 5 3 Dry grinding Shake the grinding jar gently to ensure that the sample...

Page 27: ...er ätes XRD Mill McCrone 2510 M odul Displayei nheit Bedi enung des Gerätes XRD Mill McCrone 9 mod_1427186756059_9 docx 76727 33 1 6 1 1 Speed Display of the speed level set You can select one of the four speed levels 6 1 2 Time Display of the grinding time The grinding time can be set at intervals of 10 seconds To adjust press the or Pos 6 1 0005 R ETSCH Seitenumbr uch 6 mod_1377697736040_0 docx ...

Page 28: ...ew the bottom section UT onto the steel container SB Place one grinding body MK either polycrystalline corundum supplied or tungsten carbide available separately in the stainless steel cylinder Put the sample PE in the cylinder and place the other grinding body on top of the sample Guide the steel plunger SE up to the second grinding body in the cylinder and hit the plunger hard several times usin...

Page 29: ...ther cleaning cycle is sufficient Wait until the product and rinsing liquid in the beaker or bowl has settled then pour off the clear liquid If water has been used as grindi acetone may be added after pouring the liquid off and the mixture then drained again The draining and drying phases can be considerably accelerated by using acetone in place of water A dried product can be obtained quickly usi...

Page 30: ...ilable information regarding durability Pos 7 8 0030 Warnhinweise H0070 HIN WEIS Aceton kann den PVC D eckel beschädigen XRD Mill 9 mod_1427352201170_9 docx 77311 1 Pos 7 9 0025 Ü berschriften 1 1 Überschriften 1 1 Überschriften BD A 11 Austausch der Ger ätesicherungen R etsch 0 mod_1228833758657_9 docx 4426 2 1 NOTICE H0070 Acetone may damage the PVC lid Contact between the lid and acetone should...

Page 31: ...new fuses Place the fuse holder with the inserted fuses into the opening GL Cleaning and service Replacing the machine fuses WARNING Mortal danger from electric shock Exposed power contacts When replacing fuses on the cutout or fuse adapter you may come into contact with live contacts An electric shock can lead to burns and to cardiac arrhythmias or to respiratory arrest and cardiac arrest Remove ...

Page 32: ... goods dispatch note RETSCH devices and accessories can only be accepted for repair maintenance or calibration if the returned goods despatch note has been correctly completed in full When returning a device attach the returned goods dispatch note to the outside of the packaging In order to eliminate any health risk to our employees we reserve the right to refuse acceptance and to return the respe...

Page 33: ... machines in the European Community Within the European Community the disposal of electrically operated devices is regulated by national provisions that are based on the EU Directive 2002 96 EC on Waste Electrical and Electronic Equipment WEEE Accordingly all machines supplied after 13 08 2005 in the business to business area to which this product is classified may no longer be disposed of with mu...

Page 34: ...34 ...

Page 35: ... size maximum 12 feed size 12 Front view of the device 19 Function 20 21 27 Fuse strength 15 Fuse type 15 G General safety instructions 8 Grinding jar nominal volume 12 Grinding jar clamping bracket 24 Grinding process preparation 22 Grinding set 12 H Height 13 I Inserting the grinding jar 24 Inserting the grinding jar 22 Installation height 15 Installation of the machine 15 16 L LpAeq 13 LWA 13 M...

Page 36: ...in the Display Unit 26 T Target group 8 Technical data 11 Temperature fluctuation and condensed water 14 Time 27 Transport 14 Transport scope of delivery installation 14 Type plate 16 type plate description 15 Type plate lettering 15 U Use of the machine for the intended purpose 11 Use of the mortar 28 V View of the back of the device 20 View of the control panel 21 View of the menu in the display...

Page 37: ...s validity Retsch GmbH Haan April 2016 Dr Ing Frank Janetta Manager Development Retsch GmbH Retsch Allee 1 5 42781 Haan Germany w w w retsch com BALL MILL XRD MILL McCrone 20 770 xxxx CERTIFICATE OF CE CONFORMITY Translation Certificate of CE Conformity according to EC Mechanical Engineering Directive 2006 42 EC Applied harmonized standards in particular DIN EN ISO 12100 Security of machines EC Di...

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Page 40: ...Copyright Copyright by Retsch GmbH Haan Retsch Allee 1 5 D 42781 Haan Federal Republic of Germany ...

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